FR2377827A1 - METHOD AND APPARATUS FOR THE CHROMATOGRAPHIC SEPARATION OF FRUCTOSE / DEXTROSE SOLUTIONS - Google Patents

METHOD AND APPARATUS FOR THE CHROMATOGRAPHIC SEPARATION OF FRUCTOSE / DEXTROSE SOLUTIONS

Info

Publication number
FR2377827A1
FR2377827A1 FR7801647A FR7801647A FR2377827A1 FR 2377827 A1 FR2377827 A1 FR 2377827A1 FR 7801647 A FR7801647 A FR 7801647A FR 7801647 A FR7801647 A FR 7801647A FR 2377827 A1 FR2377827 A1 FR 2377827A1
Authority
FR
France
Prior art keywords
adsorbent
fructose
excess
chamber
chromatographic separation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR7801647A
Other languages
French (fr)
Other versions
FR2377827B1 (en
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Primary Products Ingredients Americas LLC
Original Assignee
Tate and Lyle Ingredients Americas LLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Tate and Lyle Ingredients Americas LLC filed Critical Tate and Lyle Ingredients Americas LLC
Publication of FR2377827A1 publication Critical patent/FR2377827A1/en
Application granted granted Critical
Publication of FR2377827B1 publication Critical patent/FR2377827B1/fr
Granted legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
    • C13K3/00—Invert sugar; Separation of glucose or fructose from invert sugar
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
    • B01D15/1864—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns using two or more columns
    • B01D15/1871—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns using two or more columns placed in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/20—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to the conditioning of the sorbent material
    • B01D15/206—Packing or coating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/36—Selective adsorption, e.g. chromatography characterised by the separation mechanism involving ionic interaction
    • B01D15/361—Ion-exchange

Landscapes

  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • Organic Chemistry (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
  • Saccharide Compounds (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)

Abstract

La présente invention concerne un procédé permettant d'entasser de l'adsorbant de façon dense dans une colonne de séparation comportant une chambre d'au moins 1,8 m de largeur. Ce procédé comprend les étapes suivantes : a. mélanger l'adsorbant à un excès d'un réactif concentré qui cause une concentration de d'adsorbant en sa présence, l'adsorbant étant capable de gonfler lorsqu'on élimine l'excès de réactif concentré; b. disposer l'adsorbant, à son état de volume réduit, dans la colonne de séparation; c. confiner efficacement l'adsorbant dans la chambre de la colonne de séparation et; d. ensuite éliminer de l'adsorbant confiné l'excès du réactif concentré de sorte que l'adsorbant est amené à gonfler et à se tasser complètement et uniformément dans toute la chambre de la colonne. Application à la séparation fructose/dextrose.The present invention relates to a process for densely packing adsorbent in a separation column having a chamber at least 1.8 m wide. This process comprises the following steps: a. mixing the adsorbent with an excess of a concentrated reagent which causes a concentration of adsorbent in its presence, the adsorbent being capable of swelling when the excess of concentrated reagent is removed; b. disposing the adsorbent, in its reduced volume state, in the separation column; vs. effectively confining the adsorbent to the chamber of the separation column and; d. then removing from the confined adsorbent the excess of the concentrated reagent so that the adsorbent is caused to swell and settle completely and evenly throughout the column chamber. Application to the fructose / dextrose separation.

FR7801647A 1977-01-24 1978-01-20 METHOD AND APPARATUS FOR THE CHROMATOGRAPHIC SEPARATION OF FRUCTOSE / DEXTROSE SOLUTIONS Granted FR2377827A1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US76207277A 1977-01-24 1977-01-24

Publications (2)

Publication Number Publication Date
FR2377827A1 true FR2377827A1 (en) 1978-08-18
FR2377827B1 FR2377827B1 (en) 1984-08-24

Family

ID=25064028

Family Applications (1)

Application Number Title Priority Date Filing Date
FR7801647A Granted FR2377827A1 (en) 1977-01-24 1978-01-20 METHOD AND APPARATUS FOR THE CHROMATOGRAPHIC SEPARATION OF FRUCTOSE / DEXTROSE SOLUTIONS

Country Status (14)

Country Link
JP (1) JPS53114779A (en)
AR (1) AR220529A1 (en)
AU (1) AU516437B2 (en)
BE (1) BE863269A (en)
CA (1) CA1119102A (en)
DE (1) DE2802711A1 (en)
FI (1) FI65086C (en)
FR (1) FR2377827A1 (en)
GB (1) GB1548543A (en)
IN (1) IN147581B (en)
IT (1) IT1102806B (en)
MX (1) MX6742E (en)
NL (1) NL7800772A (en)
NZ (1) NZ186255A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0010769A2 (en) * 1978-11-02 1980-05-14 Mitsubishi Kasei Corporation Adsorption separation method and apparatus therefor
FR2543017A1 (en) * 1983-03-21 1984-09-28 Rhone Poulenc Spec Chim Injection and draining head for packed columns
EP3560570A1 (en) * 2018-04-23 2019-10-30 Novasep Process Method for chromatographic purification of viscous feedstocks

