GB1153107A - Process for the production of Urea - Google Patents

Process for the production of Urea

Info

Publication number
GB1153107A
GB1153107A GB42015/67A GB4201567A GB1153107A GB 1153107 A GB1153107 A GB 1153107A GB 42015/67 A GB42015/67 A GB 42015/67A GB 4201567 A GB4201567 A GB 4201567A GB 1153107 A GB1153107 A GB 1153107A
Authority
GB
United Kingdom
Prior art keywords
urea
carbon dioxide
weight
synthesis step
ammonium carbamate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB42015/67A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Toyo Koatsu Industries Inc
Original Assignee
Toyo Koatsu Industries Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Toyo Koatsu Industries Inc filed Critical Toyo Koatsu Industries Inc
Publication of GB1153107A publication Critical patent/GB1153107A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C273/02—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
    • C07C273/04—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds from carbon dioxide and ammonia
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/02—Apparatus characterised by being constructed of material selected for its chemically-resistant properties
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/02—Apparatus characterised by their chemically-resistant properties
    • B01J2219/0204—Apparatus characterised by their chemically-resistant properties comprising coatings on the surfaces in direct contact with the reactive components
    • B01J2219/0236—Metal based
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/02—Apparatus characterised by their chemically-resistant properties
    • B01J2219/025—Apparatus characterised by their chemically-resistant properties characterised by the construction materials of the reactor vessel proper
    • B01J2219/0277—Metal based
    • B01J2219/0281—Metal oxides
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/141—Feedstock

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Preventing Corrosion Or Incrustation Of Metals (AREA)

Abstract

1,153,107. Urea. TOYO KOATSU INDUSTRIES Inc. 14 Sept., 1967 [16 Sept., 1966], No. 42015/67. Heading C2C. [Also in Division C7] A process for the production of urea comprises a urea-synthesis step of reacting ammonia and carbon dioxide at urea-forming temperatures and pressures, treating the resulting ureasynthesis effluent in such a manner that the unreacted ammonium carbamate contained in said effluent is distilled off as a gaseous mixture of ammonia and carbon dioxide to obtain urea, wherein there is used for performing the process an apparatus which is so constructed that one or more surfaces thereof coming into contact with ammonium carbamate is or are of an alloy steel resistant to corrosion by ammonium carbamate, the said alloy steel containing at least 20% by weight of chromium, 1 to 7% by weight of nickel and 1 to 4% by weight of molybdenum, the balance being iron and unavoidable impurity. The said alloy may also contain manganese, silicon, tungsten, phosphorus, sulphur or nitrogen, and the urea-synthesis step is preferably conducted in the presence of less than 0À2% by volume of oxygen based on the amount of carbon dioxide used for the synthesis. At least a part of the said gaseous mixture is preferably absorbed in an absorbent and recirculated as an aqueous carbamate solution to the urea-synthesis step.
GB42015/67A 1966-09-16 1967-09-14 Process for the production of Urea Expired GB1153107A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP6084466 1966-09-16

Publications (1)

Publication Number Publication Date
GB1153107A true GB1153107A (en) 1969-05-21

Family

ID=13154065

Family Applications (1)

Application Number Title Priority Date Filing Date
GB42015/67A Expired GB1153107A (en) 1966-09-16 1967-09-14 Process for the production of Urea

Country Status (4)

Country Link
DE (1) DE1668724C3 (en)
ES (1) ES344834A1 (en)
GB (1) GB1153107A (en)
NL (1) NL141178B (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2138024A (en) * 1983-02-15 1984-10-17 Jgc Corp Corrosion resistant castable stainless steel alloy composition for use at low temperatures
US4591644A (en) * 1983-12-21 1986-05-27 Stamicarbon B.V. Method and installation for the preparation of melamine
WO1995025098A1 (en) * 1994-03-15 1995-09-21 Dsm N.V. Method for the separation of impurities from a hot synthesis gas mixture in the preparation of melamine
EP1921043A1 (en) * 2006-11-01 2008-05-14 Mitsubishi Gas Chemical Company, Inc. Method of recovering ammonia
US9890114B2 (en) 2013-05-28 2018-02-13 Toyo Engineering Corporation Urea synthesis method

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2138024A (en) * 1983-02-15 1984-10-17 Jgc Corp Corrosion resistant castable stainless steel alloy composition for use at low temperatures
US4591644A (en) * 1983-12-21 1986-05-27 Stamicarbon B.V. Method and installation for the preparation of melamine
WO1995025098A1 (en) * 1994-03-15 1995-09-21 Dsm N.V. Method for the separation of impurities from a hot synthesis gas mixture in the preparation of melamine
US5716429A (en) * 1994-03-15 1998-02-10 Dsm N.V. Method for the separation of impurities from a hot synthesis gas mixture in the preparation of melamine
CN1061979C (en) * 1994-03-15 2001-02-14 Dsm有限公司 Method for separation of impurities from hot synthesis gas mixture in preparation of melamine
EP1921043A1 (en) * 2006-11-01 2008-05-14 Mitsubishi Gas Chemical Company, Inc. Method of recovering ammonia
US7785556B2 (en) 2006-11-01 2010-08-31 Mitsubishi Gas Chemical Company, Inc. Method of recovering ammonia
US9890114B2 (en) 2013-05-28 2018-02-13 Toyo Engineering Corporation Urea synthesis method

Also Published As

Publication number Publication date
ES344834A1 (en) 1968-11-01
NL141178B (en) 1974-02-15
DE1668724C3 (en) 1973-07-19
DE1668724A1 (en) 1972-01-05
NL6712586A (en) 1968-03-18
DE1668724B2 (en) 1973-01-04

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Legal Events

Date Code Title Description
429A Application made for amendment of specification (sect. 29/1949)
429H Application (made) for amendment of specification now open to opposition (sect. 29/1949)
414F Notice of opposition given (sect. 14/1949)
429D Case decided by the comptroller ** specification amended (sect. 29/1949)
414E Application relinquished (sect. 14/1949)
CSNS Application of which complete specification have been accepted and published, but patent is not sealed