EP0065394B1 - Device and process for the production of cheese curd - Google Patents
Device and process for the production of cheese curd Download PDFInfo
- Publication number
- EP0065394B1 EP0065394B1 EP82302338A EP82302338A EP0065394B1 EP 0065394 B1 EP0065394 B1 EP 0065394B1 EP 82302338 A EP82302338 A EP 82302338A EP 82302338 A EP82302338 A EP 82302338A EP 0065394 B1 EP0065394 B1 EP 0065394B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- coagulator
- tube
- feeding
- mixture
- period
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title claims description 52
- 235000013351 cheese Nutrition 0.000 title claims description 51
- 238000004519 manufacturing process Methods 0.000 title claims description 13
- 230000015271 coagulation Effects 0.000 claims description 47
- 238000005345 coagulation Methods 0.000 claims description 47
- 235000013336 milk Nutrition 0.000 claims description 38
- 239000008267 milk Substances 0.000 claims description 38
- 210000004080 milk Anatomy 0.000 claims description 38
- 239000000203 mixture Substances 0.000 claims description 24
- 239000003795 chemical substances by application Substances 0.000 claims description 7
- 238000010438 heat treatment Methods 0.000 claims description 5
- 230000002255 enzymatic effect Effects 0.000 claims description 3
- 239000002535 acidifier Substances 0.000 claims description 2
- 238000009413 insulation Methods 0.000 claims description 2
- 239000007788 liquid Substances 0.000 claims description 2
- 230000000737 periodic effect Effects 0.000 claims 2
- 239000000047 product Substances 0.000 description 23
- 229940108461 rennet Drugs 0.000 description 11
- 108010058314 rennet Proteins 0.000 description 11
- 241000196324 Embryophyta Species 0.000 description 9
- 238000000108 ultra-filtration Methods 0.000 description 8
- 239000012141 concentrate Substances 0.000 description 7
- 238000010924 continuous production Methods 0.000 description 7
- 238000005520 cutting process Methods 0.000 description 6
- 230000000694 effects Effects 0.000 description 5
- 239000002253 acid Substances 0.000 description 4
- 238000002156 mixing Methods 0.000 description 4
- 235000018102 proteins Nutrition 0.000 description 4
- 108090000623 proteins and genes Proteins 0.000 description 4
- 102000004169 proteins and genes Human genes 0.000 description 4
- 239000012465 retentate Substances 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 238000000855 fermentation Methods 0.000 description 3
- 230000004151 fermentation Effects 0.000 description 3
- 239000007858 starting material Substances 0.000 description 3
- GUBGYTABKSRVRQ-QKKXKWKRSA-N Lactose Natural products OC[C@H]1O[C@@H](O[C@H]2[C@H](O)[C@@H](O)C(O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@H]1O GUBGYTABKSRVRQ-QKKXKWKRSA-N 0.000 description 2
- 239000005018 casein Substances 0.000 description 2
- BECPQYXYKAMYBN-UHFFFAOYSA-N casein, tech. Chemical compound NCCCCC(C(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(CC(C)C)N=C(O)C(CCC(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(C(C)O)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(COP(O)(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(N)CC1=CC=CC=C1 BECPQYXYKAMYBN-UHFFFAOYSA-N 0.000 description 2
- 235000021240 caseins Nutrition 0.000 description 2
- 235000013861 fat-free Nutrition 0.000 description 2
- 239000012634 fragment Substances 0.000 description 2
- 230000000977 initiatory effect Effects 0.000 description 2
- 239000008101 lactose Substances 0.000 description 2
- 238000005086 pumping Methods 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 235000019687 Lamb Nutrition 0.000 description 1
- 240000002129 Malva sylvestris Species 0.000 description 1
- 235000006770 Malva sylvestris Nutrition 0.000 description 1
- 239000005862 Whey Substances 0.000 description 1
- 102000007544 Whey Proteins Human genes 0.000 description 1
- 108010046377 Whey Proteins Proteins 0.000 description 1
- 230000001112 coagulating effect Effects 0.000 description 1
- 230000000295 complement effect Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000005189 flocculation Methods 0.000 description 1
- 230000016615 flocculation Effects 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 230000010354 integration Effects 0.000 description 1
- 230000020477 pH reduction Effects 0.000 description 1
- 230000010349 pulsation Effects 0.000 description 1
- 230000006833 reintegration Effects 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 235000020183 skimmed milk Nutrition 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 230000001360 synchronised effect Effects 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C19/00—Cheese; Cheese preparations; Making thereof
- A23C19/02—Making cheese curd
- A23C19/05—Treating milk before coagulation; Separating whey from curd
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01J—MANUFACTURE OF DAIRY PRODUCTS
- A01J25/00—Cheese-making
- A01J25/002—Cheese-making continuously
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C19/00—Cheese; Cheese preparations; Making thereof
- A23C19/02—Making cheese curd
- A23C19/028—Making cheese curd without substantial whey separation from coagulated milk
- A23C19/0285—Making cheese curd without substantial whey separation from coagulated milk by dialysis or ultrafiltration
Definitions
- This invention relates to a process and a device for the production of cheese curd from a liquid milk product, and more specifically for coagulating the milk product during passage through a tubular coagulator after initiation of the so-called 'renneting' procedure.
