ES2009698A6 - Preparacion de ciclopolidiorganosiloxanos mediante trasposicion en fase de vapor. - Google Patents
Preparacion de ciclopolidiorganosiloxanos mediante trasposicion en fase de vapor.Info
- Publication number
- ES2009698A6 ES2009698A6 ES8900105A ES8900105A ES2009698A6 ES 2009698 A6 ES2009698 A6 ES 2009698A6 ES 8900105 A ES8900105 A ES 8900105A ES 8900105 A ES8900105 A ES 8900105A ES 2009698 A6 ES2009698 A6 ES 2009698A6
- Authority
- ES
- Spain
- Prior art keywords
- cyclopolydiorganosiloxane
- r2sio
- cyclopolydiorganosiloxanes
- preparation
- vapor phase
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 230000008707 rearrangement Effects 0.000 title 1
- 239000012808 vapor phase Substances 0.000 title 1
- 239000003054 catalyst Substances 0.000 abstract 2
- 239000000463 material Substances 0.000 abstract 2
- 150000001339 alkali metal compounds Chemical class 0.000 abstract 1
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 239000011949 solid catalyst Substances 0.000 abstract 1
- 230000008016 vaporization Effects 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/045—Polysiloxanes containing less than 25 silicon atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/21—Cyclic compounds having at least one ring containing silicon, but no carbon in the ring
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Silicon Polymers (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PREPARACION DE CICLOPOLIDIORGANOSILOXANOS MEDIANTE TRASPOSICION EN FASE DE VAPOR. SE DESCRIBE UN PROCEDIMIENTO PARA PREPARAR UN CICLOPOLIDIORGANOSILOXANO (R2SIO)C. EL PROCEDIMIENTO COMPRENDE: (A) VAPORIZAR UNA ALIMENTACION DE UN MATERIAL DE CICLOPOLIDIORGANOSILOXANO (R2SIO)X; (B) PASAR LOS VAPORES DE (A) A TRAVES DE UN LECHO CALIENTE DE UN CATALIZADOR SOLIDO, DONDE EL CATALIZADOR COMPRENDE UN COMPUESTO DE UN METAL ALCALINO; (C) CONTROLAR LA PRESION Y LA TEMPERATURA EN EL LECHO DE CATALIZADOR CALIENTE PARA FAVORECER LA FORMACION DE (R2SIO)C EN UNA MEZCLA DE EQUILIBRIO CON OTROS CICLOPOLIDIORGANOSILOXANOS; Y (D) RECUPERAR UNA CANTIDAD DEL CICLOPOLIDIORGANOSILOXANO PRODUCTO (R2SIO)C, QUE ES SUSTANCIALMENTE MAS ALTA QUE LA CANTIDAD PRESENTE EN EL CICLOPOLIDIORGANOSILOXANO DE LA ALIMENTACION.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US07/144,287 US4764631A (en) | 1988-01-15 | 1988-01-15 | Preparation of cyclopolydiorganosiloxanes via vapor phase rearrangement |
Publications (1)
Publication Number | Publication Date |
---|---|
ES2009698A6 true ES2009698A6 (es) | 1989-10-01 |
Family
ID=22507913
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES8900105A Expired ES2009698A6 (es) | 1988-01-15 | 1989-01-12 | Preparacion de ciclopolidiorganosiloxanos mediante trasposicion en fase de vapor. |
Country Status (8)
Country | Link |
---|---|
US (1) | US4764631A (es) |
EP (1) | EP0328241B1 (es) |
JP (1) | JPH078876B2 (es) |
CN (1) | CN1020455C (es) |
BR (1) | BR8900175A (es) |
CA (1) | CA1326677C (es) |
DE (1) | DE68918877T2 (es) |
ES (1) | ES2009698A6 (es) |
Families Citing this family (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4895967A (en) * | 1988-09-26 | 1990-01-23 | General Electric Company | Method for making cyclic poly(siloxane)s |
US5110972A (en) * | 1991-07-18 | 1992-05-05 | Tremco Incorporated | Process for recycling silicone scrap and products relating thereto |
US5196559A (en) * | 1992-01-23 | 1993-03-23 | Dow Corning Corporation | Equilibration of cyclic siloxanes with novel catalysts |
US5233070A (en) * | 1992-12-23 | 1993-08-03 | Dow Corning Corporation | Process for converting chlorine end-terminated polyorganosiloxanes to polyorganocyclosiloxanes |
US5420325A (en) * | 1994-07-29 | 1995-05-30 | General Electric Company | Siloxane cracking process |
US5491249A (en) * | 1995-04-20 | 1996-02-13 | Hercules Incorporated | Process for preparing cyclic polysiloxanes from linear polysiloxanes |
JPH1045770A (ja) * | 1996-07-29 | 1998-02-17 | Toray Dow Corning Silicone Co Ltd | ヘキサメチルシクロトリシロキサンの分離方法 |
AU6559996A (en) * | 1996-09-13 | 1998-03-19 | Huntsman, Peter Harold | Process for the recovery of methyl polysiloxanes in the form of methyl cyclosiloxanes |
US6262289B1 (en) | 1997-06-11 | 2001-07-17 | Kaneka Corporation | Process for preparing cyclic oligosiloxanes |
