ES339439A1 - Process for producing beta-Methylmercaptopropionaldehyde - Google Patents
Process for producing beta-MethylmercaptopropionaldehydeInfo
- Publication number
- ES339439A1 ES339439A1 ES339439A ES339439A ES339439A1 ES 339439 A1 ES339439 A1 ES 339439A1 ES 339439 A ES339439 A ES 339439A ES 339439 A ES339439 A ES 339439A ES 339439 A1 ES339439 A1 ES 339439A1
- Authority
- ES
- Spain
- Prior art keywords
- methylmercaptopropionaldehyde
- less
- producing beta
- acrolein
- condensing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C323/00—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
A process for the production of #-methylmercaptopropionaldehyde comprises (1) reacting methyl mercaptan with acrolein in a molar ratio of 1 : 1À001-1 1À20 and in the presence of a catalyst, (2) removing from the product of step (1) impurities having a lower boiling point than #-methylmercaptopropionaldehyde by rectification under a pressure of less than 200 mm. Hg. with a retention time of less than 60 minutes, while keeping the temperature of the #-methylmercaptopropionaldehyde below 125 degrees and (3) condensing the vapour distilled in step (2) by contacting it with a previously condensed and cooled distillate from step (2).
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2486866 | 1966-04-18 |
Publications (1)
Publication Number | Publication Date |
---|---|
ES339439A1 true ES339439A1 (en) | 1968-05-01 |
Family
ID=12150171
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES339439A Expired ES339439A1 (en) | 1966-04-18 | 1967-04-18 | Process for producing beta-Methylmercaptopropionaldehyde |
Country Status (5)
Country | Link |
---|---|
BE (1) | BE697178A (en) |
DE (1) | DE1618879B1 (en) |
ES (1) | ES339439A1 (en) |
GB (1) | GB1173174A (en) |
NL (1) | NL6705426A (en) |
Families Citing this family (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5637766A (en) * | 1993-06-08 | 1997-06-10 | Novus International, Inc. | Process for the preparation of 3-(methylthio) propanal |
US5925794A (en) * | 1993-06-08 | 1999-07-20 | Novus International, Inc. | Process for the preparation of 3-(methylthio)propanal |
US5352837A (en) * | 1993-06-08 | 1994-10-04 | Novus International, Inc. | Process for the preparation of 3-(methylthio)propanal |
US5905171A (en) | 1995-06-22 | 1999-05-18 | Novus International, Inc. | Process for the preparation of 3-(methylthio)propanal |
US5663409A (en) * | 1995-06-07 | 1997-09-02 | Novus International, Inc. | Process for the preparation of 3-(methylthio) propanal and 2-hydroxy-4-(methylthio) butanenitrile |
DE102010064250A1 (en) * | 2010-12-28 | 2012-06-28 | Evonik Degussa Gmbh | Process for the preparation of methylmercaptopropionaldehyde |
EP3205643A1 (en) * | 2016-02-15 | 2017-08-16 | Evonik Degussa GmbH | Method for the preparation of 3-methylthiopropionaldehyde |
EP3339290B1 (en) * | 2016-12-22 | 2019-06-19 | Evonik Degussa GmbH | Storage of 3-methylthiopropionaldehyde and methyl mercaptan |
EP3656760A1 (en) | 2018-11-21 | 2020-05-27 | Evonik Operations GmbH | Storage stable form of 3-methylthiopropionaldehyde |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CH253951A (en) * | 1945-10-25 | 1948-04-15 | Merck & Co Inc | Process for the preparation of B-methylmercapto-propionaldehyde. |
GB687483A (en) * | 1949-07-04 | 1953-02-18 | Dow Chemical Co | Improved method for the production of beta-methylmercapto-propionaldehyde |
US2676190A (en) * | 1951-10-23 | 1954-04-20 | Du Pont | Process for the manufacture of beta-methylmercapto-propionaldehyde |
US2776996A (en) * | 1955-12-22 | 1957-01-08 | Du Pont | Manufacture of beta-methylmercaptopropionaldehyde |
-
1967
- 1967-04-18 GB GB1782367A patent/GB1173174A/en not_active Expired
- 1967-04-18 BE BE697178D patent/BE697178A/xx unknown
- 1967-04-18 DE DE1967S0109387 patent/DE1618879B1/en not_active Ceased
- 1967-04-18 NL NL6705426A patent/NL6705426A/xx unknown
- 1967-04-18 ES ES339439A patent/ES339439A1/en not_active Expired
Also Published As
Publication number | Publication date |
---|---|
GB1173174A (en) | 1969-12-03 |
BE697178A (en) | 1967-10-02 |
NL6705426A (en) | 1967-10-19 |
DE1618879B1 (en) | 1971-12-16 |
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