- the physical-chemical characteristics of the milk product being fed to a coagulator naturally effect on the coagulation process.
- the components of the milk product are mainly coagul- able protein (casein), soluble protein, fat and lactose.
- the fat content seems to have minor effect on the coagulation process.
- DS fat free dry substance content
- the dry substance content has a significant affect on the characteristics of the formed coagulum and is in particular critical to the matter whether the coagulum can be cut and reintegrated.
- the upper limit for obtaining a reintegratable cheese coagulum is in the range of about 14-17%.
- the start product in modern continuous or semi-continuous coagulation methods is not usually milk or skimmed milk as in traditional cheese making, but a milk product with increased casein content.
- the method of obtaining such concentrates does not seem to have any crucial effect on the coagulation process.
- the experiments made in contact with the elaboration of the present invention are based on the concentration by ultra filtration (UF), but other concentration methods can also be used.
- UF ultra filtration
- a UF retentate In comparison with concentrate obtained by evaporation, a UF retentate generally differs in that its lactose concentration and salt concentration remain at about the same level as the corresponding concentrations in the original milk.
- renneting is here used to include coagulation by means of rennet or by means of other enzymatic systems, acid coagulation by acid fermentation or addition of acid and combinations thereof.
- the renneting time that is the period of time between the initiation of the coagulation and the first sign of flocculation, can be regarded as a parameter dependent upon the renneting conditions, and consequently distinguishing the different known coagulation methods in terms of long renneting time and short renneting time can be of help.
- the most important renneting parameters are: Rennet concentration, temperature, pH and salt concentration.
- the renneting time can for example be reduced by: increased temperature; increased amount of rennet; and reduced pH through the addition of fermentation culture or addition of acid.
- One special method of accelerating the renneting process is so-called cold-renneting, in which rennet is admixed with the milk product at a temperature so low that coagulation does not start until the temperature is raised and it then proceeds very rapidly.
- a multi-tube process in which relatively slow coagulation is carried out by the addition of rennet and starter culture just before feeding the mass into the coagulator, is described in the US patent specification 3,899,596 (Stenne).
- a large number of vertical short tubes are filled during a filling period, whereafter the coagulation occurs in stationary state, and during a discharge period the curd is pressed out by means of pistons in upward movement.
- the main drawback of this and other multi-tube methods is the complicated machinery needed for feeding milk product into and discharging and cutting cheese curd from the large number of coagulator tubes required to reach a reasonable plant capacity. Also, the control equipment for coordinating the operation of all these tubes is complicated.
- the American patent 4,131,688 describes a continuous process for cheese coagulation, whereat a relatively slow renneting course is used. To avoid the disruption of formed coagulum through turbulence, a laminar flow through cylinders of the length of about 3 m are prescribed. Besides, special inlet means to effect the flow pattern in the cylinders are used. Even if continuous flow is achieved, the flow is very slow and hence the capacity per cylinder low also.
- the figure 30 I/h is stated, and in such a case a commercial plant of for example 6000 I/h concentrate would require 200 such cylinders. Thus, there is hardly anything gained by the reduced complexity compared with the above mentioned multi-tube plants.
- the object of the present invention is to achieve a cheese coagulation process, which by means of simple equipment makes possible production capacities of industrial scale and which is suitable for use in a continuous cheese manufacturing process.
- a coagulation process in which the milk product is subjected to 'renneting' by the addition of and admixture with an enzymatic agent and/or an acidifying agent and the mixture is introduced into an inlet end of a coagulator tube, transported through the tube under substantially adiabatic conditions and discharged from the tube as a plug of coagulated cheese curd, the process being characterised in that the mixture is fed to the coagulator tube during feeding periods which are spaced apart by stand still periods, each feeding period being of such duration that during said period there is substantially no coagulation of the mixture fed to the tube during said feeding period, and each stand still period being of such a duration that the mixture fed to the tube during the immediately preceding feeding period forms a coagulum sufficiently firm to be transported through the tube as a continuous plug by the mixture fed to the tube during the next feeding period, the residence time for the mixture in the coagulator tube being at least the duration of one feeding period and one stand still period.
- the invention also provides a device for the production of cheese curd by the process of the invention, the device comprising a long coagulator tube of constant cross section having an inlet end and an outlet end, and an arrangement to feed periodically into the inlet end of the coagulator tube a mixture of milk product with a coagulation agent, characterized in that the coagulator tube has a length/diameter ratio greater than 500, and the coagulator tube is enclosed in an envelope provided with insulation or other means to maintain the temperature of the milk product substantially constant during its residence time in the coagulator tube, said temperature being the coagulation temperature obtained through heating the milk product.
