GB2190078A - Porous glass rod as fibre preform - Google Patents
Porous glass rod as fibre preform Download PDFInfo
- Publication number
- GB2190078A GB2190078A GB08611440A GB8611440A GB2190078A GB 2190078 A GB2190078 A GB 2190078A GB 08611440 A GB08611440 A GB 08611440A GB 8611440 A GB8611440 A GB 8611440A GB 2190078 A GB2190078 A GB 2190078A
- Authority
- GB
- United Kingdom
- Prior art keywords
- vessel
- passage
- glass rod
- ofthe
- porous glass
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B37/00—Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
- C03B37/01—Manufacture of glass fibres or filaments
- C03B37/012—Manufacture of preforms for drawing fibres or filaments
- C03B37/014—Manufacture of preforms for drawing fibres or filaments made entirely or partially by chemical means, e.g. vapour phase deposition of bulk porous glass either by outside vapour deposition [OVD], or by outside vapour phase oxidation [OVPO] or by vapour axial deposition [VAD]
- C03B37/0144—Means for after-treatment or catching of worked reactant gases
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Manufacture, Treatment Of Glass Fibers (AREA)
- Glass Melting And Manufacturing (AREA)
Abstract
A porous glass rod 23 is fabricated using a reaction vessel 11 which includes an elevational passage between an exhaust port 12 in the vessel side and the top of the vessel over its interior and a burner 14 mounted in the vessel for forming glass fine particles, and a target 15 which is elevationally movable and rotatable and is inserted from the passage 13 into the vessel, wherein a downward gas stream is produced along the outer periphery of the passage 13 in the vessel. This can stabilize the fluid flow in the reaction vessel to stabilize the outer diameter and the refractive index distribution of the glass rod in the longitudinal direction. <IMAGE>
Description
SPECIFICATION
Method of fabricating porous glass rod and apparatus for fabricating the same
This invention relates to a method of and apparatus for fabricating a porous glass base material for an optical system such as optical fibers or rod lenses by means of a VAD (vapor-phase axial deposition) method.
When a porous glass base material for an optical system is fabricated by a VAD method, it is necessary to stabilize a gas stream in a reaction vessel in which an atmosphereforforming the base material is formed, and if the sufficient stability in the gas stream is not obtained, variations in the outer diameter and refractive index distribution of the porous glass base material increase.
To eliminate the variations, adequate means such as control of exhaust pressure ofthe reaction vessel, control of flow rate ofthe gas stream from the top to the interior of the reaction vessel orflow of the gas controlled under pressure have been conducted.
Priorart inventions for this are disclosed, for example, in Japanese Patent Laid-open Nos.
69234/1981 and 135738/1982 official gazettes.
In Figures 3(a) and 3(b) showing the example ofthe conventional invention in Japanese Patent
Laid-open No. 135738/1982, numeral 1 designates a reaction vessel having an exhaust port 2, numeral 3 designates a passage conductor inserted from the top to the interior of the vessel 1, numeral 4 designates a burner mounted at the end from the bottom to the interior ofthe vessel 1 forforming glass fine particles, numeral 5 designates a target, and numeral 6 designates a porous glass rod.
According to the conventional method exemplified in Figure 3, a predetermined gas is flowed from the conduit 3 to the lower portion in case offorming the porous glass rod 6, the clearance in the conduit3 is large atthe initial stage offorming the glass rod 6 as shown in Figure 3(a), and when the glass rod 6 is introduced into the conduit 3 as the rod 6 grows, the clearance decreases.
Therefore, asthe glass rod 6 grows,thefluidityof tile gasthrough the conduit3varies, andthe directivity oftheflame of the burner (the injecting direction of glass fine particles) in the vessel 1 also alters.
In the prior art invention disclosed in Japanese Patent Laid-open No.69234/1981, ,though omifled for the description, similar phenomenon also takes place.
Since variation occurs in the directivity ofthe flame ofthe burner in the conventional method as described above, the method cannot effectively preventthe outerdiameterorthe refractive index distribution of the porous glass rod 6 from varying in case offabricating the glass rod 6 having a desired length, and the control of the flow rate in the conduit 3 and the control of the pressure in the vessel 1 to be compensated are difficult.
