EP0271155B1 - Verfahren zum enzymatischen Waschen und Spülen von Geschirr. - Google Patents

Verfahren zum enzymatischen Waschen und Spülen von Geschirr. Download PDF

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Publication number
EP0271155B1
EP0271155B1 EP87202387A EP87202387A EP0271155B1 EP 0271155 B1 EP0271155 B1 EP 0271155B1 EP 87202387 A EP87202387 A EP 87202387A EP 87202387 A EP87202387 A EP 87202387A EP 0271155 B1 EP0271155 B1 EP 0271155B1
Authority
EP
European Patent Office
Prior art keywords
weight
lipase
pseudomonas
dishwashing
process according
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
EP87202387A
Other languages
English (en)
French (fr)
Other versions
EP0271155A3 (en
EP0271155A2 (de
EP0271155B2 (de
Inventor
Willem Robert Van Dijk
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Unilever PLC
Unilever NV
Original Assignee
Unilever PLC
Unilever NV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=10608788&utm_source=***_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=EP0271155(B1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Unilever PLC, Unilever NV filed Critical Unilever PLC
Publication of EP0271155A2 publication Critical patent/EP0271155A2/de
Publication of EP0271155A3 publication Critical patent/EP0271155A3/en
Application granted granted Critical
Publication of EP0271155B1 publication Critical patent/EP0271155B1/de
Publication of EP0271155B2 publication Critical patent/EP0271155B2/de
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/38—Products with no well-defined composition, e.g. natural products
    • C11D3/386—Preparations containing enzymes, e.g. protease or amylase
    • C11D3/38627—Preparations containing enzymes, e.g. protease or amylase containing lipase

Definitions

  • EP-A-0 205 208 discloses enzymatic detergent compositions comprising lipase with 1-40% anionic surfactant and builders.
  • the lipases disclosed are those that cross-react with antibody against lipase from Pseudomonas fluorescens 1 AM 1057.
  • the invention provides a process for machine dishwashing or rinsing, comprising treating dishes with an aqueous liquid having dissolved or dispersed therein an effective amount of an enzymatic dishwashing or rinsing composition comprising from 0.5-10% by weight of a detergent surfactant and from 0-90% by weight of a builder, characterised in that it further comprises from 0.005-100 LU/mg of a lipolytic enzyme.
  • the preparation of the antiserum is carried out as follows: Equal volumes of 0.1 mg/ml antigen and of Freund's adjuvant (complete or incomplete) are mixed until an emulsion is obtained. Two female rabbits are injected with 2 ml samples of the emulsion according to the following scheme:
  • the serum containing the required antibody is prepared by centrifugation of clotted blood, taken on day 67.
  • Chromobacter viscosum e.g. Chromobacter viscosum var. lipolyticum NRRLB 3673, commercially available from Toyo Jozo Co., Tagata, Japan; and further Chromobacter viscosum lipases from US Biochemical Corp., U.S.A. and Diosynth Co., The Netherlands, and lipases ex Pseudomonas gladioli.
  • Example 2 Replacing the Toyo Jozo lipase by the Amano-P lipase or Lipase MY (ex Candida cylindracea) or Amano AP-6 lipase (ex Aspergillus niger) in Example 2 gave similar results.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Detergent Compositions (AREA)

Claims (5)

1. Verfahren zum Maschinen-Geschirrwaschen oder -Spülen, das das Behandeln von Geschirr mit einer wässrigen Flüssigkeit, in der eine wirksame Menge einer enzymatischen Geschirrwasch- oder Spül-Zusammensetzung, umfassend 0,5-10 Gew.-% eines Detergensoberflächenaktiven Materials und 0-90 Gew.-% eines Builders, gelöst oder dispergiert wurde, umfaßt, dadurch gekennzeichnet, daß es weiterhin 0,005-100 LU(Lipase-Einheiten)/mg eines lipolytischen Enzyms umfaßt.
2. Verfahren nach Anspruch 1, dadurch gekennzeichnet, daß die Lipase eine bakterielle Lipase ist, die eine positive immunologische Kreuzreaktion mit dem Antikörper der Lipase, die durch Chromobacter viscosum var. lipolyticum NRRL B 3673 gebildet wird, zeigt.
3. Verfahren nach Anspruch 2, dadurch gekennzeichnet, daß die Lipase durch den Mikroorganismus, ausgewählt aus der Gruppe bestehend aus Pseudomonas fluorescens, Pseudomonas fragi, Pseudomonas nitroreducens var. lipolyticum, Pseudomonas cepacia, Pseudomonas gladioli und Chromobacter viscosum, gebildet werden kann.
4. Maschinen-Geschirrwasch-Verfahren nach einem der Ansprüche 1-3, dadurch gekennzeichnet, daß eine Zusammensetzung verwendet wird, die 20-60 Gew.-% eines Alkalimetallsilikats, 1-1-5 Gew.-% eines Bleichmittels vom Peroxytyp und 0,5-5 Gew.-% eines schwachschäumenden nicht-ionischen Detergens enthält.
5. Maschinen-Spülverfahren nach einem der Ansprüche 1-3, dadurch gekennzeichnet, daß eine Zusammensetzung verwendet wird, die in einem wässrigen Medium 0,5-10 Gew.-% eines nicht-ionischen oberflächenaktiven Materials, 5-25 Gew.-% einer organischen oder anorganischen Säure und 1-5 Gew.- % eines Hydrotops enthält.
EP87202387A 1986-12-10 1987-12-02 Verfahren zum enzymatischen Waschen und Spülen von Geschirr Expired - Lifetime EP0271155B2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GB8629538 1986-12-10
GB868629538A GB8629538D0 (en) 1986-12-10 1986-12-10 Enzymatic dishwashing & rinsing composition