- cheese coagulum can be transported through a long coagulator tube with smooth static walls without coagulum disruption if the renneting conditions are so selected that substantially no coagulation occurs during the period when milk product is fed through the inlet of the coagulator and the successive stand still period is so long that all mass downstream of the uncoagulated mass is carried forward as a continuous coagulum plug.
- the process according to the invention can also. be regarded as a combination of the principle of coagulation in a long coagulator tube, in which continuous flow under relatively slow coagulation has been regarded as the natural way of operation, and the multi-tube principle with coagulation under quiescent state, in which rapid coagulation methods have been preferred.
- the period feeding according to the invention enables the use of surprisingly high feed rates without causing coagulum disruption, and flow speeds in the range of 4-20 m/min have proved to be quite realistic. Since this speed exceeds by several times the flow speeds that are possible without coagulum disruption with continuous flow, the stand still periods do not cause any loss in capacity when compared with a corresponding coagulator tube working with a continuous feed, and an overall capacity increase is obtained.
- the required composition of the milk product to be coagulated can be obtained in different ways.
- milk with raised protein concentration is used to reduce the amount of whey that has to be drained if a cheese curd for cutting and reintegration is to be produced, and a milk product with a composition corresponding to the one of finished cheese is used if finished pieces of cheese are to be cut directly from the coagulator.
- the milk can be concentrated with as well as without its fat content.
- fat - for example in the form of cream - can be added after the ultra filtration.
- the UF retentate or - if the fat is added after the ultra filtration - the added fat alone should be subjected to homogenization.
- the renneting condition should be selected not only with respect to the desired cheese characteristics but also so that a sufficient part of the renneting time remains after introduction of the mass into the coagulator tube. Therefore this remaining part of the renneting time should be at least 3 min for a commercial application of the invention, and a total renneting time in the range of 5-20 min is suitable.
- the starting milk product is first brought to renneting temperature, which is in the range of 25-50°C where rennet is used as the main coagulation agent, and rennet and possibly fermentation culture are added in-line immediately before feeding into the coagulator.
- renneting temperature which is in the range of 25-50°C where rennet is used as the main coagulation agent, and rennet and possibly fermentation culture are added in-line immediately before feeding into the coagulator.
- renneting temperature which is in the range of 25-50°C where rennet is used as the main coagulation agent, and rennet and possibly fermentation culture are added in-line immediately before feeding into the coagulator.
- renneting temperature which is in the range of 25-50°C where rennet is used as the main coagulation agent, and rennet and possibly fermentation culture are added in-line immediately before feeding into the coagulator.
- a certain preacidification is compatible with the process of the invention, and can for example be carried out in a storage tank, from which the milk is
- each coagulator tube must contain a considerable volume of cheese curd in order to reach a high plant capacity. Since a tube diameter in the range of 5-15 cm has proved to be satisfactory, very long tubes can be required, and this criterion has surprisingly also proved to be compatible with the inventive process.
- the length/diameter ratio of the coagulator tube may be in excess of 500:1, and preferably in excess of 1000:1.
- the coagulator tube can be spirally wound with uniform curvature, but the radius of curvature should be large enough to produce only a moderate increase in flow resistance.
- the spiral form also facilitates the temperature control of the coagulator tube.
- a constant temperature in the milk mass is preferably maintained, especially during the renneting time, but also during the further transport of the coagulum through the coagulator tube.
- a sufficient temperature control can be obtained by arranging an insulating envelope around the tube spiral.
- the length of the feeding periods and the stand still periods can be varied within relatively wide limits. For optimum conditions the available renneting time should, however, be utilized for the addition of new milk product to the coagulator, and the feeding period is preferably within the range of 0.5-1.2 of the renneting time.
- the stand still periods must be sufficiently long to allow the transformation of the new fed milk product into a coagulum with sufficient cohesive strength to be transported as a plug during the next feed period. Therefore the total duration of a feeding period and a stand still period should be at least 1.5 times the renneting time, and preferably 2-4 times the renneting time.
- the length of the coagulator tube and the feeding rate is adjusted so that the total residence time of the mixture in the coagulator tube forms an integral multiple of the feeding period.
- n (1 + S/T)
- S the length of the stand still period
- T the length of the feeding period
- the number of feeding periods and stand still periods to which the curd is subjected before being discharged from the coagulator tube must be at least one stand still period and one feeding period, but preferably several such periods are used since it has been experienced that long residence times in the coagulator often improve the characteristics of the discharge coagulum having regard to cutting etc.
- a prolongation of the residence time neither requires an increase in the number of coagulator tubes, provided that the corresponding increase of the tube length is not limited, for example, by too large a pumping resistance.
