ES2199069B1 - Procedimiento para la extraccion de compuestos fenolicos a partir de un material vegetal residual mediante un tratamiento hidrotermico. - Google Patents

Procedimiento para la extraccion de compuestos fenolicos a partir de un material vegetal residual mediante un tratamiento hidrotermico.

Info

Publication number
ES2199069B1
ES2199069B1 ES200201671A ES200201671A ES2199069B1 ES 2199069 B1 ES2199069 B1 ES 2199069B1 ES 200201671 A ES200201671 A ES 200201671A ES 200201671 A ES200201671 A ES 200201671A ES 2199069 B1 ES2199069 B1 ES 2199069B1
Authority
ES
Spain
Prior art keywords
extraction
procedure
phenolic compounds
reactor
vegetable material
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
ES200201671A
Other languages
English (en)
Other versions
ES2199069A1 (es
Inventor
Mercedes Ballesteros Perdices
Maria Jose Negro Alvarez
Paloma Manzanares Secades
Ignacio Ballesteros Perdices
Jose Miguel Oliva Dominguez
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Centro de Investigaciones Energeticas Medioambientales y Tecnologicas CIEMAT
Original Assignee
Centro de Investigaciones Energeticas Medioambientales y Tecnologicas CIEMAT
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Centro de Investigaciones Energeticas Medioambientales y Tecnologicas CIEMAT filed Critical Centro de Investigaciones Energeticas Medioambientales y Tecnologicas CIEMAT
Priority to ES200201671A priority Critical patent/ES2199069B1/es
Priority to PCT/ES2003/000085 priority patent/WO2004009206A1/es
Priority to AU2003208731A priority patent/AU2003208731A1/en
Priority to US10/801,511 priority patent/US7109384B2/en
Publication of ES2199069A1 publication Critical patent/ES2199069A1/es
Application granted granted Critical
Publication of ES2199069B1 publication Critical patent/ES2199069B1/es
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/02—Solvent extraction of solids
    • B01D11/0215—Solid material in other stationary receptacles
    • B01D11/0253—Fluidised bed of solid materials
    • B01D11/0257—Fluidised bed of solid materials using mixing mechanisms, e.g. stirrers, jets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D12/00—Displacing liquid, e.g. from wet solids or from dispersions of liquids or from solids in liquids, by means of another liquid
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/004—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by obtaining phenols from plant material or from animal material
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
    • C07C37/70—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
    • C07C37/82—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by solid-liquid treatment; by chemisorption
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C39/00—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring
    • C07C39/02—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring monocyclic with no unsaturation outside the aromatic ring
    • C07C39/08—Dihydroxy benzenes; Alkylated derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C39/00—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring
    • C07C39/02—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring monocyclic with no unsaturation outside the aromatic ring
    • C07C39/10—Polyhydroxy benzenes; Alkylated derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C39/00—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring
    • C07C39/02—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring monocyclic with no unsaturation outside the aromatic ring
    • C07C39/11—Alkylated hydroxy benzenes containing also acyclically bound hydroxy groups, e.g. saligenol

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Botany (AREA)
  • Dispersion Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Fats And Perfumes (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Compounds Of Unknown Constitution (AREA)

Abstract

Procedimiento de extracción de compuestos fenólicos a partir de un material vegetal residual mediante un tratamiento hidrotérmico . El tratamiento hidrotérmico se basa en poner en contacto el material vegetal residual bruto con agua caliente en un reactor cerrado comprendiendo las siguientes etapas: a) poner en contacto, en un reactor, el material a tratar con agua y ajustar la relación sólido/líquido de manera que esté comprendida entre 1/5 y 1/15 (p/v); b) agitar; c) calentar a una temperatura entre 180° y 240°C, y a una presión tal que se mantenga el agua en fase líquida; d) mantener la mezcla en agitación durante un periodo de tiempo comprendiendo entre 4 y 30 min; y e) enfriar el reactor hasta 40°C aproximadamente, descargar la mezcla, filtrar y recuperar la fracción líquida.
ES200201671A 2002-07-17 2002-07-17 Procedimiento para la extraccion de compuestos fenolicos a partir de un material vegetal residual mediante un tratamiento hidrotermico. Expired - Fee Related ES2199069B1 (es)

Priority Applications (4)

Application Number Priority Date Filing Date Title
ES200201671A ES2199069B1 (es) 2002-07-17 2002-07-17 Procedimiento para la extraccion de compuestos fenolicos a partir de un material vegetal residual mediante un tratamiento hidrotermico.
PCT/ES2003/000085 WO2004009206A1 (es) 2002-07-17 2003-02-20 Procedimiento de extracción de compuestos fenólicos a partir de un material vegetal residual mediante un tratamiento hidrotérmico
AU2003208731A AU2003208731A1 (en) 2002-07-17 2003-02-20 Method of extracting phenolic compounds from a residual plant material using a hydrothermal process
US10/801,511 US7109384B2 (en) 2002-07-17 2003-02-20 Process to extract phenolic compounds from a residual plant material using a hydrothermal treatment

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
ES200201671A ES2199069B1 (es) 2002-07-17 2002-07-17 Procedimiento para la extraccion de compuestos fenolicos a partir de un material vegetal residual mediante un tratamiento hidrotermico.

