GB1028063A - Grease composition - Google Patents

Grease composition

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Publication number
GB1028063A
GB1028063A GB13650/63A GB1365063A GB1028063A GB 1028063 A GB1028063 A GB 1028063A GB 13650/63 A GB13650/63 A GB 13650/63A GB 1365063 A GB1365063 A GB 1365063A GB 1028063 A GB1028063 A GB 1028063A
Authority
GB
United Kingdom
Prior art keywords
carbonated
basic
mineral oil
acids
promoter
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB13650/63A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Lubrizol Corp
Original Assignee
Lubrizol Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US185521A external-priority patent/US3242079A/en
Application filed by Lubrizol Corp filed Critical Lubrizol Corp
Publication of GB1028063A publication Critical patent/GB1028063A/en
Expired legal-status Critical Current

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    • C10M159/12—Reaction products
    • C10M159/20—Reaction mixtures having an excess of neutralising base, e.g. so-called overbasic or highly basic products
    • C10M159/24—Reaction mixtures having an excess of neutralising base, e.g. so-called overbasic or highly basic products containing sulfonic radicals
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    • C10N2070/00—Specific manufacturing methods for lubricant compositions
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2070/00—Specific manufacturing methods for lubricant compositions
    • C10N2070/02—Concentrating of additives

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)

Abstract

Homogeneous grease compositions are prepared by mixing a fluid mineral oil solution containing 10-70% of a carbonated alkaline earth metal sulphonate and/or carboxylate which has at least 12 carbon atoms, was basic before carbonation, and has a metal ratio of at least 4.5, with 1-80%, based on the carbonated salt, of an active hydrogen compound selected from water, water-alcohol mixtures, and lower aliphatic carboxylic acids, at a temperature between 25 DEG C. and the reflux temperature. The carbonated sulphonates may be derived from petroleum or otherwise, and the carbonated carboxylates from aliphatic or aromatic acids, extensive exemplification being given. The carbonated salt may be basic, neutral, or slightly acidic, and may have been prepared by carbonating a basic sulphonate or carboxylate in the presence of a promoting agent selected from alcohols, phenols, mercaptans, amines, enols, and aci-nitro compounds, preferably in the presence of a mineral oil or other hydrocarbon solvent. Many active hydrogen compounds are mentioned, typical being acetic acid, dichloroacetic acid, heptoic acid, and mixtures of water with methanol, ethanol, bromo-octanol, chloro-hexanol, glycerol, diethylene glycol, and ethylene glycol monomethyl ether. The resulting greases may be used per se, or as additives to lubricants, cutting oils, fuels, asphalts or caulking compositions.ALSO:Basic alkaline earth metal salts of carboxylic and sulphonic acids having at least 12 carbon atoms are carbonated in the presence of a promoter, and preferably in a hydrocarbon solvent, especially a mineral oil. The promoter may be a phenol, alcohol, mercaptan, amine, enol, or aci-nitro compound. In examples, mixtures of either tall oil acids or petroleum sulphonates with excess metal base (CaO, BaO, Ca(OH)2 or Ba(OH)2) are carbonated in the presence of a promoter selected from heptyl and octyl phenols, and methyl and furfuryl alcohols, the solvent, when present, being mineral oil, to give final products which are basic, neutral, or slightly acidic, and have a metal ratio of at least 4.5.
GB13650/63A 1962-04-06 1963-04-05 Grease composition Expired GB1028063A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US185521A US3242079A (en) 1962-04-06 1962-04-06 Basic metal-containing thickened oil compositions
US535693A US3372115A (en) 1962-04-06 1966-03-21 Basic metal-containing thickened oil compositions

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GB1028063A true GB1028063A (en) 1966-05-04

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US (1) US3372115A (en)
BE (1) BE695686A (en)
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US4650692A (en) * 1985-11-01 1987-03-17 Ashland Oil, Inc. Metal-sulfonate/piperidine derivative combination protective coatings
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US5190678A (en) * 1990-11-02 1993-03-02 Conoco Inc. Process for the preparation of over-based group 2A metal sulfonate greases and thickened compositions
EP0490255A1 (en) * 1990-12-07 1992-06-17 Hoechst Aktiengesellschaft Process for the preparation of calciumsulfonate/-calcium carbonate complexes
US5401424A (en) * 1993-10-04 1995-03-28 The Lubrizol Corporation Mixed carboxylate overbased gels
ES2175149T3 (en) * 1995-10-10 2002-11-16 Prc Desoto Int Inc CHROMATE EXEMPT CORROSION INHIBITORS FOR ALUMINUM ALLOYS.
US5919741A (en) * 1998-01-20 1999-07-06 The Lubrizol Corporation Overbased carboxylate gels
US6107259A (en) * 1998-07-15 2000-08-22 Witco Corporation Oil soluble calcite overbased detergents and engine oils containing same
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US9976101B2 (en) 2011-10-31 2018-05-22 Nch Corporation Method of manufacturing calcium sulfonate greases using delayed addition of non-aqueous converting agents
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BR112014010522B1 (en) 2011-10-31 2022-02-15 Nch Corporation COMPLEX AND SIMPLE CALCIUM SULFONATE GREASE COMPOSITIONS, AND METHOD FOR PRODUCING AN OVERBASED CALCIUM SULFONATE COMPLEX GREASE
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US10087388B2 (en) 2016-05-18 2018-10-02 Nch Corporation Composition and method of manufacturing calcium sulfonate and calcium magnesium sulfonate greases using a delay after addition of facilitating acid
US10087387B2 (en) 2016-05-18 2018-10-02 Nch Corporation Composition and method of manufacturing calcium magnesium sulfonate greases
US10087391B2 (en) 2016-05-18 2018-10-02 Nch Corporation Composition and method of manufacturing calcium magnesium sulfonate greases without a conventional non-aqueous converting agent
US10392577B2 (en) 2016-05-18 2019-08-27 Nch Corporation Composition and method of manufacturing overbased sulfonate modified lithium carboxylate grease
US10519393B2 (en) 2016-05-18 2019-12-31 Nch Corporation Composition and method of manufacturing calcium magnesium sulfonate greases
TWI693043B (en) * 2018-07-31 2020-05-11 川湖科技股份有限公司 Adjustment mechanism
US11661563B2 (en) 2020-02-11 2023-05-30 Nch Corporation Composition and method of manufacturing and using extremely rheopectic sulfonate-based greases
AU2021261736A1 (en) 2020-04-22 2022-11-17 Chevron U.S.A. Inc. High performance grease compositions with a renewable base oil
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BE695686A (en) 1967-09-18
US3372115A (en) 1968-03-05

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