FR2985737B1 - Procede de pretraitement de la biomasse lignocellulosique avec un sel inorganique hydrate comprenant une etape d'hydrolyse acide preliminaire - Google Patents
Procede de pretraitement de la biomasse lignocellulosique avec un sel inorganique hydrate comprenant une etape d'hydrolyse acide preliminaire Download PDFInfo
- Publication number
- FR2985737B1 FR2985737B1 FR1200157A FR1200157A FR2985737B1 FR 2985737 B1 FR2985737 B1 FR 2985737B1 FR 1200157 A FR1200157 A FR 1200157A FR 1200157 A FR1200157 A FR 1200157A FR 2985737 B1 FR2985737 B1 FR 2985737B1
- Authority
- FR
- France
- Prior art keywords
- fraction
- solid fraction
- inorganic salt
- acid hydrolysis
- lignocellulosic biomass
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 238000005903 acid hydrolysis reaction Methods 0.000 title abstract 2
- 229910017053 inorganic salt Inorganic materials 0.000 title abstract 2
- 239000002029 lignocellulosic biomass Substances 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- 239000007787 solid Substances 0.000 abstract 7
- 239000007788 liquid Substances 0.000 abstract 4
- 238000000926 separation method Methods 0.000 abstract 2
- 239000002028 Biomass Substances 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 150000001450 anions Chemical group 0.000 abstract 1
- 238000010411 cooking Methods 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
- 230000000737 periodic effect Effects 0.000 abstract 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D307/40—Radicals substituted by oxygen atoms
- C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
- C07D307/48—Furfural
- C07D307/50—Preparation from natural products
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K13/00—Sugars not otherwise provided for in this class
- C13K13/002—Xylose
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P19/00—Preparation of compounds containing saccharide radicals
- C12P19/02—Monosaccharides
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P19/00—Preparation of compounds containing saccharide radicals
- C12P19/14—Preparation of compounds containing saccharide radicals produced by the action of a carbohydrase (EC 3.2.x), e.g. by alpha-amylase, e.g. by cellulase, hemicellulase
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P7/00—Preparation of oxygen-containing organic compounds
- C12P7/02—Preparation of oxygen-containing organic compounds containing a hydroxy group
- C12P7/04—Preparation of oxygen-containing organic compounds containing a hydroxy group acyclic
- C12P7/06—Ethanol, i.e. non-beverage
- C12P7/08—Ethanol, i.e. non-beverage produced as by-product or from waste or cellulosic material substrate
- C12P7/10—Ethanol, i.e. non-beverage produced as by-product or from waste or cellulosic material substrate substrate containing cellulosic material
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- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C1/00—Pretreatment of the finely-divided materials before digesting
- D21C1/04—Pretreatment of the finely-divided materials before digesting with acid reacting compounds
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C3/00—Pulping cellulose-containing materials
- D21C3/04—Pulping cellulose-containing materials with acids, acid salts or acid anhydrides
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C3/00—Pulping cellulose-containing materials
- D21C3/18—Pulping cellulose-containing materials with halogens or halogen-generating compounds
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C3/00—Pulping cellulose-containing materials
- D21C3/20—Pulping cellulose-containing materials with organic solvents or in solvent environment
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P2201/00—Pretreatment of cellulosic or lignocellulosic material for subsequent enzymatic treatment or hydrolysis
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Zoology (AREA)
- Wood Science & Technology (AREA)
- Biochemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Microbiology (AREA)
- General Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Biotechnology (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Processing Of Solid Wastes (AREA)
- Compounds Of Unknown Constitution (AREA)
Abstract
La présente invention décrit un procédé de prétraitement de biomasse lignocellulosique comprenant : a) une étape d'hydrolyse acide de la biomasse par une solution acide conduisant à une fraction liquide et à une fraction solide, b) une étape de séparation de la fraction solide et de la fraction liquide, c) une étape de séchage de la fraction solide, d) une étape de cuisson de la fraction solide séchée dans un milieu comprenant au moins un sel inorganique hydraté de formule : MX .n'H O dans lequel M un métal choisi dans les groupes 1 à 13 de la classification périodique, X est un anion et n est un nombre entier compris entre 1 et 6 et n'étant compris entre 0,5 et 12, permettant d'obtenir une fraction solide et une fraction liquide, e) une étape de séparation de la fraction solide et de la fraction liquide obtenues dans l'étape d), f) éventuellement une étape de traitement de ladite fraction solide de l'étape e).
