GB2503838B - Electrolytic exfoliation of graphite - Google Patents
Electrolytic exfoliation of graphiteInfo
- Publication number
- GB2503838B GB2503838B GB1317934.6A GB201317934A GB2503838B GB 2503838 B GB2503838 B GB 2503838B GB 201317934 A GB201317934 A GB 201317934A GB 2503838 B GB2503838 B GB 2503838B
- Authority
- GB
- United Kingdom
- Prior art keywords
- graphite
- electrolytic exfoliation
- exfoliation
- electrolytic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B1/00—Electrolytic production of inorganic compounds or non-metals
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/15—Nano-sized carbon materials
- C01B32/182—Graphene
- C01B32/184—Preparation
- C01B32/19—Preparation by exfoliation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/20—Graphite
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/20—Graphite
- C01B32/21—After-treatment
- C01B32/22—Intercalation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/20—Graphite
- C01B32/21—After-treatment
- C01B32/22—Intercalation
- C01B32/225—Expansion; Exfoliation
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB1104078.9A GB2488825A (en) | 2011-03-10 | 2011-03-10 | Electrolytic exfoliation of graphite |
PCT/GB2012/050487 WO2012120291A1 (en) | 2011-03-10 | 2012-03-05 | Electrolytic exfoliation of graphite |
Publications (3)
Publication Number | Publication Date |
---|---|
GB201317934D0 GB201317934D0 (en) | 2013-11-27 |
GB2503838A GB2503838A (en) | 2014-01-08 |
GB2503838B true GB2503838B (en) | 2017-10-25 |
Family
ID=43980774
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB1104078.9A Withdrawn GB2488825A (en) | 2011-03-10 | 2011-03-10 | Electrolytic exfoliation of graphite |
GB1317934.6A Active GB2503838B (en) | 2011-03-10 | 2012-03-05 | Electrolytic exfoliation of graphite |
Family Applications Before (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB1104078.9A Withdrawn GB2488825A (en) | 2011-03-10 | 2011-03-10 | Electrolytic exfoliation of graphite |
Country Status (2)
Country | Link |
---|---|
GB (2) | GB2488825A (en) |
WO (1) | WO2012120291A1 (en) |
Families Citing this family (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2585403A4 (en) | 2010-06-25 | 2016-07-13 | Univ Singapore | Methods of forming graphene by graphite exfoliation |
GB2523154B (en) | 2014-02-14 | 2016-04-27 | Cambridge Entpr Ltd | Method of producing graphene |
EP2933356A1 (en) * | 2014-04-17 | 2015-10-21 | Basf Se | Two-dimensional carbon materials prepared by electrochemical exfoliation |
CN105088261B (en) * | 2014-05-14 | 2017-10-20 | 国能纳米科技有限公司 | The preparation method of graphene |
CN104264179B (en) * | 2014-09-17 | 2016-06-22 | 中国科学院山西煤炭化学研究所 | A kind of method being prepared Graphene by graphite raw ore electrolysis |
CN104264178B (en) * | 2014-09-17 | 2016-11-30 | 中国科学院青海盐湖研究所 | A kind of electrocatalytic oxidation prepares the method for graphene oxide |
CN104894594A (en) * | 2015-05-26 | 2015-09-09 | 广东烛光新能源科技有限公司 | Graphene preparation method |
CN106542525B (en) * | 2016-10-27 | 2018-09-11 | 董兰田 | Continuous adhesive tape legal system takes stripping degumming and the packing method of graphene |
JP7148396B2 (en) * | 2017-06-15 | 2022-10-05 | 積水化学工業株式会社 | Carbon materials, electrode materials for power storage devices, and power storage devices |
DE102017223892A1 (en) * | 2017-12-29 | 2019-07-04 | Sixonia Tech Gmbh | Process for the preparation of a functionalized semiconductor or conductor material and its use |
CN111453719B (en) * | 2020-04-24 | 2022-05-24 | 湖北航天化学技术研究所 | High-quality graphene and preparation method thereof |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6406612B1 (en) * | 1999-05-20 | 2002-06-18 | Graftech Inc. | Expandable graphite and method |
US20040131533A1 (en) * | 2001-05-03 | 2004-07-08 | Spacie Christopher John | Extrusion of graphite bodies |
US7658901B2 (en) * | 2005-10-14 | 2010-02-09 | The Trustees Of Princeton University | Thermally exfoliated graphite oxide |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2004181383A (en) * | 2002-12-04 | 2004-07-02 | Nippon Telegr & Teleph Corp <Ntt> | Carbon material for storing hydrogen |
DE10328342B4 (en) * | 2003-06-24 | 2006-05-04 | Graphit Kropfmühl AG | Process for producing expanded graphite, expanded graphite and use |
GB2432830A (en) * | 2005-12-02 | 2007-06-06 | Morganite Elect Carbon | Formation of thermally anisotropic carbon material |
US8524067B2 (en) | 2007-07-27 | 2013-09-03 | Nanotek Instruments, Inc. | Electrochemical method of producing nano-scaled graphene platelets |
US7999027B2 (en) * | 2009-08-20 | 2011-08-16 | Nanotek Instruments, Inc. | Pristine nano graphene-modified tires |
-
2011
- 2011-03-10 GB GB1104078.9A patent/GB2488825A/en not_active Withdrawn
-
2012
- 2012-03-05 GB GB1317934.6A patent/GB2503838B/en active Active
- 2012-03-05 WO PCT/GB2012/050487 patent/WO2012120291A1/en active Application Filing
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6406612B1 (en) * | 1999-05-20 | 2002-06-18 | Graftech Inc. | Expandable graphite and method |
US20040131533A1 (en) * | 2001-05-03 | 2004-07-08 | Spacie Christopher John | Extrusion of graphite bodies |
US7658901B2 (en) * | 2005-10-14 | 2010-02-09 | The Trustees Of Princeton University | Thermally exfoliated graphite oxide |
Non-Patent Citations (6)
Title |
---|
ACS Nano, Vol. 5, 2011, Ching-Yuan et al., "High-quality thin graphene films from fast electrochemical exfoliation", pp. 2332 - 2339. * |
Carbon, Vol. 47, No. 1, 17 October 2008, Lin et al., Graphite nanoplatelet pastes vs. carbon black pastes as thermal interface materials , pages 395-305 * |
Electrochemistry Communications, Vol. 12, 2010, Lee et al. "A graphite foil electrode covered with electrochemically exfoliated graphene nanosheets', pp. 1419 - 1422. * |
Journal of Materials Science, Vol. 43, No. 8, 25 October 2007, Kalaitzidou et al., The nucleating effect of exfoliated graphite nanoplatelets and their influence on the crystal structure and electrical conductivity of polypropylene nanocomposites, pages 2895-2907 * |
Journal of Nanoscience and Nanotechnology, Vol. 11, 2011, Geng et al., "Effects of stage, intercalant species and expansion technique on exfoliation of graphite intercalation compound in graphene sheets", pp. 1084 - 1091. * |
Solar Energy Materials & Solar Cells, Vol. 93, No. 1, 1 November 2008, Kim et al., High latent heat storage and high thermal conductive phase change materials using exfoliated graphite nanoplatelets, pages 136-142 * |
Also Published As
Publication number | Publication date |
---|---|
GB2503838A (en) | 2014-01-08 |
GB201104078D0 (en) | 2011-04-27 |
GB2488825A (en) | 2012-09-12 |
WO2012120291A1 (en) | 2012-09-13 |
GB201317934D0 (en) | 2013-11-27 |
WO2012120291A4 (en) | 2012-12-13 |
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