- the capital cost for additional length of tube must be considered low in comparison with installation of further parallel lines including separate equipment for dosing, feeding and cutting etc.
- the coagulator tube was made of stainless steel having a diameter of 78 mm and a length of 350 m and was designed as a spiral with a diameter of about 3 m.
- the tube spiral was built into a heat isolated envelope.
- the milk was pumped into the coagulator for a period of 12 minutes and was kept in quiescent state for 18 minutes after which more milk was pumped again for a period of 12 minutes etc.
- the total residence time in the coagulator was 60 minutes, thus comprising two feeding periods and two stand still periods.
- the continuous coagulum plug discharged during the feeding periods was cut to coagulum fragments of 10 x 10 x 10 mm and was filled into moulds of 290 x 120 x 218 mm.
- the moulds were turned upside-down after 10, 20 and 30 minutes.
- the cheese was left in the moulds during 20 hours at room temperature.
- each cheese was divided into 8 pieces and packed under addition of 4.5 kg salt solution of 15° Be' per 15.8 kg cheese.
- the cheese was stored for two weeks at 5°C.
- the cheese so obtained contained 57.3% water, 17% fat and had a pH of 4.89.
- the cheese exhibited a typical structure and taste of traditional Feta cheese.
- the starting procedure in the beginning of the feeding period sometimes requires that a relatively large initial pump pressure is provided by the feeding device.
- this problem can be overcome by providing the feeding device with means for achieving a controlled gradual increase of the feed rate at an introductory phase of the feeding periods.
- the feeding device is provided with at least one piston pump with a controllable stroke.
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- Chemical & Material Sciences (AREA)
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Description
- This invention relates to a process and a device for the production of cheese curd from a liquid milk product, and more specifically for coagulating the milk product during passage through a tubular coagulator after initiation of the so-called 'renneting' procedure.
- During recent years extensive development has taken place in the mechanisation of cheese manufacture with a view to producing complete continuous processes. New possibilities to produce suitable protein enriched milk products and especially a rapid development within the field of ultra filtration has contributed greatly to the replacement of traditional batch coagulation procedures by a number of more or less continuous coagulation processes including the production of finished cheese direct from the coagulator as well as the production of cheese curd, which after cutting and draining is reintegrated to cheeses of desired shape.
- As an attempt to roughly classify the recently developed methods modifying the coagulation step for continuous processes, on one hand attempts have been made to achieve continuous flowthrough tubular coagulators and on the other hand so called multi-tube processes have been developed, the working principle of which is to fill a large number of parallel, relatively short tube elements, allow the coagulation to occur in quiescent state and press out the cheese curd, whereafter the tubes are refilled.
- The physical-chemical characteristics of the milk product being fed to a coagulator naturally effect on the coagulation process. The components of the milk product are mainly coagul- able protein (casein), soluble protein, fat and lactose. The fat content seems to have minor effect on the coagulation process. In the following reference is made to the fat free dry substance content (DS). The dry substance content has a significant affect on the characteristics of the formed coagulum and is in particular critical to the matter whether the coagulum can be cut and reintegrated. For direct production of finished cheese from a coagulator tube in general there is required at least about 20% fat-free DS, whereas the upper limit for obtaining a reintegratable cheese coagulum is in the range of about 14-17%.
- The start product in modern continuous or semi-continuous coagulation methods is not usually milk or skimmed milk as in traditional cheese making, but a milk product with increased casein content. The method of obtaining such concentrates does not seem to have any crucial effect on the coagulation process. The experiments made in contact with the elaboration of the present invention are based on the concentration by ultra filtration (UF), but other concentration methods can also be used. In comparison with concentrate obtained by evaporation, a UF retentate generally differs in that its lactose concentration and salt concentration remain at about the same level as the corresponding concentrations in the original milk.
- Important parameters for coagulation in coagulatortubes are above all the so called renneting conditions. The term "renneting" is here used to include coagulation by means of rennet or by means of other enzymatic systems, acid coagulation by acid fermentation or addition of acid and combinations thereof. The renneting time, that is the period of time between the initiation of the coagulation and the first sign of flocculation, can be regarded as a parameter dependent upon the renneting conditions, and consequently distinguishing the different known coagulation methods in terms of long renneting time and short renneting time can be of help. The most important renneting parameters are: Rennet concentration, temperature, pH and salt concentration. Thus, the renneting time can for example be reduced by: increased temperature; increased amount of rennet; and reduced pH through the addition of fermentation culture or addition of acid. One special method of accelerating the renneting process is so-called cold-renneting, in which rennet is admixed with the milk product at a temperature so low that coagulation does not start until the temperature is raised and it then proceeds very rapidly.
- A general philosophy adopted in several suggested processes for the adaption of cheese coagulation to enable a continuous process is the use of renneting conditions which provide rapid coagulation. This is far from surprising since a natural approach in exploiting the multi-tube principle as well as continuous coagulation in tubes of limited length would be to assume that a short residence time is necessary to achieve reasonable production rates and process economy.
