DE729723C - Black for post-treatment of phosphate surface layers - Google Patents

Black for post-treatment of phosphate surface layers

Info

Publication number
DE729723C
DE729723C DEM145259D DEM0145259D DE729723C DE 729723 C DE729723 C DE 729723C DE M145259 D DEM145259 D DE M145259D DE M0145259 D DEM0145259 D DE M0145259D DE 729723 C DE729723 C DE 729723C
Authority
DE
Germany
Prior art keywords
black
surface layers
post
treatment
phosphate surface
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
DEM145259D
Other languages
German (de)
Inventor
Dr Ludwig Schuster
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
GEA Group AG
Original Assignee
Metallgesellschaft AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Metallgesellschaft AG filed Critical Metallgesellschaft AG
Priority to DEM145259D priority Critical patent/DE729723C/en
Application granted granted Critical
Publication of DE729723C publication Critical patent/DE729723C/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/82After-treatment
    • C23C22/84Dyeing

Landscapes

  • Chemical & Material Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Chemical Treatment Of Metals (AREA)

Description

Schwärze zur Nachbehandlung von Phosphatoberflächenschichten Es ist bekannt, Phosphatschichten, die zur Verbesserung des Korrosionsschutzes auf Metallen, insbesondere Eisen, erzeugt sind, einzuschwärzen. Die hierfür bisher verwendeten Schwärzen zeigen jedoch bei einer derartigen Nachbehandlung von Phosphatschichten gewisse Nachteile. Sie ziehen z. B. nicht immer gleichmäßig auf den P'hosphatschichten auf. Außerdem sind sic noch nicht allen Anforderungen in bezug auf Abrieb-, Öl- und Wasserfestigkeit gewachsen.Blackness for post-treatment of phosphate surface layers It is known, phosphate layers that improve the corrosion protection on metals, in particular iron, are produced to be blackened. The ones previously used for this However, they show blackening with such an aftertreatment of phosphate layers certain disadvantages. You pull z. B. not always evenly on the phosphate layers on. In addition, they have not yet met all of the requirements relating to abrasion, oil and water resistance.

Gegenstand der Erfindung ist -nun eine Schwärze zur Nachbehandlung von Phosphatoberflächenschichten, mit Hilfe deren erhebliche Verbesserungen in bezug auf die obengenannten Nachteile erzielt werden.The subject of the invention is now a blackness for aftertreatment of phosphate surface layers, with the help of their considerable improvements in relation to on the above disadvantages can be achieved.

Die Schwärze besteht aus einem Lösungsgemisch von Trichloräthylen und Sprit in Mengen von zusammen etwa 9o bis 95%, einem echt löslichen schwarzen organischem Farbstoff in Mengen von 2 bis 4a/o und einem Gemisch von Polyvinylacetat und Kunstschellack in Mengen von insgesamt 3 bis 6%, vorzugsweise 4 bis 5%.The blackness consists of a mixed solution of trichlorethylene and fuel in amounts totaling about 90 to 95%, a truly soluble black organic dye in amounts of 2 to 4 a / o and a mixture of polyvinyl acetate and artificial shellac in amounts totaling 3 to 6%, preferably 4 to 5%.

Das Verhältnis von Trichloräthvlen und Sprit zueinander soll dabei innerhalb von 5 : I bis io : I liegen, es beträgt vorzugsweise 9 : I .The ratio of Trichloräthvlen and fuel to each other should be are within 5: I to 10: I, it is preferably 9: I.

Die Schwärze gemäß Erfindung zieht der p'hosphatierten Oberfläche vollkommen gleichmäßig auf, zeigt ein intensives lackähnliches Schwarz und hat gute Abrieb-, Öl- und Wasserfestigkeit.The blackness according to the invention pulls the phosphated surface completely evenly, shows an intense lacquer-like black and has good Abrasion, oil and water resistance.

Als Beispiel sei folgende Zusammensetzung genannt: 82,6% Trichloräfhylen, 3,70/0 Polyvinylacetat, 3,o 0,'o spritlösliches Nigr osinschwarz, ,9, 2 % Sprit, I, 5 0`0, Kunstschellack KR.The following composition is mentioned as an example: 82.6% trichlorethylene, 3.70 / 0 polyvinyl acetate, 3, o 0, 'o fuel-soluble nigr osin black,, 9, 2% fuel, I, 5 0`0, artificial shellac KR.

Claims (1)

PATENTANSPRUCII Schwärze zur Nachbehandlung von Phosphatoberflächenschichten, dadurch gekennzeichnet, daß sie aus einem Lösungsgemisch von Trichloräthylen und Sprit in Mengen von zusammen etwa 9o bis 950'o, einem echt löslichen schwarzen organischen Farbstoff in Mengen von 2 bis 40'c, und einem Gemisch von Polyvinylacetat und Kunstschellack in Mengen von insgesamt 3 bis 6%, vorzugsweise 4 bis 50;o,, besteht.PATENT APPLICATION Blackness for the aftertreatment of phosphate surface layers, characterized in that it consists of a mixed solution of trichlorethylene and Fuel in amounts of about 9o to 950'o together, a real soluble black organic Dye in amounts from 2 to 40'c, and a mixture of polyvinyl acetate and artificial shellac in amounts totaling from 3 to 6%, preferably from 4 to 50%.
DEM145259D 1939-06-06 1939-06-06 Black for post-treatment of phosphate surface layers Expired DE729723C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
DEM145259D DE729723C (en) 1939-06-06 1939-06-06 Black for post-treatment of phosphate surface layers

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DEM145259D DE729723C (en) 1939-06-06 1939-06-06 Black for post-treatment of phosphate surface layers

Publications (1)

Publication Number Publication Date
DE729723C true DE729723C (en) 1942-12-22

Family

ID=7335745

Family Applications (1)

Application Number Title Priority Date Filing Date
DEM145259D Expired DE729723C (en) 1939-06-06 1939-06-06 Black for post-treatment of phosphate surface layers

Country Status (1)

Country Link
DE (1) DE729723C (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2378828A1 (en) * 1977-01-28 1978-08-25 Parker Ste Continentale BLACK COLORING COMPOSITION AND ITS APPLICATION TO THE TREATMENT OF METAL PARTS
DE10014035A1 (en) * 2000-03-22 2001-10-04 Electro Chem Eng Gmbh Colored conversion layer

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2378828A1 (en) * 1977-01-28 1978-08-25 Parker Ste Continentale BLACK COLORING COMPOSITION AND ITS APPLICATION TO THE TREATMENT OF METAL PARTS
DE10014035A1 (en) * 2000-03-22 2001-10-04 Electro Chem Eng Gmbh Colored conversion layer
DE10014035B4 (en) * 2000-03-22 2006-07-13 Electro Chemical Engineering Gmbh Colored conversion layer, a solution for their preparation and their use

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