DK3307675T3 - Multi-tryk-fremgangsmåde til fremstilling af ammoniak - Google Patents

Multi-tryk-fremgangsmåde til fremstilling af ammoniak Download PDF

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Publication number
DK3307675T3
DK3307675T3 DK16729238.2T DK16729238T DK3307675T3 DK 3307675 T3 DK3307675 T3 DK 3307675T3 DK 16729238 T DK16729238 T DK 16729238T DK 3307675 T3 DK3307675 T3 DK 3307675T3
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ammonia
preparation
pressure process
pressure
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DK16729238.2T
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English (en)
Inventor
Evgeni Gorval
Reinhard Heun
Joachim Johanning
Klaus Nölker
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Thyssenkrupp Ind Solutions Ag
Thyssenkrupp Ag
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    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01CAMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00Ammonia; Compounds thereof
    • C01C1/02Preparation, purification or separation of ammonia
    • C01C1/04Preparation of ammonia by synthesis in the gas phase
    • C01C1/0405Preparation of ammonia by synthesis in the gas phase from N2 and H2 in presence of a catalyst
    • C01C1/0458Separation of NH3
    • C01C1/047Separation of NH3 by condensation
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/02Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
    • C01B3/025Preparation or purification of gas mixtures for ammonia synthesis
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01CAMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00Ammonia; Compounds thereof
    • C01C1/02Preparation, purification or separation of ammonia
    • C01C1/04Preparation of ammonia by synthesis in the gas phase
    • C01C1/0405Preparation of ammonia by synthesis in the gas phase from N2 and H2 in presence of a catalyst
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01CAMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00Ammonia; Compounds thereof
    • C01C1/02Preparation, purification or separation of ammonia
    • C01C1/04Preparation of ammonia by synthesis in the gas phase
    • C01C1/0405Preparation of ammonia by synthesis in the gas phase from N2 and H2 in presence of a catalyst
    • C01C1/0488Processes integrated with preparations of other compounds, e.g. methanol, urea or with processes for power generation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C1/00Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon
    • C07C1/02Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon from oxides of a carbon
    • C07C1/04Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon from oxides of a carbon from carbon monoxide with hydrogen
    • C07C1/0485Set-up of reactors or accessories; Multi-step processes
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C1/00Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon
    • C07C1/02Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon from oxides of a carbon
    • C07C1/12Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon from oxides of a carbon from carbon dioxide with hydrogen
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C273/00Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C273/02Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
    • C07C273/04Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds from carbon dioxide and ammonia
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/02Processes for making hydrogen or synthesis gas
    • C01B2203/0205Processes for making hydrogen or synthesis gas containing a reforming step
    • C01B2203/0227Processes for making hydrogen or synthesis gas containing a reforming step containing a catalytic reforming step
    • C01B2203/0244Processes for making hydrogen or synthesis gas containing a reforming step containing a catalytic reforming step the reforming step being an autothermal reforming step, e.g. secondary reforming processes
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/02Processes for making hydrogen or synthesis gas
    • C01B2203/0283Processes for making hydrogen or synthesis gas containing a CO-shift step, i.e. a water gas shift step
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0415Purification by absorption in liquids
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0435Catalytic purification
    • C01B2203/0445Selective methanation
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/046Purification by cryogenic separation
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465Composition of the impurity
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465Composition of the impurity
    • C01B2203/047Composition of the impurity the impurity being carbon monoxide
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465Composition of the impurity
    • C01B2203/0475Composition of the impurity the impurity being carbon dioxide
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465Composition of the impurity
    • C01B2203/048Composition of the impurity the impurity being an organic compound
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465Composition of the impurity
    • C01B2203/0495Composition of the impurity the impurity being water
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/06Integration with other chemical processes
    • C01B2203/068Ammonia synthesis
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/14Details of the flowsheet
    • C01B2203/146At least two purification steps in series
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/52Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
DK16729238.2T 2015-06-12 2016-06-09 Multi-tryk-fremgangsmåde til fremstilling af ammoniak DK3307675T3 (da)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102015210801.5A DE102015210801A1 (de) 2015-06-12 2015-06-12 Mehrdruckverfahren zur Herstellung von Ammoniak ohne Anreicherung von Inertgas
PCT/EP2016/063089 WO2016198488A1 (de) 2015-06-12 2016-06-09 Mehrdruckverfahren zur herstellung von ammoniak

Publications (1)

Publication Number Publication Date
DK3307675T3 true DK3307675T3 (da) 2020-02-03

Family

ID=56116433

Family Applications (2)

Application Number Title Priority Date Filing Date
DK16728011.4T DK3307681T3 (da) 2015-06-12 2016-06-09 Flertryksproces til produktion af ammoniak
DK16729238.2T DK3307675T3 (da) 2015-06-12 2016-06-09 Multi-tryk-fremgangsmåde til fremstilling af ammoniak

Family Applications Before (1)

Application Number Title Priority Date Filing Date
DK16728011.4T DK3307681T3 (da) 2015-06-12 2016-06-09 Flertryksproces til produktion af ammoniak

Country Status (6)

