GB1049270A - Recovery of monochlorodimethyl ether - Google Patents

Recovery of monochlorodimethyl ether

Info

Publication number
GB1049270A
GB1049270A GB4588465A GB4588465A GB1049270A GB 1049270 A GB1049270 A GB 1049270A GB 4588465 A GB4588465 A GB 4588465A GB 4588465 A GB4588465 A GB 4588465A GB 1049270 A GB1049270 A GB 1049270A
Authority
GB
United Kingdom
Prior art keywords
hydrogen chloride
monochlorodimethyl ether
spent
recovered
monochlorodimethyl
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB4588465A
Inventor
Reinhard Bachmann
Eberhard Dabrunz
Rudiger Hauptmann
Hans Reuter
Gerhard Schwachula
Dieter Warnecke
Wilhelm Wehland
Friedrich Wolf
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Filmfabrik Wolfen VEB
Original Assignee
Filmfabrik Wolfen VEB
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Filmfabrik Wolfen VEB filed Critical Filmfabrik Wolfen VEB
Priority to GB4588465A priority Critical patent/GB1049270A/en
Publication of GB1049270A publication Critical patent/GB1049270A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C43/00—Ethers; Compounds having groups, groups or groups
    • C07C43/02—Ethers
    • C07C43/03—Ethers having all ether-oxygen atoms bound to acyclic carbon atoms
    • C07C43/04—Saturated ethers
    • C07C43/12—Saturated ethers containing halogen

Abstract

Monochlorodimethyl ether is recovered from spent chloromethylation solutions by entrainment in a stream of inert gas which is passed through the solution at 0-60 DEG C. The spent solutions which are contaminated with, e.g., catalysts and by-products are, e.g., those resulting from the chloromethylation of divinyl compounds and polymers thereof. Specified inert gases are air, nitrogen and hydrogen chloride. The preferred gas is hydrogen chloride as the resulting mixture of hydrogen chloride and monochlorodimethyl ether, which also contains some methylol recovered from the spent solution, can be used in the synthesis of further monochlorodimethyl ether by reaction with additional methylol or methanol and formaldehyde or a polymeric formaldehyde. Alternatively, the monochlorodimethyl ether can be recovered directly by cooling the emerging gas stream. Examples relate to the use of hydrogen chloride.
GB4588465A 1965-10-29 1965-10-29 Recovery of monochlorodimethyl ether Expired GB1049270A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB4588465A GB1049270A (en) 1965-10-29 1965-10-29 Recovery of monochlorodimethyl ether

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB4588465A GB1049270A (en) 1965-10-29 1965-10-29 Recovery of monochlorodimethyl ether

Publications (1)

Publication Number Publication Date
GB1049270A true GB1049270A (en) 1966-11-23

Family

ID=10438967

Family Applications (1)

Application Number Title Priority Date Filing Date
GB4588465A Expired GB1049270A (en) 1965-10-29 1965-10-29 Recovery of monochlorodimethyl ether

Country Status (1)

Country Link
GB (1) GB1049270A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS60137908A (en) * 1983-12-26 1985-07-22 Mitsubishi Chem Ind Ltd Production of chloromethylated polymer
US4900796A (en) * 1988-02-02 1990-02-13 Rohm And Haas Company Process for preparing chloromethylated aromatic materials
US5600022A (en) * 1993-12-27 1997-02-04 Mitsubishi Chemical Corporation Method for recovering chloromethyl methyl ether

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS60137908A (en) * 1983-12-26 1985-07-22 Mitsubishi Chem Ind Ltd Production of chloromethylated polymer
JPS6261204B2 (en) * 1983-12-26 1987-12-21 Mitsubishi Chem Ind
US4900796A (en) * 1988-02-02 1990-02-13 Rohm And Haas Company Process for preparing chloromethylated aromatic materials
US5600022A (en) * 1993-12-27 1997-02-04 Mitsubishi Chemical Corporation Method for recovering chloromethyl methyl ether

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