Publications (4)

Publication Number Publication Date
EP0271155A2 EP0271155A2 (de) 1988-06-15
EP0271155A3 EP0271155A3 (en) 1988-08-17
EP0271155B1 true EP0271155B1 (de) 1991-09-04
EP0271155B2 EP0271155B2 (de) 2000-09-06

Family

ID=10608788

Family Applications (1)

Application Number Title Priority Date Filing Date
EP87202387A Expired - Lifetime EP0271155B2 (de) 1986-12-10 1987-12-02 Verfahren zum enzymatischen Waschen und Spülen von Geschirr

Country Status (8)

Country Link
EP (1) EP0271155B2 (de)
JP (1) JPS63161086A (de)
AU (1) AU609755B2 (de)
BR (1) BR8706685A (de)
DE (1) DE3772726D1 (de)
ES (1) ES2025635T5 (de)
GB (1) GB8629538D0 (de)
ZA (1) ZA879297B (de)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109563449A (zh) * 2016-06-23 2019-04-02 诺维信公司 酶的用途、组合物以及用于去除污垢的方法

Families Citing this family (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0218272B1 (de) * 1985-08-09 1992-03-18 Gist-Brocades N.V. Lipolytische Enzyme und deren Anwendung in Reinigungsmitteln
BE1001436A3 (fr) * 1988-02-22 1989-10-31 Synfina Sa Nouvelle lipase et compositions detergentes en contenant.
GB8813687D0 (en) * 1988-06-09 1988-07-13 Unilever Plc Enzymatic dishwashing & rinsing composition
GB8813688D0 (en) * 1988-06-09 1988-07-13 Unilever Plc Enzymatic dishwashing composition
JPH0277498A (ja) * 1988-09-14 1990-03-16 Lion Corp 自動食器洗い機用洗浄剤組成物
US4908150A (en) * 1989-02-02 1990-03-13 Lever Brothers Company Stabilized lipolytic enzyme-containing liquid detergent composition
JPH02245129A (ja) * 1989-03-17 1990-09-28 Novo Nordisk As 家畜汚れの酵素的除去法
GB8923788D0 (en) * 1989-10-23 1989-12-13 Unilever Plc Enzymatic detergent compositions and their use
JP2620384B2 (ja) * 1989-12-20 1997-06-11 花王株式会社 自動食器洗浄機用食器洗浄剤組成物
JPH0699715B2 (ja) * 1990-07-11 1994-12-07 花王株式会社 自動食器洗浄機用洗浄剤組成物
GB2247025A (en) * 1990-08-13 1992-02-19 Unilever Plc Enzymatic dishwashing and rinsing composition
US5527484A (en) * 1991-05-31 1996-06-18 Colgate-Palmolive Co. Phosphate containing powdered automatic dishwashing composition with enzymes
TR28788A (tr) 1993-05-25 1997-03-25 Henkel Ecolab Gmbh & Co Ohg Makinayla bulasik temizlemege mahsus usul ve tertibat.
DE4324106C1 (de) * 1993-05-25 1994-09-15 Henkel Ecolab Gmbh & Co Ohg Verfahren und Vorrichtung zur Zudosierung von Wirkstoffen zu einer Spülmaschine
HUT73758A (en) * 1993-08-10 1996-09-30 Procter & Gamble Manual dishwashing composition comprising lipase enzymes
US5772786A (en) * 1993-08-13 1998-06-30 The Procter & Gamble Company Detergent composition comprising lime soap dispersant and lipase enzymes
EP0846155B1 (de) * 1995-08-25 2000-02-09 Henkel Kommanditgesellschaft auf Aktien Verwendung von lipasen in niederalkalischen mitteln zum maschinellen geschirrspülen
BRPI0808513A2 (pt) 2007-03-09 2014-08-19 Danisco Us Inc Genencor Div Variantes de alfa-amilase de espécies de bacillus alcalifílico, composições compreendendo variantes de alfa-amilase e métodos de uso
US9040279B2 (en) 2008-06-06 2015-05-26 Danisco Us Inc. Saccharification enzyme composition and method of saccharification thereof
CA2726803A1 (en) 2008-06-06 2009-12-10 Danisco Us Inc. Variant alpha-amylases from bacillus subtilis and methods of use, thereof
EP2698434A1 (de) 2008-06-06 2014-02-19 Danisco US Inc. Verwendungen einer Alpha-Amylase aus Bacillus subtilis
WO2010036515A1 (en) 2008-09-25 2010-04-01 Danisco Us Inc. Alpha-amylase blends and methods for using said blends
CA2778471A1 (en) 2009-10-23 2011-04-28 Danisco Us Inc. Methods for reducing blue saccharide
JP5246300B2 (ja) * 2011-06-14 2013-07-24 Ｊｆｅスチール株式会社 車体側部構造

