EP1607106A1 - Gefässbehandlungsmaschine zur Sterilisation von Behältern mittels H202 - Google Patents
Gefässbehandlungsmaschine zur Sterilisation von Behältern mittels H202 Download PDFInfo
- Publication number
- EP1607106A1 EP1607106A1 EP05011067A EP05011067A EP1607106A1 EP 1607106 A1 EP1607106 A1 EP 1607106A1 EP 05011067 A EP05011067 A EP 05011067A EP 05011067 A EP05011067 A EP 05011067A EP 1607106 A1 EP1607106 A1 EP 1607106A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- machine according
- treatment machine
- catalyst
- container
- decomposition
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2/00—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor
- A61L2/16—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor using chemical substances
- A61L2/20—Gaseous substances, e.g. vapours
- A61L2/208—Hydrogen peroxide
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2/00—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor
- A61L2/16—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor using chemical substances
- A61L2/22—Phase substances, e.g. smokes, aerosols or sprayed or atomised substances
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2202/00—Aspects relating to methods or apparatus for disinfecting or sterilising materials or objects
- A61L2202/20—Targets to be treated
- A61L2202/23—Containers, e.g. vials, bottles, syringes, mail
Definitions
- the present invention relates to a vessel treatment machine according to the preamble of claim 1.
- Advantageous developments are in the dependent claims specified.
- H 2 O 2 sterilization is known here.
- liquid H 2 O 2 is first admixed with a fine stream of air, which is usually a stream of sterile air. Subsequently, this H 2 O 2 -air mixture is fed to an evaporator, in which the still liquid H 2 O 2 is completely evaporated.
- this vapor-air mixture is introduced into the container to be sterilized, where the H 2 O 2 immediately condenses on the cold container inner walls and forms a uniform liquid film there.
- activation of the H 2 O 2 ie for triggering the decomposition of the H 2 O 2
- This activation medium is, in most cases, sterile air blown into the containers which has been heated to the temperature required to activate the H 2 O 2 .
- the H 2 O 2 decomposes into water and free radicals, namely atomic oxygen and HO groups, which essentially perform the actual sterilization.
- the containers are blown out by means of rinsing and / or drying air and dried.
- Another disadvantage of temperature activation is that, in particular with exclusive sterilization of the inner walls of the plastic bottles more or less large temperature differences in the walls of the plastic bottles may occur, whereby e.g. through the formation of cracks to one reduced durability and impairments in terms of visual appearance the container can come.
- Object and purpose of the present invention is to avoid the disadvantages presented above while achieving a significantly reduced activation or decomposition time for the H 2 O 2 safe.
- the invention provides to accelerate the decomposition of the H 2 O 2 by the use of at least one catalyst, wherein the required decomposition temperature is also reduced.
- FIG. 1 shows, in a simplified representation, a sterilizer head 3, as it does several both rotary and linear machines for the disinfection of Containers can be arranged.
- the sterilizer head 3 to be understood as an exemplary embodiment is used for H 2 O 2 sterilization of containers, eg temperature-sensitive PET bottles.
- a container or bottle carrier is provided in each case, on which the respective bottle to be sterilized, e.g. kept hanging, and the same axis with a vertical Sterilisatorkopfachse KA, so when activated of the sterilizer head 3 a jet of hot sterilization medium into the interior the sterilizer located below the sterilization head 3 to be sterilized Bottle 4 bottle can be applied.
- the sterilizer head 3 consists of a heater or heat exchanger 5 with a Housing 6, in which u. a. a helical flow surrounding the axis KA or heating channel 7 is formed, in the illustrated embodiment in that in a circular cylindrical, coaxial with the axis KA trained through opening of the housing 6, a core 8 is inserted, the has at its periphery a spiral channel 7 forming the helical groove.
- the upper end of the outwardly closed flow channel 7 in FIG. 1 communicates with a spraying device 9, which is supplied with sterile compressed air via the connection 10 and which has a spray nozzle 11 which is connected via the connection 12 and connected to this connection.
