ES8404512A1 - Procedimiento para la determinacion de agua con ayuda de un reactivo de karl-ficher, exento de piridina. - Google Patents
Procedimiento para la determinacion de agua con ayuda de un reactivo de karl-ficher, exento de piridina.Info
- Publication number
- ES8404512A1 ES8404512A1 ES519710A ES519710A ES8404512A1 ES 8404512 A1 ES8404512 A1 ES 8404512A1 ES 519710 A ES519710 A ES 519710A ES 519710 A ES519710 A ES 519710A ES 8404512 A1 ES8404512 A1 ES 8404512A1
- Authority
- ES
- Spain
- Prior art keywords
- reagent
- determination
- water
- karl fischer
- fischer reagent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N31/00—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods
- G01N31/16—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods using titration
- G01N31/168—Determining water content by using Karl Fischer reagent
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Molecular Biology (AREA)
- Physics & Mathematics (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
- Measuring Or Testing Involving Enzymes Or Micro-Organisms (AREA)
Abstract
METODO DE DETERMINACION DE AGUA UTILIZANDO REACTIVO KARL-FISCHER EXENTO DE PIRIDINA.CONSISTE EN DISOLVER LA MUESTRA A ENSAYAR EN UN DISOLVENTE ADECUADO, QUE CONTIENE UNA SAL Y DIOXIDO DE AZUFRE; AÑADIR EL AGENTE DE VALORACION, QUE CONTIENE UNA SAL DE UNA BASE ORGANICA, TAL COMO UN COMPUESTO NITROGENADO CUYO PKB ES MENOR QUE 10, Y DE UN ACIDO ORGANICO DEBIL, TAL COMO UN ACIDO CARBOXILICO AROMATICO CUYO PKA ES MAYOR QUE 2, DIOXIDO DE AZUFRE Y YODO EN UN DISOLVENTE; Y DETERMINAR EL PUNTO FINAL DE LA VALORACION.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19823204962 DE3204962A1 (de) | 1982-02-12 | 1982-02-12 | Karl-fischer-reagenz und verfahren zur bestimmung von wasser mit hilfe dieses reagenzes |
Publications (2)
Publication Number | Publication Date |
---|---|
ES519710A0 ES519710A0 (es) | 1984-04-16 |
ES8404512A1 true ES8404512A1 (es) | 1984-04-16 |
Family
ID=6155514
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES519710A Expired ES8404512A1 (es) | 1982-02-12 | 1983-02-11 | Procedimiento para la determinacion de agua con ayuda de un reactivo de karl-ficher, exento de piridina. |
Country Status (11)
Country | Link |
---|---|
US (1) | US4550083A (es) |
EP (1) | EP0086994B1 (es) |
JP (1) | JPS58147650A (es) |
AT (1) | ATE24769T1 (es) |
AU (1) | AU559987B2 (es) |
BR (1) | BR8300679A (es) |
CA (1) | CA1203743A (es) |
DD (1) | DD238863A5 (es) |
DE (2) | DE3204962A1 (es) |
ES (1) | ES8404512A1 (es) |
IL (1) | IL67873A0 (es) |
Families Citing this family (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS6039626A (ja) * | 1983-08-11 | 1985-03-01 | Matsushita Electric Ind Co Ltd | エレクトロクロミツク表示装置 |
DE3407014A1 (de) * | 1984-02-27 | 1985-08-29 | Merck Patent Gmbh, 6100 Darmstadt | Karl-fischer-reagenz und verfahren zur bestimmung von wasser mit hilfe dieses reagenzes |
DE3411181A1 (de) * | 1984-03-27 | 1985-10-10 | Merck Patent Gmbh, 6100 Darmstadt | Karl-fischer-reagenz und verfahren zur bestimmung von wasser mit hilfe dieses reagenzes |
JPS60219555A (ja) * | 1984-04-16 | 1985-11-02 | Hikosuke Watanabe | カ−ルフイツシヤ−法による水分測定用の溶媒 |
DE3521544A1 (de) * | 1985-06-15 | 1986-12-18 | Merck Patent Gmbh, 6100 Darmstadt | Loesungsmittel fuer die wasserbestimmung nach karl-fischer |
EP0242998B1 (en) * | 1986-03-22 | 1991-07-03 | SMITH & NEPHEW plc | Disinfecting composition |
DE3904992A1 (de) * | 1989-02-18 | 1990-08-23 | Riedel De Haen Ag | Reagenz fuer die coulometrische wasserbestimmung |
JP2819603B2 (ja) * | 1989-04-21 | 1998-10-30 | キヤノン株式会社 | 撮影画面決定装置 |
DE3943118A1 (de) * | 1989-12-27 | 1991-07-04 | Merck Patent Gmbh | Karl-fischer-reagenz und verfahren zur bestimmung von wasser mit hilfe dieses reagenzes |