JP4663838B2 (ja) | 2000-01-28 | 2011-04-06 | 東レ・ダウコーニング株式会社 | 環状シロキサンの製造方法 |
US7456488B2 (en) * | 2002-11-21 | 2008-11-25 | Advanced Technology Materials, Inc. | Porogen material |
US7423166B2 (en) * | 2001-12-13 | 2008-09-09 | Advanced Technology Materials, Inc. | Stabilized cyclosiloxanes for use as CVD precursors for low-dielectric constant thin films |
US7108771B2 (en) * | 2001-12-13 | 2006-09-19 | Advanced Technology Materials, Inc. | Method for removal of impurities in cyclic siloxanes useful as precursors for low dielectric constant thin films |
JP5844153B2 (ja) * | 2008-08-27 | 2016-01-13 | ダウ コーニング コーポレーションDow Corning Corporation | ポリシロキサンの再配分方法 |
WO2021180308A1 (de) * | 2020-03-10 | 2021-09-16 | Wacker Chemie Ag | Verfahren zur aufarbeitung von (m/d/t)-methylpolysiloxan-mischungen aus wärmeträgeranwendungen |
Family Cites Families (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2438478A (en) * | 1942-02-26 | 1948-03-23 | Corning Glass Works | Method of preparing silicones and product thereof |
US2455999A (en) * | 1944-08-01 | 1948-12-14 | Corning Glass Works | Method of preparing organosilicones |
BE537467A (es) * | 1954-04-21 | |||
US2884432A (en) * | 1956-02-09 | 1959-04-28 | Dow Corning | Method of preparing cyclic siloxanes |
US2860152A (en) * | 1956-04-26 | 1958-11-11 | Dow Corning | Method of producing cyclic diorganosiloxanes |
US2979519A (en) * | 1956-06-27 | 1961-04-11 | Dow Corning | New cyclotrisiloxanes |
US3110720A (en) * | 1960-11-01 | 1963-11-12 | Union Carbide Corp | Process for producing cyclic diorganosiloxanes from diorganodihalosilanes and alkaliand alkali earth metal oxides and carbonates |
NL129878C (es) * | 1966-01-17 | |||
NL6816661A (es) * | 1968-12-18 | 1970-05-25 | ||
GB1293944A (en) * | 1969-04-18 | 1972-10-25 | Dow Corning Ltd | Preparation of cyclic siloxanes |
US3607898A (en) * | 1969-08-20 | 1971-09-21 | Gen Electric | Process for preparing cyclic syn-tetramethyltetravinyltetrasiloxane |
JPS5250791B2 (es) * | 1972-12-30 | 1977-12-27 | ||
US3846464A (en) * | 1973-11-27 | 1974-11-05 | Gen Electric | Process for preparing cyclic methylvinylsiloxanes |
US4111973A (en) * | 1977-12-01 | 1978-09-05 | General Electric Company | Process for producing a cyclotrisiloxane in a cracking reaction |
JPS54117491A (en) * | 1978-03-06 | 1979-09-12 | Asahi Chem Ind Co Ltd | Preparation of octamethyl-cyclotetrasiloxane |
US4412081A (en) * | 1982-08-27 | 1983-10-25 | General Electric Company | Methods for preparing decamethyl cyclopentasiloxane |
EP0126792B1 (de) * | 1983-05-27 | 1986-10-15 | Consortium für elektrochemische Industrie GmbH | Verfahren zur Herstellung von Hexamethylcyclotrisiloxan und eine Verwendung des so hergestellten Cyclotrisiloxans |
US4556726A (en) * | 1985-01-09 | 1985-12-03 | Union Carbide Corporation | Process for converting octamethylcyclotetrasiloxane to decamethylcyclopentasiloxane |
US4689420A (en) * | 1985-11-19 | 1987-08-25 | Dow Corning Corporation | Process for preparation of cyclopolydiorganosiloxanes |
-
1988
- 1988-01-15 US US07/144,287 patent/US4764631A/en not_active Expired - Lifetime
- 1988-12-16 CA CA000586140A patent/CA1326677C/en not_active Expired - Fee Related
-
1989
- 1989-01-10 EP EP89300183A patent/EP0328241B1/en not_active Expired - Lifetime
- 1989-01-10 DE DE68918877T patent/DE68918877T2/de not_active Expired - Lifetime
- 1989-01-12 ES ES8900105A patent/ES2009698A6/es not_active Expired
- 1989-01-13 JP JP1005075A patent/JPH078876B2/ja not_active Expired - Lifetime
- 1989-01-14 CN CN89100198A patent/CN1020455C/zh not_active Expired - Lifetime
- 1989-01-16 BR BR898900175A patent/BR8900175A/pt not_active Application Discontinuation
Also Published As
Publication number | Publication date |
---|---|
DE68918877T2 (de) | 1995-05-18 |
JPH01216999A (ja) | 1989-08-30 |
EP0328241A3 (en) | 1990-12-05 |
CA1326677C (en) | 1994-02-01 |
US4764631A (en) | 1988-08-16 |
BR8900175A (pt) | 1989-09-12 |
CN1020455C (zh) | 1993-05-05 |
JPH078876B2 (ja) | 1995-02-01 |
DE68918877D1 (de) | 1994-11-24 |
EP0328241A2 (en) | 1989-08-16 |
CN1034730A (zh) | 1989-08-16 |
EP0328241B1 (en) | 1994-10-19 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
FD1A | Patent lapsed |
Effective date: 20050113 |