- pump such as a membrane pump
- H 2 O 2 is supplied, which is then introduced to form the H 2 O 2 -air aerosol via the spray nozzle 11 as a finely sprayed jet or mist in the air flowing through the spray 9, so that this air and H 2 O 2 existing aerosol then enters the flow channel 7 of the heat exchanger 5.
- thermocouple By a heater, not shown, which e.g. from an electrical Heating cartridge can be formed with thermocouple, the heat exchanger 5 and in particular, the core 8 heated.
- the lower end of the housing 6 is formed by suitable elements which allow the vapor-air mixture containing the H 2 O 2 vapor to be continuously or else discontinuously discharged directly or indirectly into the bottles 4 to be sterilized.
- suitable elements which allow the vapor-air mixture containing the H 2 O 2 vapor to be continuously or else discontinuously discharged directly or indirectly into the bottles 4 to be sterilized.
- a tube 26 which may at least temporarily extend into the bottles 4 with its discharge opening 27, or may be positioned with its discharge opening 27 immediately in front of the mouth of the bottles 4.
- the heat exchanger is heated by the heater, and to a temperature which, taking into account all relevant parameters, such as volume and / or mass flow of H 2 O 2- containing aerosol, outlet temperature of the aerosol, specific heat capacity, etc. ensures that the im Aerosol contained H 2 O 2 at the latest when leaving the heat exchanger 5 is evaporated to the desired extent.
- At least one catalyst to initiate and support to be arranged within the path of the H 2 O 2 or the path of, the H 2 O 2 aerosol containing the decomposition process of the H 2 O 2 at low temperatures.
- the inventive arrangement of the at least one catalyst is achieved that the required for triggering the decomposition process of H 2 O 2 activation energy is reduced, so that the decomposition already proceeds at room temperature, for example, at high speed, whereby the effective free radicals not only by time-consuming thermal Activation must be generated within the bottles 4 but can be introduced directly into this.
- the platinum group precious metals known to be particularly suitable, but also e.g. Braunstein or other substances.
- the interior of the tube 26 at least partially with a catalyst fill.
- the surface of the heat exchanger 5 at least partially to coat with a material effective as a catalyst, or the heat exchanger 5 at least partially made of such a material.
- each sterilizer head or each treatment station at least one catalyst to assign directly, and / or at least one catalyst a group of sterilizer heads, and / or all sterilizer heads To assign a sterilization machine together at least one catalyst.
- the at least one catalyst is formed as an (additional) heating element, which results in further possibilities for targeted control of the decomposition process of the H 2 O 2 .
Landscapes
- Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Public Health (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Epidemiology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- General Health & Medical Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Veterinary Medicine (AREA)
- Apparatus For Disinfection Or Sterilisation (AREA)
- Catalysts (AREA)
- Filling Of Jars Or Cans And Processes For Cleaning And Sealing Jars (AREA)
- Container Filling Or Packaging Operations (AREA)
- Food Preservation Except Freezing, Refrigeration, And Drying (AREA)
Abstract
Description
- Figuren 1 und 3
- in vereinfachten Schnittdarstellungen Sterilisatorköpfe, und die
- Figur 2
- in einer vereinfachten Draufsicht eine als Rundläufer ausgebildete Gefäßbehandlungsmaschine.
Erfindungsgemäß ist vorgesehen, innerhalb des Weges des H2O2 bzw. des Weges des, das H2O2 enthaltenden Aerosols mindestens einen Katalysator zur Auslösung und Unterstützung des Zersetzungsprozesses des H2O2 bei niedrigen Temperaturen anzuordnen.
Claims (16)
- Gefäßbehandlungsmaschine, insbesondere zur Sterilisation von aus Kunststoff, Metall oder Glas bestehenden Flaschen, Dosen oder dergleichen Behälter mittels H2O2, ausgeführt in Rundläufer- oder Linearbauweise dadurch gekennzeichnet, dass im Strömungsweg des flüssigen und/oder gasförmigen H2O2 mindestens ein, die Zersetzung des H2O2 fördernder Katalysator angeordnet ist.
