GB494214A - Improvements in the treatment of organic acid anhydrides - Google Patents

Improvements in the treatment of organic acid anhydrides

Info

Publication number
GB494214A
GB494214A GB34757/37A GB3475737A GB494214A GB 494214 A GB494214 A GB 494214A GB 34757/37 A GB34757/37 A GB 34757/37A GB 3475737 A GB3475737 A GB 3475737A GB 494214 A GB494214 A GB 494214A
Authority
GB
United Kingdom
Prior art keywords
acid anhydrides
hypochlorite
treatment
organic acid
anhydride
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB34757/37A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Acordis UK Ltd
Original Assignee
British Celanese Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by British Celanese Ltd filed Critical British Celanese Ltd
Publication of GB494214A publication Critical patent/GB494214A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/54Preparation of carboxylic acid anhydrides
    • C07C51/573Separation; Purification; Stabilisation; Use of additives

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Epoxy Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Aliphatic acid anhydrides are freed from sulphur and labile organo-sulphur compounds by treating with a hypochlorite. The anhydride may be stirred with the hypochlorite and left in contact therewith for some time, decanted, and distilled with sodium acetate. In examples, calcium hypochlorite (bleaching powder having 68 per cent available chlorine) is used. The mixture of anhydride and sodium acetate is heated to about 132 DEG C. cooled, and distilled under vacuum. Specification 100,450, [Class 2 (iii)], is referred to.
GB34757/37A 1936-12-24 1937-12-15 Improvements in the treatment of organic acid anhydrides Expired GB494214A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US494214XA 1936-12-24 1936-12-24

Publications (1)

Publication Number Publication Date
GB494214A true GB494214A (en) 1938-10-21

Family

ID=21959740

Family Applications (1)

Application Number Title Priority Date Filing Date
GB34757/37A Expired GB494214A (en) 1936-12-24 1937-12-15 Improvements in the treatment of organic acid anhydrides

Country Status (1)

Country Link
GB (1) GB494214A (en)

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