GB1137582A - A method for producing and/or refining of alkali metal halides - Google Patents

A method for producing and/or refining of alkali metal halides

Info

Publication number
GB1137582A
GB1137582A GB10553/66A GB1055366A GB1137582A GB 1137582 A GB1137582 A GB 1137582A GB 10553/66 A GB10553/66 A GB 10553/66A GB 1055366 A GB1055366 A GB 1055366A GB 1137582 A GB1137582 A GB 1137582A
Authority
GB
United Kingdom
Prior art keywords
alkali metal
halide
gaseous
compound
metal halides
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB10553/66A
Inventor
Miroslav Lebl
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Czech Academy of Sciences CAS
Original Assignee
Czech Academy of Sciences CAS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Czech Academy of Sciences CAS filed Critical Czech Academy of Sciences CAS
Publication of GB1137582A publication Critical patent/GB1137582A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D17/00—Rubidium, caesium or francium compounds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00—Lithium compounds
    • C01D15/04—Halides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D3/00—Halides of sodium, potassium or alkali metals in general
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D3/00—Halides of sodium, potassium or alkali metals in general
    • C01D3/14—Purification
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B11/00—Single-crystal growth by normal freezing or freezing under temperature gradient, e.g. Bridgman-Stockbarger method
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/10—Inorganic compounds or compositions
    • C30B29/12—Halides

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Metallurgy (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Abstract

1,137,582. Alkali metal halides. CESKOSLOVENSKA AKADEMIE VED. 10 March, 1966 [23 March, 1965], No. 10553/66. Heading C1A. Alkali metal halides are produced by replacing the anion of a starting alkali metal compound other than a halide by a halogen, or alkali metal halides are refined, in a process wherein into the melted starting material consisting of said compound or halide is fed a gaseous halide of carbon or sulphur, or a thionyl or carbonyl gaseous halide or a gaseous halide consisting of a compound of a halogen, carbon and hydrogen, at a temperature not exceeding 1250‹ C., and wherein the melt of the alkali metal halide is cooled in an atmosphere of the gaseous halide. The gaseous halide may be entrained in a stream of inert gas, e.g. argon. The alkali metal compound may be chosen from the oxides, hydroxide, salts of oxygenic acids (e.g. carbonates, sulphites, sulphates, perchlorates, nitrites) and alkali metal salts of non-oxygenic acids (e.g. sulphides). The gaseous halides exemplified are CCl 4 , SOCl 2 , C 2 Cl 6 , CHCl 3 , COBr2, COCl 2 . Examples of the preparation or purification of KCl, NaCl, LiCl. RbCl and CoCl are given.
GB10553/66A 1965-03-23 1966-03-10 A method for producing and/or refining of alkali metal halides Expired GB1137582A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CS191265 1965-03-23

Publications (1)

Publication Number Publication Date
GB1137582A true GB1137582A (en) 1968-12-27

Family

ID=5354664

Family Applications (1)

Application Number Title Priority Date Filing Date
GB10553/66A Expired GB1137582A (en) 1965-03-23 1966-03-10 A method for producing and/or refining of alkali metal halides

Country Status (2)

Country Link
DE (1) DE1567913A1 (en)
GB (1) GB1137582A (en)

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3932597A (en) * 1973-11-19 1976-01-13 Hughes Aircraft Company Purification of alkali metal halides
US3969491A (en) * 1973-04-16 1976-07-13 Hughes Aircraft Company Purification of alkali metal chlorides and bromides
US4030965A (en) * 1976-06-09 1977-06-21 The Harshaw Chemical Company Crystal growth procedure
FR2336971A1 (en) * 1975-12-29 1977-07-29 Hughes Aircraft Co PROCESS FOR FORMING ALKALINE HALOGENIDE SINGLE CRYSTALS
US4055457A (en) * 1974-01-17 1977-10-25 The Harshaw Chemical Company Method for growing absorption-free alkali metal halide single crystals
US4190487A (en) * 1975-12-30 1980-02-26 Hughes Aircraft Company Reactive atmosphere processing method of crystal growth of alkaline earth chlorides
EP1088911A1 (en) * 1999-09-29 2001-04-04 Optoscint Inc. Continuous crystal plate growth process and apparatus
EP1249520A1 (en) * 2001-04-09 2002-10-16 Optoscint Inc. Apparatus and method for the purification of a material

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3969491A (en) * 1973-04-16 1976-07-13 Hughes Aircraft Company Purification of alkali metal chlorides and bromides
US3932597A (en) * 1973-11-19 1976-01-13 Hughes Aircraft Company Purification of alkali metal halides
US4055457A (en) * 1974-01-17 1977-10-25 The Harshaw Chemical Company Method for growing absorption-free alkali metal halide single crystals
FR2336971A1 (en) * 1975-12-29 1977-07-29 Hughes Aircraft Co PROCESS FOR FORMING ALKALINE HALOGENIDE SINGLE CRYSTALS
US4076574A (en) * 1975-12-29 1978-02-28 Hughes Aircraft Company Reactive atmosphere crystal growth method
US4190487A (en) * 1975-12-30 1980-02-26 Hughes Aircraft Company Reactive atmosphere processing method of crystal growth of alkaline earth chlorides
US4030965A (en) * 1976-06-09 1977-06-21 The Harshaw Chemical Company Crystal growth procedure
EP1088911A1 (en) * 1999-09-29 2001-04-04 Optoscint Inc. Continuous crystal plate growth process and apparatus
EP1249520A1 (en) * 2001-04-09 2002-10-16 Optoscint Inc. Apparatus and method for the purification of a material

Also Published As

Publication number Publication date
DE1567913A1 (en) 1970-09-24

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