ES2061882T3 - Procedimiento para la fabricacion de esteres de acido 1,2-naftoquinona-(2)-diazida-4-sulfonico sustituidos y su uso en una mezcla sensible a radiaciones. - Google Patents

Procedimiento para la fabricacion de esteres de acido 1,2-naftoquinona-(2)-diazida-4-sulfonico sustituidos y su uso en una mezcla sensible a radiaciones.

Info

Publication number
ES2061882T3
ES2061882T3 ES89119884T ES89119884T ES2061882T3 ES 2061882 T3 ES2061882 T3 ES 2061882T3 ES 89119884 T ES89119884 T ES 89119884T ES 89119884 T ES89119884 T ES 89119884T ES 2061882 T3 ES2061882 T3 ES 2061882T3
Authority
ES
Spain
Prior art keywords
substituted
diazide
acid esters
naphthoquinone
sulfonic acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES89119884T
Other languages
English (en)
Inventor
Herbert Dr Dipl-Chem Siegel
Siegfried Dr Dipl-Chem Scheler
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hoechst AG
Original Assignee
Hoechst AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hoechst AG filed Critical Hoechst AG
Application granted granted Critical
Publication of ES2061882T3 publication Critical patent/ES2061882T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/26—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of esters of sulfonic acids
    • C07C303/28—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of esters of sulfonic acids by reaction of hydroxy compounds with sulfonic acids or derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C309/00—Sulfonic acids; Halides, esters, or anhydrides thereof
    • C07C309/01—Sulfonic acids
    • C07C309/25—Sulfonic acids having sulfo groups bound to carbon atoms of rings other than six-membered aromatic rings of a carbon skeleton
    • C07C309/26—Sulfonic acids having sulfo groups bound to carbon atoms of rings other than six-membered aromatic rings of a carbon skeleton containing nitrogen atoms, not being part of nitro or nitroso groups, bound to the carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C309/00—Sulfonic acids; Halides, esters, or anhydrides thereof
    • C07C309/01—Sulfonic acids
    • C07C309/25—Sulfonic acids having sulfo groups bound to carbon atoms of rings other than six-membered aromatic rings of a carbon skeleton
    • C07C309/27—Sulfonic acids having sulfo groups bound to carbon atoms of rings other than six-membered aromatic rings of a carbon skeleton containing carboxyl groups bound to the carbon skeleton
    • G—PHYSICS
    • G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
    • G03F—PHOTOMECHANICAL PRODUCTION OF TEXTURED OR PATTERNED SURFACES, e.g. FOR PRINTING, FOR PROCESSING OF SEMICONDUCTOR DEVICES; MATERIALS THEREFOR; ORIGINALS THEREFOR; APPARATUS SPECIALLY ADAPTED THEREFOR
    • G03F7/00—Photomechanical, e.g. photolithographic, production of textured or patterned surfaces, e.g. printing surfaces; Materials therefor, e.g. comprising photoresists; Apparatus specially adapted therefor
    • G03F7/004—Photosensitive materials
    • G03F7/022—Quinonediazides

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Materials For Photolithography (AREA)

Abstract

EL INVENTO SE REFIERE A UN PROCEDIMIENTO PARA PRODUCIR ESTERES DEL ACIDO 1, 2 - NAFTOQUINONA (2) - DIAZIDA - 4 - SULFONICO DE FORMULA (I) QUE SE SUSTITUYEN EN POSICION 5, 6, 7 U 8 A TRAVES DE R. DICHO PROCEDIMIENTO CONSISTE EN: A) NITRAR EL -NAFTOL SUSTITUIDO; B) SULFONAR EL COMPUESTO DE A) CON SULFUROS ALCALINOS Y ACISOS; C) REDUCIR EL COMPUESTO DE B), PARA OBTENER EL DERIVADO DEL ACIDO NAFTALINOSULFONICO; D) OXIDAR EL DERIVADO DEL ACIDO NAFTALINOSULFONICO; E) TRATAR EL ACIDO 1, 2 - NAFTOQUINONA - 4- SULFONICO CON HIDRACIDO DEL ACIDO TOLMOLSULFONICO EN DISOLVENTES ORGANICOS Y ENTRE 20 Y 100 C; F) TRANSFORMAR EL COMPUESTO NAFTOQUINONA - DIAXIDA CON ACIDO CLOROSULFONICO EN SULFOCLORURO DEL COMPUESTO; Y G) CONDENSAR EL PRODUCTO DE F) CON UN COMPONENTE FENOLICO. UNA DEPURACION DE LOS PRODUCTOS INTERMEDIOS SE REALIZA POR PRECIPITACION O CRISTALICACION. EL PROCEDIMIENTO PERMITE UNA REALIZACION TECNICAMENTE SENCILLA CON BUEN RENDIMIENTO. LOS COMPUESTOS PRODUCIDOS COMO LOS ESTERES DEL ACIDO 1, 2 -NAFTOQUINONA - (2) - DIAZIDA - 4 - SULFONICO SUSTITUIDO MEDIANTE GRUPOS 6 - ALCOXICARBONILO SE EMPLEAN COMO COMPONENTES MEZCLAS SENSIBLES A LA RADIACION.
ES89119884T 1988-11-04 1989-10-26 Procedimiento para la fabricacion de esteres de acido 1,2-naftoquinona-(2)-diazida-4-sulfonico sustituidos y su uso en una mezcla sensible a radiaciones. Expired - Lifetime ES2061882T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE3837499A DE3837499A1 (de) 1988-11-04 1988-11-04 Verfahren zur herstellung von substituierten 1,2-naphthochinon-(2)-diazid-4-sulfonsaeureestern und deren verwendung in einem strahlungsempfindlichen gemisch

