ES8206482A1 - Procedimiento para la obtencion de amida de acido nicotinicopura a partir de amida de acido nicotinico bruta - Google Patents
Procedimiento para la obtencion de amida de acido nicotinicopura a partir de amida de acido nicotinico brutaInfo
- Publication number
- ES8206482A1 ES8206482A1 ES504207A ES504207A ES8206482A1 ES 8206482 A1 ES8206482 A1 ES 8206482A1 ES 504207 A ES504207 A ES 504207A ES 504207 A ES504207 A ES 504207A ES 8206482 A1 ES8206482 A1 ES 8206482A1
- Authority
- ES
- Spain
- Prior art keywords
- purification
- nicotin amide
- nicotinic acid
- nicotin
- amide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/78—Carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, e.g. ester or nitrile radicals
- C07D213/81—Amides; Imides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pyridine Compounds (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
PROCEDIMIENTO PARA LA OBTENCION DE AMIDA DE ACIDO NICOTINICO PURA A PARTIR DE AMIDA DE ACIDO NICOTINICO BRUTA. LA AMIDA DE ACIDO NICOTINICO BRUTA SE RECRISTALIZA EN UN ALCANOL, USANDOSE COMO DISOLVENTE 2-MWETILPROPANOL (1) CON HASTA 10-18 POR 100 EN PESO DE AGUA, DISOLVIENDOSE LA AMIDA EN EL A UNA TEMPERATURA COMPRENDIDA ENTRE 65 Y 85 C. POSTERIORMENTE LA SOLUCION CALIENTE SE TRATA CON INTERCAMBIADORES DE IONES, DEPENDIENDO CUALES SEAN ESTOS DEL TIPO DE IMPUREZAS DE LA AMIDA. TRAS ESTO LA SOLUCION SE ENFRIA Y LA AMIDA DE ACIDO NICOTINICO PURA SE SEPARA, PUDIENDOSE EMPLEAR LAS AGUAS MADRES PARA UNA CARGA ULTERIOR.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19803028791 DE3028791A1 (de) | 1980-07-30 | 1980-07-30 | Verfahren zur reinigung von nicotinsaeureamid ii. |
Publications (2)
Publication Number | Publication Date |
---|---|
ES504207A0 ES504207A0 (es) | 1982-08-16 |
ES8206482A1 true ES8206482A1 (es) | 1982-08-16 |
Family
ID=6108402
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES504207A Expired ES8206482A1 (es) | 1980-07-30 | 1981-07-23 | Procedimiento para la obtencion de amida de acido nicotinicopura a partir de amida de acido nicotinico bruta |
Country Status (9)
Country | Link |
---|---|
US (1) | US4447614A (es) |
EP (1) | EP0045080B1 (es) |
JP (1) | JPS5754173A (es) |
BR (1) | BR8104892A (es) |
CA (1) | CA1136147A (es) |
DE (2) | DE3028791A1 (es) |
ES (1) | ES8206482A1 (es) |
IN (1) | IN154600B (es) |
MX (1) | MX6429E (es) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0424316A3 (en) * | 1989-10-19 | 1991-09-25 | Ciba-Geigy Ag | Purification of 2-aryl-2h-benzotriazoles |
TW539670B (en) * | 1998-07-21 | 2003-07-01 | Reilly Ind Inc | Processes for producing highly pure nicotinamide |
CN114634269B (zh) * | 2020-12-15 | 2022-12-02 | 山东潍坊润丰化工股份有限公司 | 一种从废水中回收烟酰胺的方法 |
Family Cites Families (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2471518A (en) * | 1949-05-31 | Nicotinic acid amide and processes | ||
US2483250A (en) * | 1949-09-27 | Tt a it tt | ||
US2412749A (en) * | 1942-03-02 | 1946-12-17 | Gelatin Products Corp | Method of preparing nicotinamide |
US2544157A (en) * | 1947-05-08 | 1951-03-06 | Upjohn Co | Purification of nicotinamide |
DE828247C (de) * | 1948-10-02 | 1953-07-02 | Degussa | Verfahren zur Herstellung von Nicotinsaeureamid |
GB879551A (en) * | 1957-10-28 | 1961-10-11 | Merck & Co Inc | Ion-exchange purification of nicotinamide |
US2932648A (en) * | 1958-10-06 | 1960-04-12 | Abbott Lab | Nicotinamide process |
US3678060A (en) * | 1970-08-03 | 1972-07-18 | Merck & Co Inc | Process for separating an acid from an amide |
DE2517053A1 (de) * | 1975-04-17 | 1976-10-28 | Degussa | Verfahren zur gewinnung von nicotinsaeureamid |
DE2517054C2 (de) * | 1975-04-17 | 1985-04-25 | Degussa Ag, 6000 Frankfurt | Verfahren zur Herstellung von Nicotinsäureamid |
-
1980
- 1980-07-30 DE DE19803028791 patent/DE3028791A1/de not_active Withdrawn
-
1981
- 1981-07-20 IN IN814/CAL/81A patent/IN154600B/en unknown
- 1981-07-23 ES ES504207A patent/ES8206482A1/es not_active Expired
- 1981-07-25 EP EP81105903A patent/EP0045080B1/de not_active Expired
- 1981-07-25 DE DE8181105903T patent/DE3166837D1/de not_active Expired
- 1981-07-27 MX MX819569U patent/MX6429E/es unknown
- 1981-07-29 US US06/288,187 patent/US4447614A/en not_active Expired - Fee Related
- 1981-07-29 CA CA000382757A patent/CA1136147A/en not_active Expired
- 1981-07-29 BR BR8104892A patent/BR8104892A/pt unknown
- 1981-07-29 JP JP56117903A patent/JPS5754173A/ja active Pending
Also Published As
Publication number | Publication date |
---|---|
EP0045080B1 (de) | 1984-10-24 |
ES504207A0 (es) | 1982-08-16 |
JPS5754173A (es) | 1982-03-31 |
US4447614A (en) | 1984-05-08 |
IN154600B (es) | 1984-11-17 |
DE3166837D1 (en) | 1984-11-29 |
MX6429E (es) | 1985-05-30 |
EP0045080A1 (de) | 1982-02-03 |
BR8104892A (pt) | 1982-04-13 |
CA1136147A (en) | 1982-11-23 |
DE3028791A1 (de) | 1982-02-25 |
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