On the other hand, if the inner diameter ofthe conduit 3 is increased to decrease the variation in the fluidity in the degree to be ignored, the outer diameter ofthe glass rod 6 is stabilized, but the flowing energy from the top of the vessel reduces in this case, the glass fine particles from the burner4 behave at random in the vessel 1 and the stability of the refractive index distribution of the glass rod 6 is lost.
Accordingly, an object of this invention is to provide a method of and apparatus forfabricating a porous glass rod which can eliminate the abovementioned problems and can stabilize the fluidity in a reaction vessel to stabilize the outer diameter and the refractive index distribution of the glass rod in the longitudinal direction.
According to one aspect of this invention, there is provided a method offabricating a porous glass rod having a reaction vessel including an elevational passage from an exhaust port of the vessel side and the top ofthe vessel over the interior and a burner mounted atthe end in the vessel for forming glass fine particles, and a target elevationally movable and rotatably inserted from the passage into the vessel which comprises injecting to accumulate glass fine particles produced through the burner to form the porous glass rod at the lower end ofthe target rotated ata predetermined position in the reactor, and drawing the target in response to the growing velocity of the porous glass rod, wherein downward gas stream is produced along the outer periphery of the conduit in the vessel.
According to another aspect of this invention, there is also provided an apparatusforfabricating a porous glass rod having a reaction vessel including an elevational passage from an exhaust port ofthe vessel side and the top of the vessel over the interior and a burner mounted at the end in the vessel for forming glass fine particles, and atarget elevationally movable and rotatably inserted from the passage into the vessel which comprises a cylinder having hermetical sealability coupled with the top ofthe passage, a glass flow passage formed to flow a downward gas flow between the upper inner periphery ofthe vessel and the outer periphery ofthe passage, and a gas inlet formed atthetopof the passage.
In the invention, the glass fine particles injected from the end of the burner in the reaction vessel are accumulated on the lower end ofthetarget ofthe rotary state to form a porous glass rod, and the target is drawn in response to the growing velocity ofthe glass rod in the same manner as the conventional method, and, when the glass rod is thus formed, a downward gas stream is advantageously produced along the outer periphery ofthe passage in the vessel.
When the porous glass rod is fabricated as described above in the invention,the porous glass rod passes together with the target in the passage, and the downward gas stream is flowed to the exhaust port along the outer periphery of the passage.
Therefore, even if the clearance in the passage varies as the target first passes and the grown porous glass rod then passes through the passage, the gas stream moving downward along the outer peripheryofthe passage is not affected bythe influence of the variation in the clearance, but exhibits always stable fluidity.
As a result, the porous glass base material is substantially constantly finished by the downward gas stream of stable state, and the mutual effect of the directivity of the flame ofthe burner constant with respect to the accumulating surface and the prevention of random behavioroftheglassfine particles due to the downward gas stream allows the refractive index distribution over the longitudinal direction ofthe porous glass base material to become constant, thereby obtaining the porous glass base material having high quality and properties.
The above and other related objects and features of the invention will be apparent from a reading of the following description of the disclosure found in the accompanying drawings and the novelty thereof pointed out in the appended claims.
Figure 1 is is a n an explanatoryviewschematically showing an embodiment of a method of and apparatusforfabricating a porous glass rod according to the present invention;
Figure2 is an explanatoryviewschematically showing another embodiment of a method of and apparatusforfabricating a porous glass rod according to the invention; and Figures 3(a) and 3(b) are explanatory views showing the conventional example.
Embodiments of a method and apparatus for fabricating a porous glass rod of the invention will be described in detail with reference to the accompanying drawings.
In Figures 1 and 2, reference numeral 11 designates a reaction vessel having an exhaust port 12, numeral 13 designates a passage provided from the top over to the interior ofthe vessel 11, numeral 14 designates a burner mounted at the end from the bottom to the interior of the vessel 11 for producing glass fine particles, and numeral 15 designates a target known to rotatably and elevationally movable act.
In the construction described above, a cylinder 16 having hermetical sealability is coupled with the upper surface of the passage 13, a gas flow passage
17 is formed between the upper inner periphery of the vessel 11 and the outer periphery of the passage to generate a downward gas stream, and a gas inlet 18 is formed at the upper end of the gas flow passage 17.