Publications (1)

Publication Number Publication Date
ES2061882T3 true ES2061882T3 (es) 1994-12-16

Family

ID=6366515

Family Applications (1)

Application Number Title Priority Date Filing Date
ES89119884T Expired - Lifetime ES2061882T3 (es) 1988-11-04 1989-10-26 Procedimiento para la fabricacion de esteres de acido 1,2-naftoquinona-(2)-diazida-4-sulfonico sustituidos y su uso en una mezcla sensible a radiaciones.

Country Status (7)

Country Link
US (1) US5082932A (es)
EP (1) EP0368085B1 (es)
JP (1) JPH0825986B2 (es)
KR (1) KR900007796A (es)
AT (1) ATE98226T1 (es)
DE (2) DE3837499A1 (es)
ES (1) ES2061882T3 (es)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3926776A1 (de) * 1989-08-12 1991-02-14 Hoechst Ag Substituierte 1,2-naphthochinon-(2)-diazid-4-sulfonsaeuren, verfahren zu ihrer herstellung und ihre verwendung
DE3926774A1 (de) * 1989-08-12 1991-02-14 Hoechst Ag 7-hydroxy-1,2-naphthochinon -(2)-diazid-4-sulfonsaeure oder ihre salze, verfahren zu ihrer herstellung und ihre verwendung
US5300396A (en) * 1990-11-28 1994-04-05 Hoechst Celanese Corporation Process of making naphthoquinone diazide esters using lactone solvents
DE602005027413D1 (de) * 2005-09-01 2011-05-19 Ministry Of Information Technology Eintopfverfahren zur darstellung von diazonaphthochinonsulfonylester
PL2137140T3 (pl) * 2007-03-23 2011-04-29 Council Scient Ind Res Nowe pochodne bisfenolowe kwasu diazonaftochinono-sulfonowego użyteczne w submikronowym odwzorowywaniu fotolitograficznym oraz proces ich otrzymywania
JP2019174793A (ja) * 2018-03-26 2019-10-10 Jsr株式会社 感放射線性組成物および１，２−ナフトキノン−２−ジアジドスルホン酸誘導体

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE500222A (es) * 1949-07-23
US3046121A (en) * 1949-07-23 1962-07-24 Azoplate Corp Process for the manufacture of printing plates and light-sensitive material suttablefor use therein
GB1375461A (es) * 1972-05-05 1974-11-27
US4439516A (en) * 1982-03-15 1984-03-27 Shipley Company Inc. High temperature positive diazo photoresist processing using polyvinyl phenol
DE3629122A1 (de) * 1986-08-27 1988-03-10 Hoechst Ag Verfahren zur herstellung eines o-naphthochinondiazidsulfonsaeureesters und diesen enthaltendes lichtempfindliches gemisch
US4931549A (en) * 1987-03-24 1990-06-05 Hoechst Celanese Corporation Process for aryl-quinone and aryl-naphthoquinone diazide sulfonic acids
US4818658A (en) * 1987-04-17 1989-04-04 Shipley Company Inc. Photoactive esterification product of a diazooxide compound and a curcumin dye and photoresist materials with product
DD269846A1 (de) * 1988-01-12 1989-07-12 Bitterfeld Chemie Verfahren zur herstellung von 1,2-naphthochinondiazid(2)-sulfochlorid(4)

Also Published As

Publication number Publication date
ATE98226T1 (de) 1993-12-15
US5082932A (en) 1992-01-21
DE3837499A1 (de) 1990-05-23
JPH0825986B2 (ja) 1996-03-13
JPH02172963A (ja) 1990-07-04
EP0368085A1 (de) 1990-05-16
DE58906373D1 (de) 1994-01-20
KR900007796A (ko) 1990-06-02
EP0368085B1 (de) 1993-12-08

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