FR2910353B1 - PROCESS FOR HYDROCONVERSION IN SLURRY OF HEAVY HYDROCARBON LOADS IN THE PRESENCE OF A DISPERSE ACTIVE PHASE AND AN ALUMINUM OXIDE - Google Patents

PROCESS FOR HYDROCONVERSION IN SLURRY OF HEAVY HYDROCARBON LOADS IN THE PRESENCE OF A DISPERSE ACTIVE PHASE AND AN ALUMINUM OXIDE

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Publication number
FR2910353B1
FR2910353B1 FR0611405A FR0611405A FR2910353B1 FR 2910353 B1 FR2910353 B1 FR 2910353B1 FR 0611405 A FR0611405 A FR 0611405A FR 0611405 A FR0611405 A FR 0611405A FR 2910353 B1 FR2910353 B1 FR 2910353B1
Authority
FR
France
Prior art keywords
hydroconversion
slurry
aluminum oxide
heavy hydrocarbon
active phase
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
FR0611405A
Other languages
French (fr)
Other versions
FR2910353A1 (en
Inventor
Auberger Magalie Roy
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
IFP Energies Nouvelles IFPEN
Original Assignee
IFP Energies Nouvelles IFPEN
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by IFP Energies Nouvelles IFPEN filed Critical IFP Energies Nouvelles IFPEN
Priority to FR0611405A priority Critical patent/FR2910353B1/en
Priority to CA2615210A priority patent/CA2615210C/en
Priority to US11/961,688 priority patent/US7666296B2/en
Priority to CN2007101691878A priority patent/CN101255359B/en
Priority to SA7280723A priority patent/SA07280723B1/en
Publication of FR2910353A1 publication Critical patent/FR2910353A1/en
Application granted granted Critical
Publication of FR2910353B1 publication Critical patent/FR2910353B1/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/02—Sulfur, selenium or tellurium; Compounds thereof
    • B01J27/04—Sulfides
    • B01J27/043—Sulfides with iron group metals or platinum group metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/02—Boron or aluminium; Oxides or hydroxides thereof
    • B01J21/04—Alumina
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/02—Sulfur, selenium or tellurium; Compounds thereof
    • B01J27/04—Sulfides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/02—Sulfur, selenium or tellurium; Compounds thereof
    • B01J27/04—Sulfides
    • B01J27/047—Sulfides with chromium, molybdenum, tungsten or polonium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/02—Sulfur, selenium or tellurium; Compounds thereof
    • B01J27/04—Sulfides
    • B01J27/047—Sulfides with chromium, molybdenum, tungsten or polonium
    • B01J27/051—Molybdenum
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0018—Addition of a binding agent or of material, later completely removed among others as result of heat treatment, leaching or washing,(e.g. forming of pores; protective layer, desintegrating by heat)
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B01J37/0203—Impregnation the impregnation liquid containing organic compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B01J37/0207—Pretreatment of the support
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • B01J37/10—Heat treatment in the presence of water, e.g. steam
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/20—Sulfiding
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/40—Catalysts, in general, characterised by their form or physical properties characterised by dimensions, e.g. grain size
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/613—10-100 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/615—100-500 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/63—Pore volume
    • B01J35/635—0.5-1.0 ml/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/63—Pore volume
    • B01J35/638—Pore volume more than 1.0 ml/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/66—Pore distribution
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0027—Powdering
    • B01J37/0036—Grinding
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/107—Atmospheric residues having a boiling point of at least about 538 °C

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Catalysts (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
FR0611405A 2006-12-21 2006-12-21 PROCESS FOR HYDROCONVERSION IN SLURRY OF HEAVY HYDROCARBON LOADS IN THE PRESENCE OF A DISPERSE ACTIVE PHASE AND AN ALUMINUM OXIDE Active FR2910353B1 (en)

Priority Applications (5)