- One example of such a "fast renneting" process is given in the German patent application 1582979 (Schulz), according to which the milk is first acidified and then brought to coagulate through heating during continuous flow through thin tubes (5-40 mm). The narrow section of the tubes is probably essential to achieve tolerably uniform heating of the cheese curd. Schulz has also suggested a multi-tube process (Milch- wissenschaft 24, 1969) in which each tube is filled with preacidified milk which is coagulated in quiescent state within a few minutes, whereafter the tubes are refilled during simultaneous discharge of finished cheese curd.
- The German patent application 1792264 (Roin- er) describes another fast-renneting method in context with continuous coagulation. To avoid the difficulties in a cold-renneting process of rapidly and uniformly heating the cheese mass to the intended renneting temperature, there is suggested heavy acidification at the renneting temperature before the addition of rennet, after which the coagulation occurs within a period of seconds or some minutes during continuous flow through a coagulator tube.
- The suggested rapid coagulation processes have not resulted in satisfactory industrial applications, and probable reasons thereof are i.a. varying cheese quality due to difficulties to achieve precise and uniform control of the coagulation, and problems caused by precoagulation in the equipment for dosing and heat control.
- A multi-tube process, in which relatively slow coagulation is carried out by the addition of rennet and starter culture just before feeding the mass into the coagulator, is described in the US patent specification 3,899,596 (Stenne). A large number of vertical short tubes are filled during a filling period, whereafter the coagulation occurs in stationary state, and during a discharge period the curd is pressed out by means of pistons in upward movement. The main drawback of this and other multi-tube methods is the complicated machinery needed for feeding milk product into and discharging and cutting cheese curd from the large number of coagulator tubes required to reach a reasonable plant capacity. Also, the control equipment for coordinating the operation of all these tubes is complicated. The complexity of such multi-tube plants is exemplified by French patent application 2 340 041, having the same inventor as the above mentioned US patent, 30-40 different tubes being mounted like spokes in a wheel-like, rotatable device, and through rotating this device the tubes are successively brought to pass filling and discharge stations.
- It is obvious that the main aim within the field of continuous cheese coagulation is to succeed in pumping the start product under coagulation through one single tube or a small number of coagulator tubes at a capacity acceptable for industrial use.
- The American patent 4,131,688 describes a continuous process for cheese coagulation, whereat a relatively slow renneting course is used. To avoid the disruption of formed coagulum through turbulence, a laminar flow through cylinders of the length of about 3 m are prescribed. Besides, special inlet means to effect the flow pattern in the cylinders are used. Even if continuous flow is achieved, the flow is very slow and hence the capacity per cylinder low also. The figure 30 I/h is stated, and in such a case a commercial plant of for example 6000 I/h concentrate would require 200 such cylinders. Thus, there is hardly anything gained by the reduced complexity compared with the above mentioned multi-tube plants.
- A very special continuous coagulation method is described in the British patent specification 1 410 289 (Stenne). UF-retentate is continuously pumped through a long (20 m) coagulator tube (d = 100 mm). To avoid the adherence of coagulated cheese curd along the tube walls, the walls of the coagulator must be flexible so as to be deformed by means of a pulsation effect imposed to the retentate pumped into the tube. The need for such wall deformations indicates that continuous coagulation in tubes with stiff walls results in that the formed coagulum is broken by cheese curd adhering on the tube walls. Further. also this process seems to be restricted in that the flow velocity cannot be increased over a certain limit due to the risk of coagulum disruption through turbulence. The examples indicate that the velocity through the coagulator should be in the range of 1-2 m/min.
- The object of the present invention is to achieve a cheese coagulation process, which by means of simple equipment makes possible production capacities of industrial scale and which is suitable for use in a continuous cheese manufacturing process.
- According to the invention there is provided a coagulation process in which the milk product is subjected to 'renneting' by the addition of and admixture with an enzymatic agent and/or an acidifying agent and the mixture is introduced into an inlet end of a coagulator tube, transported through the tube under substantially adiabatic conditions and discharged from the tube as a plug of coagulated cheese curd, the process being characterised in that the mixture is fed to the coagulator tube during feeding periods which are spaced apart by stand still periods, each feeding period being of such duration that during said period there is substantially no coagulation of the mixture fed to the tube during said feeding period, and each stand still period being of such a duration that the mixture fed to the tube during the immediately preceding feeding period forms a coagulum sufficiently firm to be transported through the tube as a continuous plug by the mixture fed to the tube during the next feeding period, the residence time for the mixture in the coagulator tube being at least the duration of one feeding period and one stand still period.
