FR2398799A1 - Isomerising hops extract to form iso-alpha-acids for beer - using non aq. alkali followed by aq. extraction - Google Patents
Isomerising hops extract to form iso-alpha-acids for beer - using non aq. alkali followed by aq. extractionInfo
- Publication number
- FR2398799A1 FR2398799A1 FR7822184A FR7822184A FR2398799A1 FR 2398799 A1 FR2398799 A1 FR 2398799A1 FR 7822184 A FR7822184 A FR 7822184A FR 7822184 A FR7822184 A FR 7822184A FR 2398799 A1 FR2398799 A1 FR 2398799A1
- Authority
- FR
- France
- Prior art keywords
- alpha
- acids
- solvent
- soln
- alkali
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000002253 acid Substances 0.000 title abstract 6
- 239000003513 alkali Substances 0.000 title abstract 4
- 235000013405 beer Nutrition 0.000 title abstract 3
- 229940106579 hops extract Drugs 0.000 title abstract 3
- 239000001906 humulus lupulus l. absolute Substances 0.000 title abstract 3
- 238000000605 extraction Methods 0.000 title 1
- 239000002904 solvent Substances 0.000 abstract 5
- -1 alkali metal salts Chemical class 0.000 abstract 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 4
- 229910052783 alkali metal Inorganic materials 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- 235000008694 Humulus lupulus Nutrition 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 238000000638 solvent extraction Methods 0.000 abstract 1
- 238000005406 washing Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12C—BEER; PREPARATION OF BEER BY FERMENTATION; PREPARATION OF MALT FOR MAKING BEER; PREPARATION OF HOPS FOR MAKING BEER
- C12C3/00—Treatment of hops
- C12C3/04—Conserving; Storing; Packing
- C12C3/08—Solvent extracts from hops
- C12C3/10—Solvent extracts from hops using carbon dioxide
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Health & Medical Sciences (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Food Science & Technology (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The hops extract contg. alpha-acids or a soln. of these in a non-water miscible solvent is contacted with an essentially non-aqs. alkali to form resinous alkali metal salts of alpha-acids, or a non-aq. soln. of these. The salts are heated to form iso alpha-acid salts which are recovered by partitioning between a substantially non-polar water-immiscible solvent and water at pH 8.2-9.5. In a specified process is above, a solvent soln. of hops extract is used with alkali not exceeding 140% of the stoichiometric amt. based on the alpha-acids, pref. 105-140%. For prepn. of a bittering agent for beer, hops is extracted with a volatile solvent, the solvent is evaporated from the extract, followed by treatment of the extract as above and sepn. of the aq. soln. of iso alpha-acid salts. In the aq. extn., the amt. of water used is a specific variation is sufficient to dissolve the iso-alpha-acid salts, but insufficient to convert a substantial amt. of beta-acids into their alkali metal salts. Used in making beer. Process enables prepn. of a prod. free of undesirable beta-acids. The use of anhydrous alkali enables lower working volumes giving improved productivity with a simple, fast and complete sepn. by final water washing.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US81923277A | 1977-07-26 | 1977-07-26 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| FR2398799A1 true FR2398799A1 (en) | 1979-02-23 |
Family
ID=25227558
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FR7822184A Pending FR2398799A1 (en) | 1977-07-26 | 1978-07-26 | Isomerising hops extract to form iso-alpha-acids for beer - using non aq. alkali followed by aq. extraction |
Country Status (6)
| Country | Link |
|---|---|
| BE (1) | BE869277A (en) |
| DK (1) | DK333078A (en) |
| ES (1) | ES472129A1 (en) |
| FR (1) | FR2398799A1 (en) |
| IT (1) | IT7826121A0 (en) |
| NL (1) | NL7807919A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2429255A1 (en) * | 1978-06-20 | 1980-01-18 | Mueller Adam | PROCESS FOR TREATING HOPS WITH CARBON DIOXIDE AS AN EXTRACTION AGENT |