Application Number Priority Date Filing Date Title
FR0611405A FR2910353B1 (en) 2006-12-21 2006-12-21 PROCESS FOR HYDROCONVERSION IN SLURRY OF HEAVY HYDROCARBON LOADS IN THE PRESENCE OF A DISPERSE ACTIVE PHASE AND AN ALUMINUM OXIDE
CA2615210A CA2615210C (en) 2006-12-21 2007-12-19 Process for slurry hydroconversion of heavy hydrocarbon charges in the presence of a dispersed active phase and an alumina oxide
US11/961,688 US7666296B2 (en) 2006-12-21 2007-12-20 Process for the hydroconversion in a slurry of heavy hydrocarbonaceous feedstocks in the presence of a dispersed phase and an alumina-based oxide
CN2007101691878A CN101255359B (en) 2006-12-21 2007-12-21 Process for hydroconversion in slurry of heavy hydrocarbonaceous feedstocks in presence of dispersed phase and alumina-based oxide
SA7280723A SA07280723B1 (en) 2006-12-21 2007-12-29 Process for the Hydroconversion in a Slurry of Heavy Hydrocarbonaceous Feedstocks in the Presence of a Dispersed Phase and an Alumina-Based Oxide

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR0611405A FR2910353B1 (en) 2006-12-21 2006-12-21 PROCESS FOR HYDROCONVERSION IN SLURRY OF HEAVY HYDROCARBON LOADS IN THE PRESENCE OF A DISPERSE ACTIVE PHASE AND AN ALUMINUM OXIDE

Publications (2)

Publication Number Publication Date
FR2910353A1 FR2910353A1 (en) 2008-06-27
FR2910353B1 true FR2910353B1 (en) 2009-03-06

Family

ID=38469153

Family Applications (1)

Application Number Title Priority Date Filing Date
FR0611405A Active FR2910353B1 (en) 2006-12-21 2006-12-21 PROCESS FOR HYDROCONVERSION IN SLURRY OF HEAVY HYDROCARBON LOADS IN THE PRESENCE OF A DISPERSE ACTIVE PHASE AND AN ALUMINUM OXIDE

Country Status (5)

Country Link
US (1) US7666296B2 (en)
CN (1) CN101255359B (en)
CA (1) CA2615210C (en)
FR (1) FR2910353B1 (en)
SA (1) SA07280723B1 (en)

Families Citing this family (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2958658B1 (en) 2010-04-13 2012-03-30 Inst Francais Du Petrole METHOD FOR HYDROCONVERSION OF PETROLEUM LOADS VIA SLURRY TECHNOLOGY FOR RECOVERING METALS FROM THE CATALYST AND THE LOAD USING A LEACHING STEP.
FR2958656B1 (en) 2010-04-13 2012-05-11 Inst Francais Du Petrole METHOD FOR HYDROCONVERSION OF PETROLEUM LOADS VIA SLURRY TECHNOLOGY FOR RECOVERING METALS FROM THE CATALYST AND THE LOAD USING AN EXTRACTION STEP
FR2958657B1 (en) 2010-04-13 2012-05-11 Inst Francais Du Petrole METHOD OF HYDROCONVERSIONING PETROLEUM LOADS THROUGH SLURRY TECHNOLOGY FOR RECOVERING METALS FROM THE CATALYST AND THE LOAD USING A COKEFACTION STEP.
US9243194B2 (en) 2009-10-08 2016-01-26 IFP Energies Nouvelles Process for hydroconversion of heavy carbon-containing feedstocks that integrate a boiling-bed technology and a slurry technology
US8704020B2 (en) * 2010-12-13 2014-04-22 Exxonmobil Research And Engineering Company Catalytic hydrothermal treatment of biomass
US8624070B2 (en) 2010-12-13 2014-01-07 Exxonmobil Research And Engineering Company Phosphorus recovery from hydrothermal treatment of biomass
US8704019B2 (en) * 2010-12-13 2014-04-22 Exxonmobil Research And Engineering Company Catalyst recovery in hydrothermal treatment of biomass
US8487148B2 (en) 2010-12-13 2013-07-16 Exxonmobil Research And Engineering Company Hydrothermal treatment of biomass with heterogeneous catalyst
FR2974109B1 (en) 2011-04-14 2013-04-12 IFP Energies Nouvelles BIOMASS HYDROCONVERSION PROCESS INCORPORATING A TECHNOLOGY USING A REACTOR COMPRISING A DISPERSED CATALYST
FR2974108B1 (en) * 2011-04-14 2014-11-28 IFP Energies Nouvelles HYDROCONVERSION PROCESS OF BIOMASS INCLUDING A BOILING BED TECHNOLOGY AND A SLURRY TECHNOLOGY
FR3027911B1 (en) 2014-11-04 2018-04-27 IFP Energies Nouvelles METHOD FOR CONVERTING PETROLEUM LOADS COMPRISING A BOILING BED HYDROCRACKING STEP, MATURATION STEP AND SEDIMENT SEPARATION STEP FOR THE PRODUCTION OF LOW SEDIMENT FOLDS
FR3027912B1 (en) 2014-11-04 2018-04-27 IFP Energies Nouvelles PROCESS FOR PRODUCING HEAVY FUEL TYPE FUELS FROM A HEAVY HYDROCARBON LOAD USING A SEPARATION BETWEEN THE HYDROTREATING STEP AND THE HYDROCRACKING STEP
FR3074699B1 (en) * 2017-12-13 2019-12-20 IFP Energies Nouvelles PROCESS FOR HYDROCONVERSION OF HEAVY HYDROCARBON CHARGE INTO HYBRID REACTOR
FR3074698B1 (en) * 2017-12-13 2019-12-27 IFP Energies Nouvelles PROCESS FOR HYDROCONVERSION TO HEAVY HYDROCARBON LOAD SLURRY
FR3075810B1 (en) 2017-12-21 2020-09-11 Ifp Energies Now IMPROVED RESIDUE CONVERSION PROCESS INTEGRATING DEEP HYDROCONVERSION STAGES AND A DESASPHALTING STAGE
FR3114598B1 (en) 2020-09-25 2023-09-29 Ifp Energies Now METHOD FOR TREATMENT OF PLASTIC PYROLYSIS OILS AND/OR RECOVERED SOLID FUELS LOADED WITH IMPURITIES
FR3122663B1 (en) 2021-05-07 2024-04-26 Ifp Energies Now INTEGRATED PROCESS FOR TREATMENT OF PLASTICS PYROLYSIS OILS AND/OR RECOVERED SOLID FUELS LOADED WITH IMPURITIES
FR3128225A1 (en) 2021-10-19 2023-04-21 IFP Energies Nouvelles METHOD FOR TREATMENT OF PYROLYSIS OILS FROM PLASTICS AND/OR SOLID RECOVERY FUELS LOADED WITH IMPURITIES