- The invention also provides a device for the production of cheese curd by the process of the invention, the device comprising a long coagulator tube of constant cross section having an inlet end and an outlet end, and an arrangement to feed periodically into the inlet end of the coagulator tube a mixture of milk product with a coagulation agent, characterized in that the coagulator tube has a length/diameter ratio greater than 500, and the coagulator tube is enclosed in an envelope provided with insulation or other means to maintain the temperature of the milk product substantially constant during its residence time in the coagulator tube, said temperature being the coagulation temperature obtained through heating the milk product. It has been surprisingly found, that cheese coagulum can be transported through a long coagulator tube with smooth static walls without coagulum disruption if the renneting conditions are so selected that substantially no coagulation occurs during the period when milk product is fed through the inlet of the coagulator and the successive stand still period is so long that all mass downstream of the uncoagulated mass is carried forward as a continuous coagulum plug. The process according to the invention can also. be regarded as a combination of the principle of coagulation in a long coagulator tube, in which continuous flow under relatively slow coagulation has been regarded as the natural way of operation, and the multi-tube principle with coagulation under quiescent state, in which rapid coagulation methods have been preferred. By this combination several surprising results and possibilities have been achieved: besides the fact that an acceptable solution has been given to the problem of curd adhesion to stationary tube walls, the object of providing high flow through a small number of coagulator tubes has been reached. Thus, the period feeding according to the invention enables the use of surprisingly high feed rates without causing coagulum disruption, and flow speeds in the range of 4-20 m/min have proved to be quite realistic. Since this speed exceeds by several times the flow speeds that are possible without coagulum disruption with continuous flow, the stand still periods do not cause any loss in capacity when compared with a corresponding coagulator tube working with a continuous feed, and an overall capacity increase is obtained. As an example of said capacity it may be noted that when cheese curd is produced in a coagulator tube as described in the detailed Example given below with stand still periods of twice the duration of the feeding periods, meaning that three parallel coagulator tubes will enable continuous production, a capacity of 4.000 lit cheese curd per hour is obtained. In a preferred process according to the invention adapted to provide continuous production the milk product after addition of coagulation agent in a dosing plant is fed continuously to a coagulator comprising several coagulatortubes, the coagulator tubes being alternately connected with and disconnected from the dosing plant so that the mixture is continuously fed from the dosing plant to the tubes, and each coagulator tube being connected with and disconnected from the dosing plant during periods corresponding to said feeding periods and stand still periods, respectively.
- As mentioned above, the required composition of the milk product to be coagulated can be obtained in different ways. Preferably milk with raised protein concentration is used to reduce the amount of whey that has to be drained if a cheese curd for cutting and reintegration is to be produced, and a milk product with a composition corresponding to the one of finished cheese is used if finished pieces of cheese are to be cut directly from the coagulator. By modern ultra filtration technique the milk can be concentrated with as well as without its fat content. In the latter case fat - for example in the form of cream - can be added after the ultra filtration. In order to reduce the fat losses in connection with the draining procedure, the UF retentate or - if the fat is added after the ultra filtration - the added fat alone should be subjected to homogenization.
- Since the process according to the invention is based on coagulation in a small number of long coagulated tubes and relatively slow renneting, the renneting condition should be selected not only with respect to the desired cheese characteristics but also so that a sufficient part of the renneting time remains after introduction of the mass into the coagulator tube. Therefore this remaining part of the renneting time should be at least 3 min for a commercial application of the invention, and a total renneting time in the range of 5-20 min is suitable. According to a preferred embodiment of the invention the starting milk product is first brought to renneting temperature, which is in the range of 25-50°C where rennet is used as the main coagulation agent, and rennet and possibly fermentation culture are added in-line immediately before feeding into the coagulator. However, a certain preacidification is compatible with the process of the invention, and can for example be carried out in a storage tank, from which the milk is pumped to the coagulator with rennet addition and with possible control of the renneting temperature. The dosing of rennet and possible starter culture may be carried out in-line by means of dosing pumps which are synchronized with the feed pump for feeding the milk mass into the coagulator tube. Such equipment is well known to those skilled in the art.
- From the combination of slow coagulation with a simple coagulator unit comprising only a few coagulator tubes it follows that each coagulator tube must contain a considerable volume of cheese curd in order to reach a high plant capacity. Since a tube diameter in the range of 5-15 cm has proved to be satisfactory, very long tubes can be required, and this criterion has surprisingly also proved to be compatible with the inventive process. The length/diameter ratio of the coagulator tube may be in excess of 500:1, and preferably in excess of 1000:1. To provide a compact coagulator unit, the coagulator tube can be spirally wound with uniform curvature, but the radius of curvature should be large enough to produce only a moderate increase in flow resistance. The spiral form also facilitates the temperature control of the coagulator tube. In the process of the invention a constant temperature in the milk mass is preferably maintained, especially during the renneting time, but also during the further transport of the coagulum through the coagulator tube. For practical use a sufficient temperature control can be obtained by arranging an insulating envelope around the tube spiral.