- Gefäßbehandlungsmaschine nach Anspruch 1, dadurch gekennzeichnet, dass der mindestens eine Katalysator auf dem Weg des H2O2 von seiner Quelle zu dem zu behandelnden Behälter (4) angeordnet ist.
- Gefäßbehandlungsmaschine nach Anspruch 1 oder 2, dadurch gekennzeichnet, dass der mindestens eine Katalysator innerhalb eines, das H2O2 und/oder dessen Zersetzungsprodukte in oder an die Behälter (4) leitenden Rohres (26) angeordnet ist.
- Gefäßbehandlungsmaschine nach einem der vorhergehenden Ansprüche, dadurch gekennzeichnet, dass der Katalysator als ein, das H2O2 und/oder dessen Zersetzungsprodukte in oder an die Behälter (4) leitendes, aus porösem Material bestehendes Rohr (26) mit ausgebildet ist.
- Gefäßbehandlungsmaschine nach einem der vorhergehenden Ansprüche, dadurch gekennzeichnet, dass die Oberfläche des Wärmetauschers (5) zumindest teilweise als Katalysator ausgebildet ist.
- Gefäßbehandlungsmaschine nach einem der vorhergehenden Ansprüche, dadurch gekennzeichnet, dass der Wärmetauscher (5) zumindest teilweise aus katalytisch wirksamen Material besteht.
- Gefäßbehandlungsmaschine nach einem der vorhergehenden Ansprüche, dadurch gekennzeichnet, dass der mindestens eine Katalysator aus Edelmetallen der Platingruppe und/oder Braunstein besteht.
- Gefäßbehandlungsmaschine nach einem der vorhergehenden Ansprüche, dadurch gekennzeichnet, dass der mindestens eine Katalysator mittels pulvermetallurgischer Verfahren hergestellt ist.
- Gefäßbehandlungsmaschine nach einem der vorhergehenden Ansprüche, dadurch gekennzeichnet, dass der mindestens eine Katalysator aus, aus Draht kleinen Durchmessers hergestellten Drahtgeflechten besteht.
- Gefäßbehandlungsmaschine nach einem der vorhergehenden Ansprüche, dadurch gekennzeichnet, dass der mindestens eine Katalysator als Heizelement für das H2O2 bzw. dessen Zersetzungsprodukte ausgebildet ist.
- Gefäßbehandlungsmaschine nach einem der vorhergehenden Ansprüche, dadurch gekennzeichnet, dass jedem Sterilisator mindestens ein Katalysator unmittelbar zugeordnet ist.
- Gefäßbehandlungsmaschine nach einem der vorhergehenden Ansprüche, dadurch gekennzeichnet, dass einer Gruppe von Sterilisatoren mindestens ein Katalysator unmittelbar zugeordnet ist.
- Gefäßbehandlungsmaschine nach einem der vorhergehenden Ansprüche, dadurch gekennzeichnet, dass allen Sterilisatoren einer Gefäßbehandlungsmaschine mindestens ein Katalysator unmittelbar zugeordnet ist.
- Verfahren zum Betrieb einer Gefäßbehandlungsmaschine nach einem der vorhergehenden Ansprüche, dadurch gekennzeichnet, dass die Zersetzung des H2O2 bei einer Temperatur unterhalb der maximal zulässigen Temperatur der zu behandelnden Behälter erfolgt.
- Verfahren zum Betrieb einer Gefäßbehandlungsmaschine nach einem der vorhergehenden Ansprüche, dadurch gekennzeichnet, dass die Zersetzung des H2O2 bei einer Temperatur unterhalb der Rückverformungs- und/oder Schrumpfungstemperatur von Kunststoffbehältern erfolgt.