In the case of the first embodiment in Figure 1, the gas inlet 18 is formed of a plurality of circular through holes perforated equidistantly on the upper surface of the vessel 11, and in the case of the second embodiment in Figure2,thegas inlet 18 isformed through a member having a gas guide inlet 19 and a ring-shaped gas outlet 20, and a piping system 22 having a flow rate regulator 21 is connected to the inlet 19.
In Figures 1 and 2, numeral 23 designates a porous glass rod.
When the porous glass rod 23 is fabricated by the apparatus exemplified as above, the target 15 is inserted atthe lower end to a predetermined position in the vessel 11, and rotated to inject and accumulate product, i.e., glass fine particles produced by flame hydrolysis reaction through the burner 1 4toward the lower end of the target 15.
The porous glass rod 23 is formed on the lower end of thetarget 15 by the accumulation of such glassfine particles, and thetarget 15 is drawn upwardly in the passage 13 and the cylinder 16 in response to the growing velocity of the glass rod 23.
In this case, the vessel 11 is evacuated from the exhaust port 12, and predetermined gas is introduced from the piping system 22 by means of natural introduction upon evacuating ofthevessel or the forcible introduction from the gas inlet 18 into the gas flow passage 17, thereby causing a downward gas flow to occur along the outer periphery ofthe passage 13.
As described above, the downward gas stream flowed to the exhaust port 12 along the outer periphery ofthe passage 13 exhibits stable fluidity not affected by the variation in the clearance in the passage 13, and causes the mutual effect of the directivity of the constant flame of the burnerwith respect to the accumulating area and the prevention of random behaviour of the glass fine particles, thereby maintaining the outer diameter and the refractive index distribution ofthe glass base material 23 constant over the longitudinal direction of the base material.
When the porous glass rod 23 is fabricated according to the method of the invention described above, it is preferable to control pressure or flow rate to maintain the exhaust gas pressure in the vessel 11 or the flow rate of the downward gas stream constant. These controls are regulated by an exhaust amount regulator (not shown) in the piping system connected to the exhaust port 12 and the flow rate regulator21 ofthe piping system 22 connected tothe gas inlet 19.
According to the invention as described above, when the porous glass rod is fabricated by means of the VAD method, the downward gas stream is generated along the outer periphery ofthe passage in the reaction vessel. Therefore, the porous glass base material having constant outer diameter and refractive index distribution over the longitudinal direction can be provided by the stable downward gas stream not affected by the variation in the clearance in the passage.
On the other hand, according to the apparatus of the invention as described above, the arrangement comprises not only the exhaust port and the passage ofthe vessel, the burner for generating glass fine particles, and the target, but the glass flow passage formed between the upper inner periphery of the vessel and the outer periphery of the passage, the gas inlet formed at the upper end of the gas flow passage, and the cylinder having hermetical sealability is coupled with the passage. Therefore, the predetermined downward gas stream can be facilitated, and the drawing operation of the glass rod can be performed without loss of the atmosphere in the reaction vessel by utilizing the cylinderofthe passage.
Claims (9)
1. A method offabricating a porous glass rod using a reaction vessel which includes an elevational passage between an exhaust port of the vessel side and the top of the vessel over its interior, a burner mounted in the vessel forforming glass fine particles, and a target which is elevationally movable and rotatable and is inserted from the passage into the vessel, said method comprising producing glass fine particles by means ofthe burner and accumulating these to form the porous glass rod at the lower end ofthetargetwhen rotated ata predetermined position in the reactor, and drawing the target in response to the growing porous glass rod, wherein a downward gas stream is produced along the outer periphery of the passage in the vessel.
2. A method according to Claim 1,further comprising regulating the gas stream so that a constant flow rate of the downward gas stream along the outer periphery of the passage is obtained.
3. Amethod according to Claim 1,further comprising regulating the flow rate of the downward gas stream along the outer periphery ofthe passage so that a constant exhaust gas pressure in the vessel is obtained.