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS59199765A (en) * 1983-04-27 1984-11-12 Canon Inc Dye purification equipment
JPS59199769A (en) * 1983-04-27 1984-11-12 Canon Inc Dye purification equipment
JPS609753A (en) * 1983-06-30 1985-01-18 Canon Inc Ink manufacturing device
WO2011078772A1 (en) * 2009-12-22 2011-06-30 Ge Healthcare Bio-Sciences Ab Method for dry packing chromatography columns
KR20160048847A (en) * 2013-09-05 2016-05-04 다우 글로벌 테크놀로지스 엘엘씨 Chromatographic separation of sugars using blend of cation exchange resins

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1420827A (en) * 1965-01-07 1965-12-10 Colonial Sugar Refining Co Process and apparatus for the separation of fructose and glucose from syrups containing these substances
FR1488694A (en) * 1965-08-05 1967-07-13 Boehringer & Soehne Gmbh Process for obtaining pure fructose and glucose from sucrose or invert sugars containing sucrose
FR2056628A5 (en) * 1969-08-13 1971-05-14 Suomen Sokeri Oy
US3928193A (en) * 1975-02-14 1975-12-23 Suomen Sokeri Oy Process for large scale chromatography

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3044904A (en) * 1960-02-15 1962-07-17 Central Aguirre Sugar Company Separation of dextrose and levulose
FR2219797B1 (en) * 1973-03-01 1978-03-03 Roussel Uclaf
JPS5217089A (en) * 1975-07-30 1977-02-08 Hitachi Ltd Process for production of separation columns for liquid chromatographi es

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1420827A (en) * 1965-01-07 1965-12-10 Colonial Sugar Refining Co Process and apparatus for the separation of fructose and glucose from syrups containing these substances
FR1488694A (en) * 1965-08-05 1967-07-13 Boehringer & Soehne Gmbh Process for obtaining pure fructose and glucose from sucrose or invert sugars containing sucrose
US3483031A (en) * 1965-08-05 1969-12-09 Boehringer & Soehne Gmbh Method of recovering pure glucose and fructose from sucrose or from sucrose-containing invert sugars
FR2056628A5 (en) * 1969-08-13 1971-05-14 Suomen Sokeri Oy
US3928193A (en) * 1975-02-14 1975-12-23 Suomen Sokeri Oy Process for large scale chromatography
FR2300598A1 (en) * 1975-02-14 1976-09-10 Suomen Sokeri Oy INDUSTRIAL CHROMATOGRAPHY PROCESS

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0010769A2 (en) * 1978-11-02 1980-05-14 Mitsubishi Kasei Corporation Adsorption separation method and apparatus therefor
EP0010769A3 (en) * 1978-11-02 1980-05-28 Mitsubishi Chemical Industries Limited Adsorption separation method and apparatus therefor
FR2543017A1 (en) * 1983-03-21 1984-09-28 Rhone Poulenc Spec Chim Injection and draining head for packed columns
EP3560570A1 (en) * 2018-04-23 2019-10-30 Novasep Process Method for chromatographic purification of viscous feedstocks
WO2019206842A1 (en) * 2018-04-23 2019-10-31 Novasep Process Method for chromatographic purification of viscous loads
US11987853B2 (en) 2018-04-23 2024-05-21 Novasep Process Solutions Method for chromatographic purification of viscous loads

Also Published As

Publication number Publication date
IT7847715A0 (en) 1978-01-20
BE863269A (en) 1978-07-24
NL7800772A (en) 1978-07-26
DE2802711A1 (en) 1978-07-27
CA1119102A (en) 1982-03-02
FR2377827B1 (en) 1984-08-24
MX6742E (en) 1986-06-18
FI780194A (en) 1978-07-25
JPS53114779A (en) 1978-10-06
GB1548543A (en) 1979-07-18
FI65086C (en) 1984-03-12
NZ186255A (en) 1980-02-21
IT1102806B (en) 1985-10-07
AR220529A1 (en) 1980-11-14
FI65086B (en) 1983-11-30
AU3269078A (en) 1979-08-02
IN147581B (en) 1980-04-26
AU516437B2 (en) 1981-06-04

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