- Verfahren zum Betrieb einer Gefäßbehandlungsmaschine nach einem der vorhergehenden Ansprüche, dadurch gekennzeichnet, dass die Zersetzung des H2O2 bei Raumtemperatur erfolgt, vorzugsweise im Temperaturbereich von15 bis 25 °C.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
PL05011067T PL1607106T3 (pl) | 2004-06-19 | 2005-05-23 | Maszyna do obróbki pojemników do sterylizacji pojemników za pomocą H₂O₂ |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE102004029803A DE102004029803B4 (de) | 2004-06-19 | 2004-06-19 | Gefäßbehandlungsmaschine zur Sterilisation von Behältern mittels H2O2 |
DE102004029803 | 2004-06-19 |
Publications (2)
Publication Number | Publication Date |
---|---|
EP1607106A1 true EP1607106A1 (de) | 2005-12-21 |
EP1607106B1 EP1607106B1 (de) | 2011-02-09 |
Family
ID=34936805
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP05011067A Not-in-force EP1607106B1 (de) | 2004-06-19 | 2005-05-23 | Gefässbehandlungsmaschine zur Sterilisation von Behältern mittels H202 |
Country Status (6)
Country | Link |
---|---|
US (1) | US20060011262A1 (de) |
EP (1) | EP1607106B1 (de) |
JP (1) | JP2006001649A (de) |
AT (1) | ATE497789T1 (de) |
DE (2) | DE102004029803B4 (de) |
PL (1) | PL1607106T3 (de) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE102007001970A1 (de) * | 2007-01-13 | 2008-07-17 | Khs Ag | Verfahren und Vorrichtung zur Sterilisation von Behältern aus Metall |
WO2008121455A2 (en) * | 2007-03-06 | 2008-10-09 | Steris Inc. | Decontamination unit with collapsible decontamination enclosure and decontamination process |
CN103223181A (zh) * | 2013-05-21 | 2013-07-31 | 上海净达制药设备***工程有限公司 | 一种气化过氧化氢旋转真空灭菌装置 |
CN112660514A (zh) * | 2019-10-15 | 2021-04-16 | 克罗内斯股份公司 | 在饮料灌装设施中的容器的灭菌 |
Families Citing this family (13)
Publication number | Priority date | Publication date | Assignee | Title |
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DE102005009875B4 (de) * | 2005-03-01 | 2008-01-17 | Sig Technology Ag | Verfahren und Vorrichtung zur Sterilisation der Oberfläche von Objekten |
DE102006038747A1 (de) * | 2006-08-17 | 2008-03-20 | Khs Ag | Dichtanordnung für eine Drehlagervorrichtung |
DE102008015675A1 (de) * | 2008-03-25 | 2009-10-01 | Khs Ag | Gefäßbehandlungsmaschine |
DE102008031369B4 (de) * | 2008-07-04 | 2011-04-07 | Khs Gmbh | Verfahren zur Behandlung von Kunststoff-Einwegbehältern |
DE102009043496A1 (de) | 2009-09-30 | 2011-04-14 | Khs Gmbh | Verfahren und Vorrichtung zur Sterilisation von Oberflächen |
DE102009043726A1 (de) | 2009-10-01 | 2011-04-07 | Khs Gmbh | Verfahren und Vorrichtung zur Sterilisation von Oberflächen |
WO2011038799A1 (de) | 2009-09-30 | 2011-04-07 | Khs Gmbh | Verfahren und vorrichtung zur sterilisation von oberflächen |
BR112012026443A2 (pt) * | 2010-04-16 | 2016-08-09 | Gustavo Pérez López | um recipiente de líquido projetado para incluir dispositivo de resfriamento autônomo seletivo e dispositivo de refrigeração aplicável ao referido recipiente de líquido |
JP5972195B2 (ja) | 2013-03-11 | 2016-08-17 | サントリーホールディングス株式会社 | Pet製ボトルの殺菌装置及び殺菌方法 |
US10440989B2 (en) * | 2016-11-11 | 2019-10-15 | Portland Engineering, Inc. | E-cigarette vaporizer cartridge filling method and apparatus |
