GB1096033A - Method of preparing alkenynoxysilanes - Google Patents
Method of preparing alkenynoxysilanesInfo
- Publication number
- GB1096033A GB1096033A GB2942365A GB2942365A GB1096033A GB 1096033 A GB1096033 A GB 1096033A GB 2942365 A GB2942365 A GB 2942365A GB 2942365 A GB2942365 A GB 2942365A GB 1096033 A GB1096033 A GB 1096033A
- Authority
- GB
- United Kingdom
- Prior art keywords
- organic base
- enyn
- alkenynoxysilanes
- preparing
- alcohol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 2
- 150000007530 organic bases Chemical class 0.000 abstract 2
- 239000000376 reactant Substances 0.000 abstract 2
- 239000000463 material Substances 0.000 abstract 1
- -1 nitrogen-containing organic base Chemical class 0.000 abstract 1
- 125000000962 organic group Chemical group 0.000 abstract 1
- 150000001367 organochlorosilanes Chemical class 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
- 150000004756 silanes Chemical class 0.000 abstract 1
- 238000005292 vacuum distillation Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/18—Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
- C07F7/1804—Compounds having Si-O-C linkages
- C07F7/1872—Preparation; Treatments not provided for in C07F7/20
- C07F7/188—Preparation; Treatments not provided for in C07F7/20 by reactions involving the formation of Si-O linkages
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
Abstract
Alkenynoxy silanes are prepared by reacting an organochlorosilane with an enyn alcohol, preferably in the presence of a nitrogen-containing organic base, between 60-70 DEG C. for 5-10 hours, using a molar ratio of reactants between 9:10 and 10:9, and a like molar ratio of organic base with respect to either reactant. The enyn alcohol is suitably tertiary and of formula <FORM:1096033/C3/1> where R1 is H or an organic group. The product may be obtained by separation and vacuum distillation. The organic base may be liberated for re-use by addition of an alkaline reacting material.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB2942365A GB1096033A (en) | 1965-07-12 | 1965-07-12 | Method of preparing alkenynoxysilanes |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB2942365A GB1096033A (en) | 1965-07-12 | 1965-07-12 | Method of preparing alkenynoxysilanes |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1096033A true GB1096033A (en) | 1967-12-20 |
Family
ID=10291341
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB2942365A Expired GB1096033A (en) | 1965-07-12 | 1965-07-12 | Method of preparing alkenynoxysilanes |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB1096033A (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4294975A (en) * | 1979-05-31 | 1981-10-13 | Shin-Etsu Chemical Co. Ltd. | Hydroalkenyloxysilanes |
US5089649A (en) * | 1989-04-28 | 1992-02-18 | Shin-Etsu Chemical Co., Ltd. | Organosilicon compound |
-
1965
- 1965-07-12 GB GB2942365A patent/GB1096033A/en not_active Expired
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4294975A (en) * | 1979-05-31 | 1981-10-13 | Shin-Etsu Chemical Co. Ltd. | Hydroalkenyloxysilanes |
US5089649A (en) * | 1989-04-28 | 1992-02-18 | Shin-Etsu Chemical Co., Ltd. | Organosilicon compound |
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