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3231486A (en) 1960-12-16 1966-01-25 Union Carbide Corp Catalytic hydrogenation of carbonized coal vapors
US3231488A (en) * 1963-10-28 1966-01-25 Universal Oil Prod Co Process for hydrorefining heavy hydrocarbon charge stocks and catalyst therefor
US3361682A (en) * 1965-06-11 1968-01-02 Engelhard Ind Inc Alumina-based catalyst and method of preparing same
US5244648A (en) * 1980-12-23 1993-09-14 Rhone-Poulenc Industries Process for the preparation of alumina agglomerates
FR2528721B1 (en) * 1982-06-17 1986-02-28 Pro Catalyse Ste Fse Prod Cata SUPPORTED CATALYST HAVING INCREASED RESISTANCE TO POISONS AND ITS USE IN PARTICULAR FOR THE HYDROTREATMENT OF OIL FRACTIONS CONTAINING METALS
FR2534828B1 (en) * 1982-10-21 1986-12-26 Pro Catalyse ALUMINA, SILICA OR SILICA-ALUMINA-BASED CATALYSTS, THEIR PREPARATION AND THEIR USE IN THE FIELD OF HYDROPROCESSING OF HYDROCARBON OILS
US6712955B1 (en) * 1997-07-15 2004-03-30 Exxonmobil Research And Engineering Company Slurry hydroprocessing using bulk multimetallic catalysts
CA2216671C (en) * 1997-09-24 2000-12-05 Richard Anthony Mcfarlane Process for dispersing transition metal catalytic particles in heavy oil
FR2787040B1 (en) * 1998-12-10 2001-01-19 Inst Francais Du Petrole HYDROTREATMENT OF HYDROCARBON CHARGES IN A BOILING BED REACTOR
FR2787041B1 (en) * 1998-12-10 2001-01-19 Inst Francais Du Petrole HYDROCARBON CHARGE HYDROTREATMENT CATALYST IN A FIXED BED REACTOR

Also Published As

Publication number Publication date
FR2910353A1 (en) 2008-06-27
SA07280723B1 (en) 2010-12-01
CA2615210A1 (en) 2008-06-21
US7666296B2 (en) 2010-02-23
CN101255359A (en) 2008-09-03
US20080177124A1 (en) 2008-07-24
CN101255359B (en) 2013-10-30
CA2615210C (en) 2015-10-13

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