4. An apparatusforfabricating a porous glass rod, said apparatus having a reaction vessel including an elevational passage between an exhaust port of the vessel side and the top ofthe vessel over its interior, a burner mounted in the vessel for forming glass fine particles, a target which is elevationally movable and rotatable and is inserted from the passage into the vessel, a cylinder having hermetical sealability coupled with the top of the passage, a gas flow passage for a downward gas flow between the upper inner periphery of the vessel and the outer periphery ofthe passage, and a gas inlet formed atthetop ofthe passage.
5. An apparatus according to Claim 4,wherein said gas inlet comprises a pluraiity ofthrough holes in the upper surface of the reaction vessel.
6. An apparatus according to Claim 4, wherein said gas inlet is formed through a member having a ,OS guide inlet and a ring-shaped gas outlet.
7. An apparatus according to Claim 4,5or6, wherein said gas inlet is connected with a piping system having a flow rate regulator.
8. A method of fabricating a porous glass rod, said method being as claimed in Claim 1 and substantially as herein described with reference to
Figure 1 or 2 ofthe accompanying drawings.
9. An apparatus forfabricating a porous glass
rod, substantially as herein described with reference to Figure 1 or 2 ofthe accompanying drawings.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP3809885A JPS61197439A (en) | 1985-02-27 | 1985-02-27 | Production of porous glass rod and devices therefor |
Publications (3)
Publication Number | Publication Date |
---|---|
GB8611440D0 GB8611440D0 (en) | 1986-06-18 |
GB2190078A true GB2190078A (en) | 1987-11-11 |
GB2190078B GB2190078B (en) | 1990-04-11 |
Family
ID=12515998
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB8611440A Expired - Fee Related GB2190078B (en) | 1985-02-27 | 1986-05-10 | Method of fabricating porous glass rod and apparatus for fabricating the same |
Country Status (2)
Country | Link |
---|---|
JP (1) | JPS61197439A (en) |
GB (1) | GB2190078B (en) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2603472B2 (en) * | 1987-05-12 | 1997-04-23 | 旭硝子株式会社 | Manufacturing method of porous quartz glass base material |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB2017077A (en) * | 1978-03-03 | 1979-10-03 | Hitachi Ltd | Producing optical fibre preform |
GB2092124A (en) * | 1980-12-12 | 1982-08-11 | Nippon Telegraph & Telephone | Process for producing an optical fiber preform and apparatus therefor |
GB2092125A (en) * | 1980-12-12 | 1982-08-11 | Nippon Telegraph & Telephone | Process for producing an optical fiber preform and apparatus therefor |
GB2119503A (en) * | 1982-04-26 | 1983-11-16 | Western Electric Co | An exhaust system for a vapor deposition chamber |
GB2128982A (en) * | 1979-10-09 | 1984-05-10 | Nippon Telegraph & Telephone | Fabrication method of optical fiber preforms |
-
1985
- 1985-02-27 JP JP3809885A patent/JPS61197439A/en active Granted
-
1986
- 1986-05-10 GB GB8611440A patent/GB2190078B/en not_active Expired - Fee Related
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB2017077A (en) * | 1978-03-03 | 1979-10-03 | Hitachi Ltd | Producing optical fibre preform |
GB2128982A (en) * | 1979-10-09 | 1984-05-10 | Nippon Telegraph & Telephone | Fabrication method of optical fiber preforms |
GB2092124A (en) * | 1980-12-12 | 1982-08-11 | Nippon Telegraph & Telephone | Process for producing an optical fiber preform and apparatus therefor |
GB2092125A (en) * | 1980-12-12 | 1982-08-11 | Nippon Telegraph & Telephone | Process for producing an optical fiber preform and apparatus therefor |
GB2119503A (en) * | 1982-04-26 | 1983-11-16 | Western Electric Co | An exhaust system for a vapor deposition chamber |
Also Published As
Publication number | Publication date |
---|---|
GB2190078B (en) | 1990-04-11 |
JPS61197439A (en) | 1986-09-01 |
GB8611440D0 (en) | 1986-06-18 |
JPH0526732B2 (en) | 1993-04-19 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PCNP | Patent ceased through non-payment of renewal fee |
Effective date: 20010510 |