FR2406650A1 - PROCESS FOR PURIFYING SILICONE RESINS WITH A VIEW TO REDUCING THEIR WEIGHT LOSS UNDER PRESSURE VACUUM - Google Patents
PROCESS FOR PURIFYING SILICONE RESINS WITH A VIEW TO REDUCING THEIR WEIGHT LOSS UNDER PRESSURE VACUUMInfo
- Publication number
- FR2406650A1 FR2406650A1 FR7731902A FR7731902A FR2406650A1 FR 2406650 A1 FR2406650 A1 FR 2406650A1 FR 7731902 A FR7731902 A FR 7731902A FR 7731902 A FR7731902 A FR 7731902A FR 2406650 A1 FR2406650 A1 FR 2406650A1
- Authority
- FR
- France
- Prior art keywords
- reducing
- view
- silicone resins
- under pressure
- weight loss
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/32—Post-polymerisation treatment
- C08G77/34—Purification
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Silicon Polymers (AREA)
- Detergent Compositions (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Extraction Or Liquid Replacement (AREA)
Abstract
L'invention se rapporte aux silicones. Elle concerne un procédé de purification de résines silicones commerciales, caractérisé en ce qu'il consiste : A. à dissoudre la résine silicone commerciale dans un solvant, B. à précipiter les chaînes longues de prépolymère par un non solvant, C. à séparer le précipité formé, et D. à évaporer ensuite le solvant et le non solvant résiduels du précipité séparé. Les résines obtenues sont utiles notamment dans des applications spatiales.The invention relates to silicones. It relates to a process for the purification of commercial silicone resins, characterized in that it consists: A. in dissolving the commercial silicone resin in a solvent, B. in precipitating the long prepolymer chains with a non-solvent, C. in separating the precipitate formed, and D. then evaporating the residual solvent and non-solvent from the separated precipitate. The resins obtained are useful in particular in space applications.
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR7731902A FR2406650A1 (en) | 1977-10-24 | 1977-10-24 | PROCESS FOR PURIFYING SILICONE RESINS WITH A VIEW TO REDUCING THEIR WEIGHT LOSS UNDER PRESSURE VACUUM |
GB7841512A GB2009195A (en) | 1977-10-24 | 1978-10-23 | Process of Purification of Silicone Materials |
DE19782846305 DE2846305C2 (en) | 1977-10-24 | 1978-10-24 | Process for removing low molecular weight organopolysiloxanes and impurities from curable organopolysiloxanes of technical purity |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR7731902A FR2406650A1 (en) | 1977-10-24 | 1977-10-24 | PROCESS FOR PURIFYING SILICONE RESINS WITH A VIEW TO REDUCING THEIR WEIGHT LOSS UNDER PRESSURE VACUUM |
Publications (2)
Publication Number | Publication Date |
---|---|
FR2406650A1 true FR2406650A1 (en) | 1979-05-18 |
FR2406650B1 FR2406650B1 (en) | 1981-12-18 |
Family
ID=9196847
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FR7731902A Granted FR2406650A1 (en) | 1977-10-24 | 1977-10-24 | PROCESS FOR PURIFYING SILICONE RESINS WITH A VIEW TO REDUCING THEIR WEIGHT LOSS UNDER PRESSURE VACUUM |
Country Status (3)
Country | Link |
---|---|
DE (1) | DE2846305C2 (en) |
FR (1) | FR2406650A1 (en) |
GB (1) | GB2009195A (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2639951A1 (en) * | 1988-11-25 | 1990-06-08 | Rhone Poulenc Chimie | PROCESS FOR OBTAINING A THREADABLE AND CERAMISABLE POLYCARBOSILANE |
EP0492001A1 (en) * | 1990-12-28 | 1992-07-01 | Dow Corning Toray Silicone Company, Limited | Silicone-modified thermoplastic resin |
FR2747683A1 (en) * | 1996-04-19 | 1997-10-24 | Centre Nat Etd Spatiales | Stabilisation of silicone resins for use in spatial applications |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE4300168A1 (en) * | 1993-01-07 | 1994-07-14 | Penn White Ltd | Depolymerization agents and depolymerization processes for silicones |
DE10032820A1 (en) * | 2000-07-06 | 2002-01-24 | Wacker Chemie Gmbh | Process for the isolation of polyorganosiloxanes |
-
1977
- 1977-10-24 FR FR7731902A patent/FR2406650A1/en active Granted
-
1978
- 1978-10-23 GB GB7841512A patent/GB2009195A/en not_active Withdrawn
- 1978-10-24 DE DE19782846305 patent/DE2846305C2/en not_active Expired
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2639951A1 (en) * | 1988-11-25 | 1990-06-08 | Rhone Poulenc Chimie | PROCESS FOR OBTAINING A THREADABLE AND CERAMISABLE POLYCARBOSILANE |
EP0377351A1 (en) * | 1988-11-25 | 1990-07-11 | Rhone-Poulenc Chimie | Process for preparing a spinnable ceramic-forming polycarbosilane |
US5028678A (en) * | 1988-11-25 | 1991-07-02 | Rhone-Poulenc Chimie | Extrudable pre-ceramic polycarbosilanes |
EP0492001A1 (en) * | 1990-12-28 | 1992-07-01 | Dow Corning Toray Silicone Company, Limited | Silicone-modified thermoplastic resin |
FR2747683A1 (en) * | 1996-04-19 | 1997-10-24 | Centre Nat Etd Spatiales | Stabilisation of silicone resins for use in spatial applications |
Also Published As
Publication number | Publication date |
---|---|
DE2846305C2 (en) | 1983-05-05 |
DE2846305A1 (en) | 1979-04-26 |
FR2406650B1 (en) | 1981-12-18 |
GB2009195A (en) | 1979-06-13 |
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