USD846608S1 (en) * | 2017-03-14 | 2019-04-23 | M&M Machinery Services, Inc. | Receiver for a bottling machine |
US11166490B2 (en) | 2019-11-13 | 2021-11-09 | Portland Engineering, Inc. | E-cigarette vaporizer device filling system and method |
US20220132939A1 (en) * | 2020-11-04 | 2022-05-05 | Anthony Hamilton | E-Cigarette Vaporizer Cartridge Filling Device |
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US4214867A (en) * | 1978-07-18 | 1980-07-29 | Matthey Bishop, Inc. | Method and apparatus for catalytic heat exchange |
US4742667A (en) * | 1981-11-14 | 1988-05-10 | Mueller Horst | Method of and apparatus for sterilizing packaging material, especially container-type packages |
NL9201556A (nl) * | 1992-09-07 | 1994-04-05 | E M Engineering F T S B V | Werkwijze en inrichting voor het reinigen van vloeistof. |
JP2000153285A (ja) * | 1998-11-17 | 2000-06-06 | Shinsanso Kagaku Kk | 高度酸化処理方法 |
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2004
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2005
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- 2005-05-23 PL PL05011067T patent/PL1607106T3/pl unknown
- 2005-05-23 AT AT05011067T patent/ATE497789T1/de active
- 2005-05-23 EP EP05011067A patent/EP1607106B1/de not_active Not-in-force
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- 2005-06-17 US US11/156,267 patent/US20060011262A1/en not_active Abandoned
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Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE102007001970A1 (de) * | 2007-01-13 | 2008-07-17 | Khs Ag | Verfahren und Vorrichtung zur Sterilisation von Behältern aus Metall |
WO2008083824A2 (de) * | 2007-01-13 | 2008-07-17 | Khs Ag | Verfahren und vorrichtung zur sterilisation von behältern aus metall |
WO2008083824A3 (de) * | 2007-01-13 | 2008-09-18 | Khs Ag | Verfahren und vorrichtung zur sterilisation von behältern aus metall |
WO2008121455A2 (en) * | 2007-03-06 | 2008-10-09 | Steris Inc. | Decontamination unit with collapsible decontamination enclosure and decontamination process |
WO2008121455A3 (en) * | 2007-03-06 | 2008-11-20 | Steris Inc | Decontamination unit with collapsible decontamination enclosure and decontamination process |
US8216523B2 (en) | 2007-03-06 | 2012-07-10 | Steris Inc. | Decontamination unit with collapsible decontamination enclosure and decontamination process |
CN103223181A (zh) * | 2013-05-21 | 2013-07-31 | 上海净达制药设备***工程有限公司 | 一种气化过氧化氢旋转真空灭菌装置 |
CN103223181B (zh) * | 2013-05-21 | 2015-06-17 | 上海净达制药设备***工程有限公司 | 一种气化过氧化氢旋转真空灭菌装置 |
CN112660514A (zh) * | 2019-10-15 | 2021-04-16 | 克罗内斯股份公司 | 在饮料灌装设施中的容器的灭菌 |
EP3808382A1 (de) * | 2019-10-15 | 2021-04-21 | Krones Ag | Sterilisation von behältern in getränkeabfüllanlagen |
Also Published As
Publication number | Publication date |
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DE502005010947D1 (de) | 2011-03-24 |
US20060011262A1 (en) | 2006-01-19 |
PL1607106T3 (pl) | 2011-07-29 |
DE102004029803B4 (de) | 2007-01-11 |
EP1607106B1 (de) | 2011-02-09 |
DE102004029803A1 (de) | 2006-01-12 |
JP2006001649A (ja) | 2006-01-05 |
ATE497789T1 (de) | 2011-02-15 |
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