GB1349528A - Method for thy hydrogenation of unsaturated oils - Google Patents
Method for thy hydrogenation of unsaturated oilsInfo
- Publication number
- GB1349528A GB1349528A GB2624571*A GB2624571A GB1349528A GB 1349528 A GB1349528 A GB 1349528A GB 2624571 A GB2624571 A GB 2624571A GB 1349528 A GB1349528 A GB 1349528A
- Authority
- GB
- United Kingdom
- Prior art keywords
- oil
- hydrogenation
- heat exchange
- coil
- coolant
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
- C11C3/12—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by hydrogenation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
- B01J2219/00083—Coils
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Fats And Perfumes (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
Abstract
1349528 Temperature control of oil hydrogenation, evaporating and condensing CHEMETRON CORP 19 April 1971 [8 April 1970] 26245/71 Headings B1B B1F and B1X [Also in Division C5] A method for the batch hydrogenation of unsaturated oil comprises heating the oil by heat exchange with a condensable heat exchange medium, e.g. steam, and condensing at least some of the heat exchange medium under a first pressure with heat exchange with the oil to provide a body of liquid medium in thermal communication with the heated oil, introducing hydrogen into the heated oil to establish an exothermic hydrogenation reaction, removing heat from the reacting oil to control hydrogenation temperature by allowing heat exchange medium to vaporize from the body of liquid medium under a second pressure lower than the said first pressure, and subsequently further reducing the pressure over the body of liquid medium to cool the hydrogenated oil to filtering temperature. In the figure, a batch of soybean oil with catalyst is introduced into the vessel 10 through 14. Valves 56 and 67 are closed and valve 52 is opened to admit steam at 150 p.s.i.g. into the upper end of coil 48. Condensate valve 62 is opened and the steam heats the oil to 300F. Condensate valve 62 is closed and steam condenses in the coil until the coil is 50-75% full. Valve 52 is closed, and valves 56 and 67 are opened. Hydrogen is introduced at 5 p.s.i.g. through sparger 32. As the oil temperature rises, control regulator valve 90 begins to open and drains condensate from condenser 76 into the lower end of the heat exchange coil 48. As heat is generated by the hydrogenation it is absorbed by vaporization of the coolant in coil 48. As coolant vaporises more liquid coolant is introduced into the lower end of the coil until a state of equilibrium exists, the vapour from the coolant passing through vapour 54 to separator 58, and dry vapour is condensed in condenser 76 by water coolant. When hydrogenation is complete, all the condensate is drained from condenser 76 and causes reduction in pressure in the condensing system.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US2650970A | 1970-04-08 | 1970-04-08 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1349528A true GB1349528A (en) | 1974-04-03 |
Family
ID=21832244
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB2624571*A Expired GB1349528A (en) | 1970-04-08 | 1971-04-19 | Method for thy hydrogenation of unsaturated oils |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US3732266A (en) |
| JP (1) | JPS524561B1 (en) |
| BR (1) | BR7102052D0 (en) |
| CA (1) | CA1008463A (en) |
| DE (1) | DE2116894C3 (en) |
| ES (1) | ES389980A1 (en) |
| FR (1) | FR2089414A5 (en) |
| GB (1) | GB1349528A (en) |
| NL (1) | NL171173B (en) |
| SE (1) | SE369528B (en) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS539707A (en) * | 1976-07-15 | 1978-01-28 | Nippon Shokubai Kagaku Kogyo Co Ltd | Method and reactor for preparation of ethanolamines |
| US5360920A (en) * | 1992-08-07 | 1994-11-01 | The Procter & Gamble Company | Hydrogenation in a plate heat exchanger |
| US6955793B1 (en) | 1997-06-18 | 2005-10-18 | Arencibia Jr Jose P | Temperature controlled reaction vessel |
| AU2001255341A1 (en) * | 2000-04-13 | 2001-10-30 | Jose P. Arencibia Jr. | Temperature controlled reaction vessel |
| EP1508367B1 (en) * | 2003-08-22 | 2005-11-02 | Maschinenbau Scholz GmbH & Co. KG | Device for the temperature regulation of the inner space of pressure vessels |
| IN2012DN06560A (en) | 2009-12-30 | 2015-10-23 | Vitag Holdings Llc | |
| CN104826565A (en) * | 2015-03-31 | 2015-08-12 | 山东胜星化工有限公司 | Hydrogenation reaction ammonium salt crystallization prevention device |
| CN104826567B (en) * | 2015-05-07 | 2016-06-15 | 中石化南京工程有限公司 | A kind of Cyclohexanone Production platinum catalysis hydrogenation heat energy is for the device of dehydrogenating technology |
| CN107937129B (en) * | 2017-11-15 | 2021-03-23 | 四川航佳生物科技有限公司 | Temperature control system and process in edible animal oil and fat refining process |
-
1970
- 1970-04-08 US US00026509A patent/US3732266A/en not_active Expired - Lifetime
-
1971
- 1971-03-25 CA CA108,737A patent/CA1008463A/en not_active Expired
- 1971-04-06 BR BR2052/71A patent/BR7102052D0/en unknown
- 1971-04-06 DE DE2116894A patent/DE2116894C3/en not_active Expired
- 1971-04-06 ES ES389980A patent/ES389980A1/en not_active Expired
- 1971-04-06 JP JP46020800A patent/JPS524561B1/ja active Pending
- 1971-04-07 SE SE04526/71A patent/SE369528B/xx unknown
- 1971-04-07 NL NLAANVRAGE7104653,A patent/NL171173B/en not_active Application Discontinuation
- 1971-04-08 FR FR7112528A patent/FR2089414A5/fr not_active Expired
- 1971-04-19 GB GB2624571*A patent/GB1349528A/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| DE2116894A1 (en) | 1971-10-21 |
| FR2089414A5 (en) | 1972-01-07 |
| NL171173B (en) | 1982-09-16 |
| DE2116894B2 (en) | 1979-09-06 |
| CA1008463A (en) | 1977-04-12 |
| JPS524561B1 (en) | 1977-02-04 |
| SE369528B (en) | 1974-09-02 |
| ES389980A1 (en) | 1973-06-16 |
| BR7102052D0 (en) | 1973-04-10 |
| NL7104653A (en) | 1971-10-12 |
| US3732266A (en) | 1973-05-08 |
| DE2116894C3 (en) | 1980-05-22 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| PCNP | Patent ceased through non-payment of renewal fee |