Family Cites Families (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2071237A5 (en) † 1969-12-22 1971-09-17 Kronwitter Wolfram Dish washers - using amylase as cleaning agent
DE2062465B2 (de) † 1970-12-18 1976-11-25 Henkel & Cie GmbH, 4000 Düsseldorf Geschirrspuelmittel
GB1372034A (en) * 1970-12-31 1974-10-30 Unilever Ltd Detergent compositions
US3950277A (en) * 1973-07-25 1976-04-13 The Procter & Gamble Company Laundry pre-soak compositions
US4101457A (en) † 1975-11-28 1978-07-18 The Procter & Gamble Company Enzyme-containing automatic dishwashing composition
DE2727463A1 (de) † 1976-06-24 1978-01-05 Procter & Gamble Reinigungsmittel, das insbesondere zur verwendung in geschirrspuelmaschinen geeignet ist
FI791296A (fi) † 1978-04-21 1979-10-22 Peter Michael John Bedding Foerfaranden och material foer putsning av mjuka kontaktlinser
US4421664A (en) * 1982-06-18 1983-12-20 Economics Laboratory, Inc. Compatible enzyme and oxidant bleaches containing cleaning composition
DK289083A (da) * 1983-06-23 1984-12-24 Novo Industri As Lipase, fremgangsmaade til fremstilling deraf og anvendelse deraf
GB8328075D0 (en) † 1983-10-20 1983-11-23 Unilever Plc Dishwashing compositions
DE3428834A1 (de) † 1984-08-04 1986-02-13 Henkel KGaA, 4000 Düsseldorf Geschirreinigungsmittel
DE3428848A1 (de) † 1984-08-04 1986-02-13 Henkel KGaA, 4000 Düsseldorf Geschirreinigungsmittel
DE3428833A1 (de) † 1984-08-04 1986-02-13 Henkel KGaA, 4000 Düsseldorf Geschirreinigungsmittel
GB8514707D0 (en) * 1985-06-11 1985-07-10 Unilever Plc Enzymatic detergent composition
GB8514708D0 (en) * 1985-06-11 1985-07-10 Unilever Plc Enzymatic detergent composition
DK154572C (da) * 1985-08-07 1989-04-24 Novo Industri As Enzymatisk detergentadditiv, detergent og fremgangsmaade til vask af tekstiler
JPS62129397A (ja) * 1985-11-29 1987-06-11 ライオン株式会社 洗浄剤組成物
JPH0689355B2 (ja) * 1986-05-06 1994-11-09 サンスタ−株式会社 洗浄剤組成物
GB8624050D0 (en) † 1986-10-07 1986-11-12 Unilever Plc Machine dishwashing compositions
JPS6434559A (en) * 1987-07-30 1989-02-06 Seiko Epson Corp Structure for taking out cavity
JPS6434560A (en) * 1987-07-30 1989-02-06 Seiko Epson Corp Die structure

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109563449A (zh) * 2016-06-23 2019-04-02 诺维信公司 酶的用途、组合物以及用于去除污垢的方法

Also Published As

Publication number Publication date
BR8706685A (pt) 1988-07-19
EP0271155A3 (en) 1988-08-17
DE3772726D1 (de) 1991-10-10
EP0271155A2 (de) 1988-06-15
ZA879297B (en) 1989-08-30
AU8222387A (en) 1988-06-16
JPS63161086A (ja) 1988-07-04
GB8629538D0 (en) 1987-01-21
AU609755B2 (en) 1991-05-09
ES2025635T3 (es) 1992-04-01
ES2025635T5 (es) 2001-01-16
EP0271155B2 (de) 2000-09-06

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