DE4102042A1 (de) * | 1991-01-24 | 1992-07-30 | Bayer Ag | Substituierte aminosaeureamid-derivate deren herstellung und verwendung als fungizide |
DE4123976A1 (de) * | 1991-07-19 | 1993-01-21 | Riedel De Haen Ag | Katholyt fuer die coulometrische wasserbestimmung nach karl fischer |
JPH05164830A (ja) * | 1991-12-17 | 1993-06-29 | Teac Corp | 自動追尾装置 |
US5389545A (en) * | 1993-07-26 | 1995-02-14 | Dahms; Harald | Reagents, methods and kits for water determination |
DE4421453A1 (de) * | 1994-06-18 | 1995-12-21 | Riedel De Haen Ag | Karl-Fischer-Reagenz |
EP0933634B1 (de) * | 1998-01-29 | 2006-02-08 | Sigma-Aldrich Laborchemikalien GmbH | Verwendung eines Salzes als Zusatz in Karl-Fischer Reagenzien zur Stabilisierung der Ethanol-Lösungsmittelkomponente |
JP4709200B2 (ja) * | 2007-11-21 | 2011-06-22 | 三菱日立製鉄機械株式会社 | 双ドラム式連続鋳造設備 |
CN109254110A (zh) * | 2018-09-30 | 2019-01-22 | 东莞市杉杉电池材料有限公司 | 一种锂离子电池电解液水分检测用卡尔费休试剂及其制备方法 |
US11714072B2 (en) * | 2019-03-28 | 2023-08-01 | Honeywell International Inc. | Reagent compositions and method for Karl Fischer titration |
Family Cites Families (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
BE519298A (es) * | 1953-04-13 | |||
NL101617C (es) * | 1956-11-09 | |||
ATE7540T1 (de) * | 1979-07-26 | 1984-06-15 | J.T. Baker Chemicals B.V. | Reagenz zur quantitativen bestimmung von wasser und seine verwendung zur quantitativen bestimmung von wasser. |
JPS5664658A (en) * | 1979-10-31 | 1981-06-01 | Mitsubishi Chem Ind Ltd | Karl fisher reagent |
US4378972A (en) * | 1980-03-05 | 1983-04-05 | Riedel-De Haen Aktiengesellschaft | Titration agent and method for using same |
DE3010436A1 (de) * | 1980-03-19 | 1981-09-24 | Merck Patent Gmbh, 6100 Darmstadt | Pyridinfreies karl-fischer-reagenz und verfahren zur bestimmung von wasser mit hilfe dieses reagenzes |
ATE11457T1 (de) * | 1980-09-02 | 1985-02-15 | J.T. Baker Chemicals B.V. | Reagenz fuer die quantitative bestimmung von wasser und seine anwendung hierfuer. |
DE3048237A1 (de) * | 1980-12-20 | 1982-07-15 | Merck Patent Gmbh, 6100 Darmstadt | "pyridinfreies karl-fischer-reagenz und verfahren zur bestimmung von wasser mit hilfe dieses reagenzes" |
EP0056826A1 (en) * | 1981-01-22 | 1982-08-04 | J.T. Baker Chemicals B.V. | Reagent for quantitative determination of water and its use therefor |
-
1982
- 1982-02-12 DE DE19823204962 patent/DE3204962A1/de not_active Withdrawn
-
1983
- 1983-01-29 EP EP83100843A patent/EP0086994B1/de not_active Expired
- 1983-01-29 AT AT83100843T patent/ATE24769T1/de not_active IP Right Cessation
- 1983-01-29 DE DE8383100843T patent/DE3368997D1/de not_active Expired
- 1983-02-01 AU AU10877/83A patent/AU559987B2/en not_active Ceased
- 1983-02-08 CA CA000421097A patent/CA1203743A/en not_active Expired
- 1983-02-09 IL IL67873A patent/IL67873A0/xx not_active IP Right Cessation
- 1983-02-10 BR BR8300679A patent/BR8300679A/pt not_active IP Right Cessation
- 1983-02-10 JP JP58019872A patent/JPS58147650A/ja active Granted
- 1983-02-10 DD DD83247860A patent/DD238863A5/de unknown
- 1983-02-11 ES ES519710A patent/ES8404512A1/es not_active Expired
- 1983-02-16 US US06/466,187 patent/US4550083A/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
DE3368997D1 (en) | 1987-02-12 |
IL67873A0 (en) | 1983-06-15 |
EP0086994B1 (de) | 1987-01-07 |
JPH0513265B2 (es) | 1993-02-22 |
BR8300679A (pt) | 1983-11-08 |
DD238863A5 (de) | 1986-09-03 |
ES519710A0 (es) | 1984-04-16 |
ATE24769T1 (de) | 1987-01-15 |
AU559987B2 (en) | 1987-03-26 |
EP0086994A1 (de) | 1983-08-31 |
DE3204962A1 (de) | 1983-08-25 |
JPS58147650A (ja) | 1983-09-02 |
US4550083A (en) | 1985-10-29 |
AU1087783A (en) | 1983-08-18 |
CA1203743A (en) | 1986-04-29 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
FD1A | Patent lapsed |
Effective date: 19970401 |