| EP0199101A1 (en) * | 1985-04-12 | 1986-10-29 | Hopstabil Hopfenverarbeitungs-Gesellschaft mbH | Process for the preparation of isohumulones and their use |
| US5702737A (en) * | 1994-09-13 | 1997-12-30 | Kalamazoo Holdings, Inc. | Preparation of a readily-dispersible hop extract for imparting hoppy aroma and flavor to beer using a lipase |
| US5750179A (en) * | 1994-09-13 | 1998-05-12 | Kalamazoo Holdings, Inc. | Process for producing a water-soluble lipidic hop extract |
| WO2024054738A1 (en) * | 2022-09-08 | 2024-03-14 | Young Living Essential Oils, Lc | Methods and systems for extracting additional beneficial lipid-soluble compounds from plant materials in environmentally sustainable ways |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2174815A1 (en) * | 1972-03-15 | 1973-10-19 | Bush Boake Allen Ltd | Isomerised hop extracts - prepn by contacting a soln of hop extracts contg alpha-acids beta-acids and hop oils with a base |
| GB1423129A (en) * | 1971-08-04 | 1976-01-28 | Bush Boake Allen Ltd | Isomerised hop extracts |
| FR2359894A1 (en) * | 1976-07-29 | 1978-02-24 | Albright & Wilson | PROCESS FOR THE ISOMERIZATION OF ALPHA-ACIDS CONTAINED IN A HOP EXTRACT |
| FR2359895A1 (en) * | 1976-07-29 | 1978-02-24 | Albright & Wilson | PROCESS FOR OBTAINING AN ISOMERIZED HOP EXTRACT |
-
1978
- 1978-07-26 BE BE189508A patent/BE869277A/en unknown
- 1978-07-26 NL NL7807919A patent/NL7807919A/en not_active Application Discontinuation
- 1978-07-26 FR FR7822184A patent/FR2398799A1/en active Pending
- 1978-07-26 IT IT7826121A patent/IT7826121A0/en unknown
- 1978-07-26 DK DK333078A patent/DK333078A/en unknown
- 1978-07-26 ES ES472129A patent/ES472129A1/en not_active Expired
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1423129A (en) * | 1971-08-04 | 1976-01-28 | Bush Boake Allen Ltd | Isomerised hop extracts |
| FR2174815A1 (en) * | 1972-03-15 | 1973-10-19 | Bush Boake Allen Ltd | Isomerised hop extracts - prepn by contacting a soln of hop extracts contg alpha-acids beta-acids and hop oils with a base |
| FR2359894A1 (en) * | 1976-07-29 | 1978-02-24 | Albright & Wilson | PROCESS FOR THE ISOMERIZATION OF ALPHA-ACIDS CONTAINED IN A HOP EXTRACT |
| FR2359895A1 (en) * | 1976-07-29 | 1978-02-24 | Albright & Wilson | PROCESS FOR OBTAINING AN ISOMERIZED HOP EXTRACT |
Non-Patent Citations (2)
| Title |
|---|
| EXBK/57 * |
| EXBK/77 * |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2429255A1 (en) * | 1978-06-20 | 1980-01-18 | Mueller Adam | PROCESS FOR TREATING HOPS WITH CARBON DIOXIDE AS AN EXTRACTION AGENT |
| US4338348A (en) | 1978-06-20 | 1982-07-06 | Mueller Adam | Isomerization of alpha acids |
| WO1983000701A1 (en) * | 1978-06-20 | 1983-03-03 | Müller, Adam | Method for the treatment of hop with co2 as an extraction means and treatment of such extract |
| EP0199101A1 (en) * | 1985-04-12 | 1986-10-29 | Hopstabil Hopfenverarbeitungs-Gesellschaft mbH | Process for the preparation of isohumulones and their use |
| US5702737A (en) * | 1994-09-13 | 1997-12-30 | Kalamazoo Holdings, Inc. | Preparation of a readily-dispersible hop extract for imparting hoppy aroma and flavor to beer using a lipase |
| US5750179A (en) * | 1994-09-13 | 1998-05-12 | Kalamazoo Holdings, Inc. | Process for producing a water-soluble lipidic hop extract |
| AU697032B2 (en) * | 1994-09-13 | 1998-09-24 | Kalamazoo Holdings, Inc. | A solubilized hop extract for imparting hoppy aroma and flavor to beer |
| WO2024054738A1 (en) * | 2022-09-08 | 2024-03-14 | Young Living Essential Oils, Lc | Methods and systems for extracting additional beneficial lipid-soluble compounds from plant materials in environmentally sustainable ways |
Also Published As
| Publication number | Publication date |
|---|---|
| BE869277A (en) | 1979-01-26 |
| NL7807919A (en) | 1979-01-30 |
| DK333078A (en) | 1979-01-27 |
| IT7826121A0 (en) | 1978-07-26 |
| ES472129A1 (en) | 1979-10-01 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| TP | Transmission of property |