ES455423A1 - Process for the production of 1,3-dichloroacetone oxime and its acetate derivatives - Google Patents
Process for the production of 1,3-dichloroacetone oxime and its acetate derivativesInfo
- Publication number
- ES455423A1 ES455423A1 ES455423A ES455423A ES455423A1 ES 455423 A1 ES455423 A1 ES 455423A1 ES 455423 A ES455423 A ES 455423A ES 455423 A ES455423 A ES 455423A ES 455423 A1 ES455423 A1 ES 455423A1
- Authority
- ES
- Spain
- Prior art keywords
- production
- dichloroacetone oxime
- dichloroacetone
- oxime
- acetate derivatives
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- YWXYBQXZYIIPSM-UHFFFAOYSA-N n-(1,3-dichloropropan-2-ylidene)hydroxylamine Chemical compound ON=C(CCl)CCl YWXYBQXZYIIPSM-UHFFFAOYSA-N 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 2
- 150000001242 acetic acid derivatives Chemical class 0.000 title 1
- WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical compound CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 abstract 3
- SUNMBRGCANLOEG-UHFFFAOYSA-N 1,3-dichloroacetone Chemical compound ClCC(=O)CCl SUNMBRGCANLOEG-UHFFFAOYSA-N 0.000 abstract 2
- MQRDNTHUNXTMLF-UHFFFAOYSA-N acetic acid;n-(1,3-dichloropropan-2-ylidene)hydroxylamine Chemical compound CC(O)=O.ON=C(CCl)CCl MQRDNTHUNXTMLF-UHFFFAOYSA-N 0.000 abstract 1
- 230000000844 anti-bacterial effect Effects 0.000 abstract 1
- 239000003899 bactericide agent Substances 0.000 abstract 1
- 239000000417 fungicide Substances 0.000 abstract 1
- 150000002443 hydroxylamines Chemical class 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
- A01N33/16—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds containing nitrogen-to-oxygen bonds
- A01N33/24—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds containing nitrogen-to-oxygen bonds only one oxygen atom attached to the nitrogen atom
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
- C07C249/08—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes by reaction of hydroxylamines with carbonyl compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C251/00—Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C251/32—Oximes
- C07C251/34—Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
- C07C251/36—Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with the carbon atoms of the oxyimino groups bound to hydrogen atoms or to acyclic carbon atoms
- C07C251/38—Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with the carbon atoms of the oxyimino groups bound to hydrogen atoms or to acyclic carbon atoms to carbon atoms of a saturated carbon skeleton
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C251/00—Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C251/32—Oximes
- C07C251/34—Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
- C07C251/44—Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with the carbon atom of at least one of the oxyimino groups being part of a ring other than a six-membered aromatic ring
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C251/00—Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C251/32—Oximes
- C07C251/62—Oximes having oxygen atoms of oxyimino groups esterified
- C07C251/64—Oximes having oxygen atoms of oxyimino groups esterified by carboxylic acids
- C07C251/66—Oximes having oxygen atoms of oxyimino groups esterified by carboxylic acids with the esterifying carboxyl groups bound to hydrogen atoms, to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
- C07C2601/14—The ring being saturated
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
1,3-Dichloroacetone oxime is prepared by reacting 1,3-dichloropropanone with a hydroxylamine salt. The pH of the reaction system is brought to a value of </= 2, which is maintained during the reaction. 1,3-Dichloroacetone oxime acetate is prepared by the above process, the resulting product being reacted with acetic anhydride. 1,3-Dichloroacetone oxime can be used as intermediate for the preparation of fungicides and bactericides.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US65379776A | 1976-01-30 | 1976-01-30 | |
US05/751,491 US4128580A (en) | 1976-01-30 | 1976-12-21 | Process for the production of 1,3-dichloroacetone oxime and its acetate derivative |
Publications (1)
Publication Number | Publication Date |
---|---|
ES455423A1 true ES455423A1 (en) | 1978-05-01 |
Family
ID=27096594
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES455423A Expired ES455423A1 (en) | 1976-01-30 | 1977-01-28 | Process for the production of 1,3-dichloroacetone oxime and its acetate derivatives |
Country Status (17)
Country | Link |
---|---|
JP (1) | JPS52113910A (en) |
AT (1) | AT354411B (en) |
AU (1) | AU505546B2 (en) |
CA (1) | CA1102817A (en) |
CH (1) | CH623302A5 (en) |
DD (1) | DD130783A5 (en) |
DE (1) | DE2703370A1 (en) |
DK (1) | DK32677A (en) |
ES (1) | ES455423A1 (en) |
FI (1) | FI770196A (en) |
FR (1) | FR2339592A1 (en) |
GB (1) | GB1525682A (en) |
IL (1) | IL51353A (en) |
IT (1) | IT1079462B (en) |
NL (1) | NL7700914A (en) |
NO (1) | NO143941C (en) |
SE (1) | SE7700863L (en) |
-
1977
- 1977-01-21 FI FI770196A patent/FI770196A/fi not_active Application Discontinuation
- 1977-01-24 JP JP597677A patent/JPS52113910A/en active Pending
- 1977-01-25 AT AT43377A patent/AT354411B/en not_active IP Right Cessation
- 1977-01-26 CH CH94377A patent/CH623302A5/en not_active IP Right Cessation
- 1977-01-26 FR FR7702113A patent/FR2339592A1/en active Granted
- 1977-01-26 CA CA270,498A patent/CA1102817A/en not_active Expired
- 1977-01-26 DK DK32677A patent/DK32677A/en not_active Application Discontinuation
- 1977-01-27 DE DE19772703370 patent/DE2703370A1/en not_active Withdrawn
- 1977-01-27 SE SE7700863A patent/SE7700863L/en unknown
- 1977-01-27 GB GB3341/77A patent/GB1525682A/en not_active Expired
- 1977-01-28 AU AU21761/77A patent/AU505546B2/en not_active Expired
- 1977-01-28 DD DD7700197144A patent/DD130783A5/en unknown
- 1977-01-28 NL NL7700914A patent/NL7700914A/en not_active Application Discontinuation
- 1977-01-28 IL IL51353A patent/IL51353A/en unknown
- 1977-01-28 NO NO770280A patent/NO143941C/en unknown
- 1977-01-28 ES ES455423A patent/ES455423A1/en not_active Expired
- 1977-01-28 IT IT47838/77A patent/IT1079462B/en active
Also Published As
Publication number | Publication date |
---|---|
AU505546B2 (en) | 1979-11-22 |
AU2176177A (en) | 1978-08-03 |
AT354411B (en) | 1979-01-10 |
FR2339592A1 (en) | 1977-08-26 |
IL51353A (en) | 1980-06-30 |
NO770280L (en) | 1977-08-02 |
FI770196A (en) | 1977-07-31 |
GB1525682A (en) | 1978-09-20 |
NO143941C (en) | 1981-05-13 |
SE7700863L (en) | 1977-07-31 |
JPS52113910A (en) | 1977-09-24 |
ATA43377A (en) | 1979-06-15 |
NO143941B (en) | 1981-02-02 |
CH623302A5 (en) | 1981-05-29 |
CA1102817A (en) | 1981-06-09 |
DK32677A (en) | 1977-07-31 |
IL51353A0 (en) | 1977-03-31 |
FR2339592B1 (en) | 1980-08-29 |
NL7700914A (en) | 1977-08-02 |
DD130783A5 (en) | 1978-05-03 |
IT1079462B (en) | 1985-05-13 |
DE2703370A1 (en) | 1977-08-04 |
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