Priority Applications (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR1200157A FR2985737B1 (fr) | 2012-01-18 | 2012-01-18 | Procede de pretraitement de la biomasse lignocellulosique avec un sel inorganique hydrate comprenant une etape d'hydrolyse acide preliminaire |
EP12821262.8A EP2804951A1 (fr) | 2012-01-18 | 2012-12-11 | Procede de pretraitement de la biomasse lignocellulosique avec un sel inorganique hydrate comprenant une etape d'hydrolyse acide preliminaire |
US14/372,818 US20140352688A1 (en) | 2012-01-18 | 2012-12-11 | Process for pretreatment of lignocellulosic biomass with a hydrated inorganic salt comprising a preliminary acid hydrolysis stage |
PCT/FR2012/000515 WO2013107948A1 (fr) | 2012-01-18 | 2012-12-11 | Procede de pretraitement de la biomasse lignocellulosique avec un sel inorganique hydrate comprenant une etape d'hydrolyse acide preliminaire |
BR112014017596A BR112014017596A8 (pt) | 2012-01-18 | 2012-12-11 | Processo de pré-tratamento da biomassa lignocelulósica com um sal inorgânico hidratado, compreendendo uma etapa de hidrólise ácida preliminar |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR1200157 | 2012-01-18 | ||
FR1200157A FR2985737B1 (fr) | 2012-01-18 | 2012-01-18 | Procede de pretraitement de la biomasse lignocellulosique avec un sel inorganique hydrate comprenant une etape d'hydrolyse acide preliminaire |
Publications (2)
Publication Number | Publication Date |
---|---|
FR2985737A1 FR2985737A1 (fr) | 2013-07-19 |
FR2985737B1 true FR2985737B1 (fr) | 2020-01-10 |
Family
ID=47666388
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FR1200157A Active FR2985737B1 (fr) | 2012-01-18 | 2012-01-18 | Procede de pretraitement de la biomasse lignocellulosique avec un sel inorganique hydrate comprenant une etape d'hydrolyse acide preliminaire |
Country Status (5)
Country | Link |
---|---|
US (1) | US20140352688A1 (fr) |
EP (1) | EP2804951A1 (fr) |
BR (1) | BR112014017596A8 (fr) |
FR (1) | FR2985737B1 (fr) |
WO (1) | WO2013107948A1 (fr) |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20170211231A1 (en) * | 2014-07-10 | 2017-07-27 | Leaf Sciences Pty Ltd | Methods for Treating Lignocellulosic Material |
FR3029531B1 (fr) * | 2014-12-08 | 2018-06-01 | IFP Energies Nouvelles | Procede de pretraitement de biomasse lignocellulosique dans les sels inorganiques hydrates |
CA2995560C (fr) * | 2015-08-31 | 2023-08-01 | Avantium Knowledge Centre B.V. | Procede de recuperation d'acide chlorhydrique |
TWI653085B (zh) | 2016-06-13 | 2019-03-11 | 鼎唐能源科技股份有限公司 | 從水解纖維素製程產物水溶液中分離醣類的方法 |
CN109097502B (zh) * | 2018-07-23 | 2021-08-10 | 华南理工大学 | 一种可循环使用的草酸预处理木质纤维制备木糖的方法 |
CN109182395B (zh) * | 2018-08-17 | 2020-10-20 | 中国科学院青岛生物能源与过程研究所 | 与纤维小体全菌糖化匹配的木质纤维类生物质的预处理方法 |
Family Cites Families (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR1003093A (fr) | 1946-12-03 | 1952-03-13 | Volcan Sa | Robinet régulateur |
FR1003092A (fr) | 1946-12-03 | 1952-03-13 | Lit-armoire | |
GB767096A (en) | 1953-06-18 | 1957-01-30 | Coal Industry Patents Ltd | Improvements in or relating to devices for taking samples |
EP0091221B1 (fr) * | 1982-04-05 | 1987-09-09 | Imperial Chemical Industries Plc | Dissolution et hydrolyse des hydrates de carbone |
US4452640A (en) * | 1982-05-11 | 1984-06-05 | Purdue Research Foundation | Quantitative hydrolysis of cellulose to glucose using zinc chloride |
AU2003904323A0 (en) | 2003-08-13 | 2003-08-28 | Viridian Chemical Pty Ltd | Solvents based on salts of aryl acids |
FI116142B (fi) | 2003-09-11 | 2005-09-30 | Kemira Oyj | Esteröintimenetelmä |
US8182557B2 (en) * | 2007-02-06 | 2012-05-22 | North Carolina State University | Use of lignocellulosics solvated in ionic liquids for production of biofuels |
US8652261B2 (en) * | 2009-09-01 | 2014-02-18 | Kior, Inc. | Process for dissolving cellulose-containing biomass material in an ionic liquid medium |
WO2011027223A1 (fr) | 2009-09-01 | 2011-03-10 | Paul O'connor | Prétraitement d'un matériau de biomasse solide contenant de la cellulose au moyen d'un milieu liquide ionique |
NL2004761C2 (en) * | 2010-05-25 | 2011-11-29 | Univ Delft Tech | Process for the treatment of lignocellulosic biomass. |
FR2963009B1 (fr) * | 2010-07-23 | 2013-01-04 | IFP Energies Nouvelles | Procede de production de sucres a partir de biomasse lignocellulosique pretraitee avec des sels inorganiques hydrates |
FR2963008B1 (fr) * | 2010-07-23 | 2013-01-04 | IFP Energies Nouvelles | Procede de production de sucres a partir de biomasse lignocellulosique pretraitee avec un melange de sels inorganiques hydrates et de sels metalliques |
-
2012
- 2012-01-18 FR FR1200157A patent/FR2985737B1/fr active Active
- 2012-12-11 EP EP12821262.8A patent/EP2804951A1/fr not_active Withdrawn
- 2012-12-11 US US14/372,818 patent/US20140352688A1/en not_active Abandoned
- 2012-12-11 WO PCT/FR2012/000515 patent/WO2013107948A1/fr active Application Filing
- 2012-12-11 BR BR112014017596A patent/BR112014017596A8/pt not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
BR112014017596A2 (fr) | 2017-06-20 |
FR2985737A1 (fr) | 2013-07-19 |
WO2013107948A1 (fr) | 2013-07-25 |
US20140352688A1 (en) | 2014-12-04 |
BR112014017596A8 (pt) | 2017-07-11 |
EP2804951A1 (fr) | 2014-11-26 |
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