GB1100407A - Silicon carbon dies - Google Patents

Silicon carbon dies

Info

Publication number
GB1100407A
GB1100407A GB49702/65A GB4970265A GB1100407A GB 1100407 A GB1100407 A GB 1100407A GB 49702/65 A GB49702/65 A GB 49702/65A GB 4970265 A GB4970265 A GB 4970265A GB 1100407 A GB1100407 A GB 1100407A
Authority
GB
United Kingdom
Prior art keywords
sic
substrate
die
me2cl2si
ratio
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB49702/65A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dow Silicones Corp
Original Assignee
Dow Corning Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Corning Corp filed Critical Dow Corning Corp
Publication of GB1100407A publication Critical patent/GB1100407A/en
Expired legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21CMANUFACTURE OF METAL SHEETS, WIRE, RODS, TUBES OR PROFILES, OTHERWISE THAN BY ROLLING; AUXILIARY OPERATIONS USED IN CONNECTION WITH METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL
    • B21C3/00Profiling tools for metal drawing; Combinations of dies and mandrels
    • B21C3/18Making tools by operations not covered by a single other subclass; Repairing
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B23MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23PMETAL-WORKING NOT OTHERWISE PROVIDED FOR; COMBINED OPERATIONS; UNIVERSAL MACHINE TOOLS
    • B23P15/00Making specific metal objects by operations not covered by a single other subclass or a group in this subclass
    • B23P15/24Making specific metal objects by operations not covered by a single other subclass or a group in this subclass dies
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/01Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes on temporary substrates, e.g. substrates subsequently removed by etching

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Chemical Vapour Deposition (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Metal Extraction Processes (AREA)

Abstract

A SiC die is produced by depositing a layer of SiC from the vapour phase on to a substrate, removing the substrate, and finishing the SiC to the final die configuration. The SiC may be formed by reducing an alkylsilane having a C:Si ratio of at least 1.75:1 (e.g. Me2Cl2Si, Me3ClSi, PrCl3Si, or a mixture of MeCl3Si and Me2Cl2Si) with H2 at 1150-1250 DEG C., e.g. using a H2:silane ratio of 1:1 to 20:1. The substrate may be tubular or rod shaped, and may be of Si, Ta, C, W, or alloys. It is removed by sand blasting or etching, e.g. with HF-HNO3. The substrate may be preformed to the internal configuration of the die and finished by polishing. Alternatively, the SiC coated rod may be cut longitudinally into sections, the substrate removed, and 3 of the sectors rounded and formed into the 2 legs and cross-bar in a reactor for further deposition of SiC. These rods are then machined using diamond tools or electron discharge, and cut to length. The SiC may be doped by incorporating N2, PCl3 or BCl3 in the gas.
GB49702/65A 1965-01-15 1965-11-23 Silicon carbon dies Expired GB1100407A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US425875A US3293950A (en) 1965-01-15 1965-01-15 Wire drawing die

Publications (1)

Publication Number Publication Date
GB1100407A true GB1100407A (en) 1968-01-24

Family

ID=23688401

Family Applications (1)

Application Number Title Priority Date Filing Date
GB49702/65A Expired GB1100407A (en) 1965-01-15 1965-11-23 Silicon carbon dies

Country Status (5)

Country Link
US (1) US3293950A (en)
FR (1) FR1464359A (en)
GB (1) GB1100407A (en)
NL (1) NL6600426A (en)
SE (1) SE305172B (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5698261A (en) * 1993-08-17 1997-12-16 Aktsionernoe Obschestvo Russkoe Obschestvo Prikladnoi Elektroniki Process for producing silicon carbide layers and an article

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3828628A (en) * 1970-11-24 1974-08-13 Peugeot & Renault Methods of extruding helical gear blanks
IE48798B1 (en) * 1978-08-18 1985-05-15 De Beers Ind Diamond Method of making tool inserts,wire-drawing die blank and drill bit comprising such inserts
JPS5658817A (en) * 1979-10-18 1981-05-22 Bridgestone Corp Dividing method of ring shaped metal mold and cutting apparatus therefor
US9683286B2 (en) 2006-04-28 2017-06-20 Gtat Corporation Increased polysilicon deposition in a CVD reactor
CN102027156A (en) * 2008-03-26 2011-04-20 Gt太阳能公司 Systems and methods for distributing gas in a chemical vapor deposition reactor

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5698261A (en) * 1993-08-17 1997-12-16 Aktsionernoe Obschestvo Russkoe Obschestvo Prikladnoi Elektroniki Process for producing silicon carbide layers and an article

Also Published As

Publication number Publication date
NL6600426A (en) 1966-07-18
FR1464359A (en) 1966-12-30
US3293950A (en) 1966-12-27
SE305172B (en) 1968-10-14

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