- The length of the feeding periods and the stand still periods can be varied within relatively wide limits. For optimum conditions the available renneting time should, however, be utilized for the addition of new milk product to the coagulator, and the feeding period is preferably within the range of 0.5-1.2 of the renneting time. The stand still periods must be sufficiently long to allow the transformation of the new fed milk product into a coagulum with sufficient cohesive strength to be transported as a plug during the next feed period. Therefore the total duration of a feeding period and a stand still period should be at least 1.5 times the renneting time, and preferably 2-4 times the renneting time. The length of the coagulator tube and the feeding rate is adjusted so that the total residence time of the mixture in the coagulator tube forms an integral multiple of the feeding period. The mutual ratio between the length of a feeding period and a stand still period gives directly the minimum number of coagulator tubes required for continuous production of cheese curd. Mathematically the number of simultaneously operated coagulator tubes in a coagulator unit may be expressed as n (1 + S/T), where n is the number of simultaneously fed coagulator tubes, S the length of the stand still period and T the length of the feeding period.
- The number of feeding periods and stand still periods to which the curd is subjected before being discharged from the coagulator tube must be at least one stand still period and one feeding period, but preferably several such periods are used since it has been experienced that long residence times in the coagulator often improve the characteristics of the discharge coagulum having regard to cutting etc. A prolongation of the residence time neither requires an increase in the number of coagulator tubes, provided that the corresponding increase of the tube length is not limited, for example, by too large a pumping resistance. The capital cost for additional length of tube must be considered low in comparison with installation of further parallel lines including separate equipment for dosing, feeding and cutting etc.
- The further treatment of the cheese curd after it is discharged as a plug from one or several coagulator tubes does not fall within the scope of the present invention. Different methods to cut the cheese curd by means of cutting devices directly applied to the outlet of the coagulator to cut the cheese curd into cheese fragments as well as finished pieces of cheese are known. It is however obvious, that the present process, which permits continuous discharge of cheese curd to high capacity from a small number of coagulator tubes, is extremely practical for integration in an entirely continuous cheese process for the production of various cheese products.
- 64.000 I milk containing 2.95% fat was pasteurized at 80°C during 15 sec and cooled to 50°C. The product was ultra filtrated to a dry substance concentration (TS) of 27%. The concentrate was heated at 78°C during 30 sec, homogenized at 75 bar and 56°C and conveyed under cooling to a mixing tank. To the tank was also added complementary colour and 0.006% lamb lipas (Chr. Hansen). From the mixing tank 4.100 I/h concentrate was pumped under in-line mixing with 1.5% starter culture of single strain type followed by also in-line mixing of rennet solution with strength 1:100 in an amount of 7% with respect to concentrate, whereafter the renneted concentrate of 33°C was fed directly into a coagulator tube. The coagulator tube was made of stainless steel having a diameter of 78 mm and a length of 350 m and was designed as a spiral with a diameter of about 3 m. The tube spiral was built into a heat isolated envelope. The milk was pumped into the coagulator for a period of 12 minutes and was kept in quiescent state for 18 minutes after which more milk was pumped again for a period of 12 minutes etc. The total residence time in the coagulator was 60 minutes, thus comprising two feeding periods and two stand still periods.
- The continuous coagulum plug discharged during the feeding periods was cut to coagulum fragments of 10 x 10 x 10 mm and was filled into moulds of 290 x 120 x 218 mm. The moulds were turned upside-down after 10, 20 and 30 minutes. The cheese was left in the moulds during 20 hours at room temperature. Then each cheese was divided into 8 pieces and packed under addition of 4.5 kg salt solution of 15° Be' per 15.8 kg cheese. The cheese was stored for two weeks at 5°C. The cheese so obtained contained 57.3% water, 17% fat and had a pH of 4.89. The cheese exhibited a typical structure and taste of traditional Feta cheese.
- The starting procedure in the beginning of the feeding period sometimes requires that a relatively large initial pump pressure is provided by the feeding device. According to a preferred embodiment of the feeding device, however, this problem can be overcome by providing the feeding device with means for achieving a controlled gradual increase of the feed rate at an introductory phase of the feeding periods. Preferably, the feeding device is provided with at least one piston pump with a controllable stroke.