Country Link
US (1) US20200039831A1 (da)
EP (2) EP3307675B1 (da)
JP (1) JP6503479B2 (da)
DE (1) DE102015210801A1 (da)
DK (2) DK3307681T3 (da)
WO (2) WO2016198487A1 (da)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2017102206A1 (en) * 2015-12-16 2017-06-22 Haldor Topsøe A/S A process for production of ammonia from inert-free synthesis gas in multiple reaction systems
DE102016122374A1 (de) * 2016-11-21 2018-05-24 Thyssenkrupp Ag Vollintegrierter Ammoniak-Harnstoff-Komplex
DE102017204208A1 (de) 2017-03-14 2018-09-20 Thyssenkrupp Ag Verfahren und Anlage zur Erzeugung und Aufbereitung eines Synthesegasgemisches
DK3401280T3 (da) 2017-05-11 2022-03-21 Gascontec Gmbh Fremgangsmåde til fremstilling af ammoniak
EP3401299B1 (de) 2017-05-12 2021-11-03 L'air Liquide, Société Anonyme Pour L'Étude Et L'exploitation Des Procédés Georges Claude Reaktor zum durchführen exothermer gleichgewichtsreaktionen
DE102018210921A1 (de) 2018-07-03 2019-08-14 Thyssenkrupp Ag Vermeidung von VOC und HAP Emissionen aus dem Entgaser von Synthesegas verarbeitenden Anlagen
DE102018117657A1 (de) 2018-07-20 2020-01-23 Thyssenkrupp Ag Verfahren und Vorrichtung zur Herstellung von Ammoniak oder Wasserstoff und Verwendung der Vorrichtung
DE102018117654A1 (de) 2018-07-20 2019-10-17 Thyssenkrupp Ag Vorrichtung mit einem Dampfreformer, Verfahren unter Verwendung der Vorrichtung und eine entsprechende Verwendung der Vorrichtung
EP3715320A1 (en) * 2019-03-27 2020-09-30 Siemens Aktiengesellschaft Method for generating a gas-product
KR102384194B1 (ko) * 2021-10-07 2022-04-08 박수경 모듈화가 가능한 암모니아 생성 시스템

Family Cites Families (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3442613A (en) 1965-10-22 1969-05-06 Braun & Co C F Hydrocarbon reforming for production of a synthesis gas from which ammonia can be prepared
DE3047257A1 (de) * 1980-12-16 1982-07-08 Didier Engineering Gmbh, 4300 Essen Verfahren zur erzeugung von ammoniak-synthesegas
DD225029A3 (de) 1982-12-10 1985-07-17 Bendix Horst Dieter Verfahren zur energetisch guenstigen synthese von ammoniak
US4578214A (en) 1984-02-06 1986-03-25 C F Braun & Co. Process for ammonia syngas manufacture
GB2186870A (en) * 1986-02-26 1987-08-26 Foster Wheeler Energy Ltd Ammonia synthesis
DE4304567C1 (de) * 1993-02-16 1994-04-28 Uhde Gmbh Verfahren zur Dampferzeugung bei der katalytischen heterogenen Synthese und Vorrichtung zur Durchführung dieses Verfahrens
DE10055818A1 (de) 2000-11-10 2002-05-23 Ammonia Casale Sa Verfahren zum Herstellen von Ammoniak aus einem Stickstoff-Wasserstoff-Gemisch aus Erdgas
DE10057863C2 (de) * 2000-11-21 2002-10-24 Uhde Gmbh Mehrdruckverfahren zur Herstellung von Ammoniak
US7090816B2 (en) 2003-07-17 2006-08-15 Kellogg Brown & Root Llc Low-delta P purifier for nitrogen, methane, and argon removal from syngas
DE102004028200B3 (de) * 2004-05-28 2005-12-15 Hippweb E.K. Verfahren zur Durchführung heterogen katalytischer exothermer Gasphasenreaktionen für die Methanolsynthese
EP2172417A1 (en) 2008-10-02 2010-04-07 Ammonia Casale S.A. Process for the production of ammonia synthesis gas
JP5355062B2 (ja) * 2008-12-15 2013-11-27 東洋エンジニアリング株式会社 メタノール及びアンモニアの併産方法
EP2301886A1 (en) * 2009-09-03 2011-03-30 Ammonia Casale S.A. Waste heat recovery in a chemical process and plant, particularly for the synthesis of ammonia
US8889093B2 (en) * 2010-09-16 2014-11-18 Kellogg Brown & Root Llc High pressure cyrogenic process and system for producing ammonia products
DE102011016759A1 (de) * 2011-04-12 2012-10-18 Thyssenkrupp Uhde Gmbh Verfahren zur Herstellung von NH3
US9643856B2 (en) 2013-08-07 2017-05-09 Kellogg Brown+Root LLC Methods and systems for making ammonia in a double ammonia converter system

Also Published As

Publication number Publication date
EP3307675B1 (de) 2019-10-30
JP2018518446A (ja) 2018-07-12
EP3307681A1 (de) 2018-04-18
US20200039831A1 (en) 2020-02-06
EP3307681B1 (de) 2019-04-17
JP6503479B2 (ja) 2019-04-17
DK3307681T3 (da) 2019-06-24
EP3307675A1 (de) 2018-04-18
WO2016198487A1 (de) 2016-12-15
WO2016198488A1 (de) 2016-12-15
DE102015210801A1 (de) 2016-12-15

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