GB1350923A - Method for preparing oxides of fissile materials - Google Patents
Method for preparing oxides of fissile materialsInfo
- Publication number
- GB1350923A GB1350923A GB1694571A GB1694571A GB1350923A GB 1350923 A GB1350923 A GB 1350923A GB 1694571 A GB1694571 A GB 1694571A GB 1694571 A GB1694571 A GB 1694571A GB 1350923 A GB1350923 A GB 1350923A
- Authority
- GB
- United Kingdom
- Prior art keywords
- zone
- apparent density
- product
- nitrate
- uranium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
- B01J2/02—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops
- B01J2/04—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops in a gaseous medium
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G43/00—Compounds of uranium
- C01G43/01—Oxides; Hydroxides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G43/00—Compounds of uranium
- C01G43/01—Oxides; Hydroxides
- C01G43/025—Uranium dioxide
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/11—Powder tap density
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/12—Surface area
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Abstract
1350923 Uranium oxides COMMISSARIAT A L'ENERGIE ATOMIQUE 25 May 1971 [25 May 1970] 16945/71 Heading ClA Uranium oxides are prepared by spraying a mixture of a uranium nitrate solution and formic acid, into a first zone in a vessel maintained at 150-300‹ C., and calcining the product from the first zone in a second zone in the same vessel. The nitrate may be aqueous uranyl nitrate and may be mixed with 0À4 ml. formic acid/gm.U. The solution may be sprayed in with air or H 2 / N 2 mixture as an atomizing gas the gas being first brought to the temperature of the first zone. The calcining may be carried out at 800‹ C. in air to yield U 3 O 8 , or in hydrogen to yield UO 2 . The intermediate product has a specific area of 2À5-7 m.<SP>2</SP>/gm. and an apparent density of 0À9-1À8 g./cm.<SP>3</SP>. A U 3 O 8 product has a specific area of 2À7 m.<SP>2</SP>/gm., an average grain diameter of 1À2 Á and an apparent density of 1À5 g./cm.<SP>3</SP>. The UO 2 products have specific areas of 1À4- 4-5 m.<SP>2</SP>/g., average grain diameter of 0À5-1À6 Á and apparent density of 1À2-2À6 g./cm.<SP>3</SP>.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR7018979A FR2088170B1 (en) | 1970-05-25 | 1970-05-25 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1350923A true GB1350923A (en) | 1974-04-24 |
Family
ID=9056053
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB1694571A Expired GB1350923A (en) | 1970-05-25 | 1971-05-25 | Method for preparing oxides of fissile materials |
Country Status (3)
Country | Link |
---|---|
BE (1) | BE767322A (en) |
FR (1) | FR2088170B1 (en) |
GB (1) | GB1350923A (en) |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6656391B1 (en) | 1998-11-26 | 2003-12-02 | Commissariat A L'energie Atomique | Preparation by spray-drying of a flowable uranium dioxide powder obtained by dry process conversion of UF6 |
RU2494479C1 (en) * | 2012-04-09 | 2013-09-27 | Российская Федерация, от имени которой выступает Федеральное государственное унитарное предприятие "Федеральный центр ядерной и радиационной безопасности" | Method for obtaining solid solutions of oxides of actinides |
RU2543086C1 (en) * | 2013-08-26 | 2015-02-27 | Федеральное государственное унитарное предприятие "Научно-производственное объединение "Радиевый институт имени В.Г. Хлопина" | Method of obtaining individual and mixed metal oxides |
RU2570510C2 (en) * | 2014-04-30 | 2015-12-10 | Федеральное государственное бюджетное учреждение науки Институт катализа им. Г.К. Борескова Сибирского отделения Российской академии наук | Catalyst (versions), method of thereof preparation (versions) and method of purification of liquid radioactive wastes |
RU2662526C2 (en) * | 2013-10-22 | 2018-07-26 | Коммиссариат А Л' Энержи Атомик Э Оз Энержи Альтернатив | Process for preparing a powder comprising a solid solution of uranium dioxide and of a dioxide of at least one other actinide and/or lanthanide element |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
AT366845B (en) * | 1977-05-24 | 1982-05-10 | Oesterr Forsch Seibersdorf | METHOD FOR PRODUCING SPHERICAL FUEL PARTICLES |
FR2526006A1 (en) * | 1982-04-30 | 1983-11-04 | Comurhex | PROCESS FOR OBTAINING UO3 OF HIGH SPECIFIC SURFACE FROM URANYLE HYDRATE NITRATE |
FR2555566B1 (en) * | 1983-11-25 | 1989-02-17 | Comurhex | PROCESS FOR THE PREPARATION OF POWDER METAL OXIDES FROM AQUEOUS SOLUTIONS OR SOLID MIXTURES OF METAL NITRATES |
GB2210605B (en) * | 1987-10-05 | 1991-06-26 | Merck Patent Gmbh | Process for the preparation of metal oxide powders |
DE3805063A1 (en) * | 1988-02-18 | 1989-08-31 | Kernforschungsz Karlsruhe | METHOD FOR PRODUCING NUCLEAR FUEL MIXED OXIDS FROM A NITRATE SOLUTION |
FR2998484B1 (en) * | 2012-11-28 | 2014-12-05 | Commissariat Energie Atomique | PROCESS FOR PRODUCING SOLID MICROSPHERLES OF ACTINIDE COMPOUNDS FROM AN ACTINIDE SALT SOLUTION AND THE ASSOCIATED DEVICE |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR1308621A (en) * | 1961-09-13 | 1962-11-09 | Commissariat Energie Atomique | Improvements in uranium dioxide manufacturing processes |
FR1588805A (en) * | 1968-05-10 | 1970-03-16 |
-
1970
- 1970-05-25 FR FR7018979A patent/FR2088170B1/fr not_active Expired
-
1971
- 1971-05-18 BE BE767322A patent/BE767322A/en unknown
- 1971-05-25 GB GB1694571A patent/GB1350923A/en not_active Expired
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6656391B1 (en) | 1998-11-26 | 2003-12-02 | Commissariat A L'energie Atomique | Preparation by spray-drying of a flowable uranium dioxide powder obtained by dry process conversion of UF6 |
RU2494479C1 (en) * | 2012-04-09 | 2013-09-27 | Российская Федерация, от имени которой выступает Федеральное государственное унитарное предприятие "Федеральный центр ядерной и радиационной безопасности" | Method for obtaining solid solutions of oxides of actinides |
RU2543086C1 (en) * | 2013-08-26 | 2015-02-27 | Федеральное государственное унитарное предприятие "Научно-производственное объединение "Радиевый институт имени В.Г. Хлопина" | Method of obtaining individual and mixed metal oxides |
RU2662526C2 (en) * | 2013-10-22 | 2018-07-26 | Коммиссариат А Л' Энержи Атомик Э Оз Энержи Альтернатив | Process for preparing a powder comprising a solid solution of uranium dioxide and of a dioxide of at least one other actinide and/or lanthanide element |
RU2570510C2 (en) * | 2014-04-30 | 2015-12-10 | Федеральное государственное бюджетное учреждение науки Институт катализа им. Г.К. Борескова Сибирского отделения Российской академии наук | Catalyst (versions), method of thereof preparation (versions) and method of purification of liquid radioactive wastes |
Also Published As
Publication number | Publication date |
---|---|
FR2088170A1 (en) | 1972-01-07 |
FR2088170B1 (en) | 1975-01-10 |
BE767322A (en) | 1971-10-18 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PS | Patent sealed | ||
PLE | Entries relating assignments, transmissions, licences in the register of patents | ||
PCNP | Patent ceased through non-payment of renewal fee |