GB1377486A - Polyether purification process - Google Patents
Polyether purification processInfo
- Publication number
- GB1377486A GB1377486A GB472271A GB472271A GB1377486A GB 1377486 A GB1377486 A GB 1377486A GB 472271 A GB472271 A GB 472271A GB 472271 A GB472271 A GB 472271A GB 1377486 A GB1377486 A GB 1377486A
- Authority
- GB
- United Kingdom
- Prior art keywords
- polyethers
- condensation product
- propylene oxide
- treatment
- feb
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/30—Post-polymerisation treatment, e.g. recovery, purification, drying
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Polyesters Or Polycarbonates (AREA)
Abstract
1377486 Polyethers IMPERIAL CHEMICAL INDUSTRIES Ltd 2 Feb 1972 [16 Feb 1971] 4722/71 Heading C2C [Also in Division C3] Polyethers contaminated with basic inorganic materials are purified by treatment in the presence of water with a compound containing at least one carboxylic acid group and at least two hydroxyl groups, suitably tartaric acid. Treatment temperatures preferably range from 25‹ to 150‹ C. Volatile material including water may be removed by subsequent heating under reduced pressure, and a further filtration step removes insoluble material. The acid-treated material may be optionally treated with an insoluble basic material and also with an adsorbent material to remove coloured impurities. Polyethers suitable for treatment include those having a hydroxyl equivalent weight of from 60 to 3000 obtained by the polymerization of one or more alkylene oxides in the presence of an alkaline catalyst and optional amounts of compounds containing one or more active hydrogen atoms. Examples describe the preparation and purification of ethylene oxide endcapped glycerol-propylene oxide condensation products (M.W. 3500), of a tolylene diaminepropylene oxide condensation product (M.W. 470), of a low molecular weight condensation product of propylene oxide and a mixture of triethanolamine and tolylene diamine, and of a glycerol-propylene oxide condensation product (M.W. 310).
Priority Applications (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB472271A GB1377486A (en) | 1971-02-16 | 1971-02-16 | Polyether purification process |
AU38877/72A AU3887772A (en) | 1971-02-16 | 1972-02-10 | Purification process |
NL7201819A NL7201819A (en) | 1971-02-16 | 1972-02-11 | |
IT2054672A IT961142B (en) | 1971-02-16 | 1972-02-14 | PROCESS FOR REMOVING IMPURITIES OF INORGANIC BASES FROM POLYETER MATERIALS |
ES399844A ES399844A1 (en) | 1971-02-16 | 1972-02-16 | Polyether purification process |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB472271A GB1377486A (en) | 1971-02-16 | 1971-02-16 | Polyether purification process |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1377486A true GB1377486A (en) | 1974-12-18 |
Family
ID=9782557
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB472271A Expired GB1377486A (en) | 1971-02-16 | 1971-02-16 | Polyether purification process |
Country Status (5)
Country | Link |
---|---|
AU (1) | AU3887772A (en) |
ES (1) | ES399844A1 (en) |
GB (1) | GB1377486A (en) |
IT (1) | IT961142B (en) |
NL (1) | NL7201819A (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2365596A1 (en) * | 1976-09-27 | 1978-04-21 | Witco Chemical Corp | COMPOSITIONS BASED ON POLYETHER-POLYOLS AND THEIR APPLICATION TO THE PREPARATION OF POLYURETHANE FOAMS |
EP0107080A1 (en) * | 1982-09-29 | 1984-05-02 | The B.F. GOODRICH Company | Decolorizing polymers of epihalohydrin |
GB2135322A (en) * | 1983-01-21 | 1984-08-30 | Vyzk Ustav Petrochem | A process for purifying at least partially water-soluble polyethers and/or copolymers |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5248833A (en) * | 1992-09-22 | 1993-09-28 | Arco Chemical Technology, L.P. | Process for purifying polyols made with double metal cyanide catalysts |
-
1971
- 1971-02-16 GB GB472271A patent/GB1377486A/en not_active Expired
-
1972
- 1972-02-10 AU AU38877/72A patent/AU3887772A/en not_active Expired
- 1972-02-11 NL NL7201819A patent/NL7201819A/xx unknown
- 1972-02-14 IT IT2054672A patent/IT961142B/en active
- 1972-02-16 ES ES399844A patent/ES399844A1/en not_active Expired
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2365596A1 (en) * | 1976-09-27 | 1978-04-21 | Witco Chemical Corp | COMPOSITIONS BASED ON POLYETHER-POLYOLS AND THEIR APPLICATION TO THE PREPARATION OF POLYURETHANE FOAMS |
EP0107080A1 (en) * | 1982-09-29 | 1984-05-02 | The B.F. GOODRICH Company | Decolorizing polymers of epihalohydrin |
GB2135322A (en) * | 1983-01-21 | 1984-08-30 | Vyzk Ustav Petrochem | A process for purifying at least partially water-soluble polyethers and/or copolymers |
Also Published As
Publication number | Publication date |
---|---|
AU3887772A (en) | 1973-08-16 |
NL7201819A (en) | 1972-08-18 |
ES399844A1 (en) | 1975-04-01 |
IT961142B (en) | 1973-12-10 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PS | Patent sealed | ||
PLNP | Patent lapsed through nonpayment of renewal fees |