Claims (12)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
SE8103062A SE427407B (en) | 1981-05-15 | 1981-05-15 | PROCEDURE AND APPARATUS FOR CREAM PREPARATION |
SE8103062 | 1981-05-15 |
Publications (3)
Publication Number | Publication Date |
---|---|
EP0065394A2 EP0065394A2 (en) | 1982-11-24 |
EP0065394A3 EP0065394A3 (en) | 1984-05-02 |
EP0065394B1 true EP0065394B1 (en) | 1986-09-24 |
Family
ID=20343843
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP82302338A Expired EP0065394B1 (en) | 1981-05-15 | 1982-05-07 | Device and process for the production of cheese curd |
Country Status (9)
Country | Link |
---|---|
US (1) | US4499109A (en) |
EP (1) | EP0065394B1 (en) |
AU (1) | AU532159B2 (en) |
CA (1) | CA1199519A (en) |
DE (1) | DE3273411D1 (en) |
DK (1) | DK158120C (en) |
IE (1) | IE52819B1 (en) |
NZ (1) | NZ200488A (en) |
SE (1) | SE427407B (en) |
Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
NZ211254A (en) * | 1984-03-06 | 1988-03-30 | Commw Of Australia | Continuous production of cheese from milk retentate |
DK167168B1 (en) * | 1989-07-13 | 1993-09-13 | Md Foods Amba | PROCEDURE FOR CONTINUOUS PRODUCTION OF COTTAGE CHEESE FROM ULTRAFILTERED MILK |
EP0695124A1 (en) * | 1993-04-27 | 1996-02-07 | Unilever N.V. | Cast cheese and a method of producing |
ES2286130T3 (en) * | 2001-07-06 | 2007-12-01 | Emmi Schweiz Ag | PROCEDURE AND DEVICE FOR PRODUCING CONTINUOUSLY AND QUICKLY PROTEIN GEL SYSTEMS, ESPECIALLY MILK-BASED GEL SYSTEMS IN CHEESE PRODUCTION OR CHEESE TYPE. |
US6982100B2 (en) * | 2002-08-02 | 2006-01-03 | Land O'lakes, Inc. | Method for cheese manufacture |
US6902750B2 (en) * | 2002-08-02 | 2005-06-07 | Land O'lakes, Inc. | Method for the manufacture of process cheese |
NZ551402A (en) * | 2006-11-20 | 2009-02-28 | Fonterra Co Operative Group | Process for producing cheese comprising passing starting milk and an enzyme capable of converting kappa casein into para-kappa casein through a flow device |
DK178034B1 (en) * | 2014-01-24 | 2015-03-30 | Jh Consulting V Jørgen Henriksen | Production of acidified white cheese |
Family Cites Families (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2781269A (en) * | 1955-06-30 | 1957-02-12 | Univ Ohio State Res Found | Method and apparatus for the continuous production of cheese-forming curd |
US2908575A (en) * | 1956-03-27 | 1959-10-13 | Nat Dairy Prod Corp | Method and apparatus for the continuous production of cheese curd |
GB1206011A (en) * | 1967-01-03 | 1970-09-23 | Alfa Laval Ab | Improvements in methods of and apparatus for the continuous production of cheese curd |
FR2256718B2 (en) * | 1972-09-04 | 1981-08-28 | Nestle Sa Soc Ass Tech Prod | |
CH584514A5 (en) * | 1973-04-16 | 1977-02-15 | Claudel Sa | |
DE2351371A1 (en) * | 1973-10-12 | 1975-09-04 | Alpma Alpenland Masch | METHOD AND DEVICE FOR MAKING CHEESE |
US3985622A (en) * | 1975-01-30 | 1976-10-12 | Phillips Petroleum Company | Method and apparatus for conducting fermentation |
FR2326150A1 (en) * | 1975-10-03 | 1977-04-29 | Agronomique Inst Nat Rech | PROCESS AND DEVICE FOR THE CONTINUOUS MANUFACTURING OF CHEESES |
-
1981
- 1981-05-15 SE SE8103062A patent/SE427407B/en not_active IP Right Cessation
-
1982
- 1982-04-28 CA CA000401856A patent/CA1199519A/en not_active Expired
- 1982-04-30 NZ NZ200488A patent/NZ200488A/en unknown
- 1982-05-04 IE IE1055/82A patent/IE52819B1/en not_active IP Right Cessation
- 1982-05-07 EP EP82302338A patent/EP0065394B1/en not_active Expired
- 1982-05-07 DE DE8282302338T patent/DE3273411D1/en not_active Expired
- 1982-05-13 DK DK216182A patent/DK158120C/en not_active IP Right Cessation
- 1982-05-14 AU AU83727/82A patent/AU532159B2/en not_active Ceased
- 1982-05-17 US US06/379,092 patent/US4499109A/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
US4499109A (en) | 1985-02-12 |
IE52819B1 (en) | 1988-03-16 |
EP0065394A2 (en) | 1982-11-24 |
DK158120C (en) | 1990-08-27 |
SE427407B (en) | 1983-04-11 |
DK158120B (en) | 1990-04-02 |
AU532159B2 (en) | 1983-09-22 |
DK216182A (en) | 1982-11-16 |
DE3273411D1 (en) | 1986-10-30 |
CA1199519A (en) | 1986-01-21 |
NZ200488A (en) | 1985-07-12 |
AU8372782A (en) | 1982-11-18 |
IE821055L (en) | 1982-11-15 |
EP0065394A3 (en) | 1984-05-02 |
SE8103062L (en) | 1982-11-16 |
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