Publications (2)

Publication Number Publication Date
ES2199069A1 ES2199069A1 (es) 2004-02-01
ES2199069B1 true ES2199069B1 (es) 2005-02-01

Family

ID=30470572

Family Applications (1)

Application Number Title Priority Date Filing Date
ES200201671A Expired - Fee Related ES2199069B1 (es) 2002-07-17 2002-07-17 Procedimiento para la extraccion de compuestos fenolicos a partir de un material vegetal residual mediante un tratamiento hidrotermico.

Country Status (4)

Country Link
US (1) US7109384B2 (es)
AU (1) AU2003208731A1 (es)
ES (1) ES2199069B1 (es)
WO (1) WO2004009206A1 (es)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2415136A (en) * 2004-06-17 2005-12-21 Natraceutical Sa Obtaining olive polyphenol concentrate from a by-product of olive oil extraction using membrane separation techniques
ES2283191B1 (es) * 2005-09-02 2008-10-16 Antas Pharma, S.A. Biomasa de pulpa de oliva con alto contenido en antioxidantes fenolicos, procedimiento de obtencion, formulaciones y usos de las mismas.
JP2009510003A (ja) * 2005-09-30 2009-03-12 ディーエスエム アイピー アセッツ ビー．ブイ． ポリフェノールを含有する新規の組成物
WO2008090460A1 (en) 2007-01-26 2008-07-31 Probelte Pharma, S.A. Process and apparatus for the production of hydroxytyrosol containing extract from olives and solids containing residues of olive oil extraction
EP1953133A1 (en) * 2007-01-26 2008-08-06 Probelte Pharma, S.A. Process and apparatus for the production of hydroxytyrosol from olive oil extraction residues
US8968811B2 (en) 2007-01-26 2015-03-03 Probelte Pharma, S.A. Hydroxytrosol containing extract obtained from olives and solids containing residues of olive oil extraction
US8658221B2 (en) * 2007-12-17 2014-02-25 Bayer Cropscience Ag Extraction process for plant ingredients
ES2374675B1 (es) * 2010-08-09 2013-01-04 Consejo Superior De Investigaciones Científicas (Csic) Dispositivo y procedimiento para el tratamiento de los subproductos de la obtención de aceite de oliva.
US8940129B2 (en) 2010-12-30 2015-01-27 Uop Llc Process for reducing one or more insoluble solids in a black liquor
ES2395032B1 (es) * 2011-06-21 2013-12-13 Consejo Superior De Investigaciones Científicas (Csic) Extracto fenólico de los subproductos de la aceituna tratados térmicamente.
CN102701914B (zh) * 2012-06-21 2014-04-23 桂林三宝药业有限公司 从橄榄叶中提取羟基酪醇的方法
CN106316797A (zh) * 2015-06-30 2017-01-11 四川小叶本草生物科技有限公司 一种固定化酶法耦合膜技术制备羟基酪醇的方法
IT201700042090A1 (it) 2017-04-14 2018-10-14 Levius Vita Foods Srl Procedimento per la preparazione di olio d’oliva ad alto contenuto di idrossitirosolo
IT201800005151A1 (it) * 2018-05-08 2019-11-08 Estratto di acque di vegetazione per uso nel trattamento e/o nella prevenzione del cancro prostatico

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ES2145701B1 (es) * 1998-03-30 2001-02-01 Consejo Superior Investigacion Procedimiento de obtencion de hidroxitirosol a partir de hueso de aceituna.
DE60229501D1 (de) * 2001-02-15 2008-12-04 Consejo Superior Investigacion Verfahren zur gewinnung von gereinigtem hydroxytyrosol aus von dem olivenbaum erhaltenen produkten und nebenprodukten

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
ALONSO-SALCES, R.M. et al. Pressurized liquid extraction for the determination of polyphenols in apple. Journal of Chromatography A, 9 de Noviembre de 2001, Vol. 933, páginas 37-43. *
BALLESTEROS, I. et al. Ethanol Production from Olive Oil Extraction Residue Pretreated with Hot Water. Applied Biochemistry and Biotechnology, primavera 2002, Vols. 98-100, páginas 717-732. *
PIRISI, F.M. et al. Phenolic Compounds in Virgin Olive Oil. 2. Reappraisal of the Extraction, HPLC Separation and Quantification Procedures. Journal of Agricultural and Food Chemistry, Abril del 2000, Vol. 48, páginas 1.191-1.196. *

Also Published As

Publication number Publication date
ES2199069A1 (es) 2004-02-01
WO2004009206A1 (es) 2004-01-29
US7109384B2 (en) 2006-09-19
US20040176647A1 (en) 2004-09-09
AU2003208731A1 (en) 2004-02-09

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