DE69114610T2 - Herstellung von n-phosphonomethylglyzin durch oxydation von n-phosphonomethyliminodiessigsäure. - Google Patents

Herstellung von n-phosphonomethylglyzin durch oxydation von n-phosphonomethyliminodiessigsäure.

Info

Publication number: DE69114610T2
Authority: DE; Germany
Prior art keywords: phosphonomethylglyzine; oxydation; production; phosphonomethyliminodiacetic acid; phosphonomethyliminodiacetic
Prior art date: 1990-03-12
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired - Fee Related

Application number

DE69114610T

Other languages

English (en)

Other versions

DE69114610D1 (de

Inventor

Ramon Juan Martin

Madronero Julio Munoz

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Monsanto Co

Original Assignee

Monsanto Co

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1990-03-12

Filing date

1991-03-12

Publication date

1996-05-02

1991-03-12 Application filed by Monsanto Co filed Critical Monsanto Co

1995-12-21 Publication of DE69114610D1 publication Critical patent/DE69114610D1/de

1996-05-02 Application granted granted Critical

1996-05-02 Publication of DE69114610T2 publication Critical patent/DE69114610T2/de

2011-03-13 Anticipated expiration legal-status Critical

Status Expired - Fee Related legal-status Critical Current

Links

AZIHIQIVLANVKD-UHFFFAOYSA-N N-(phosphonomethyl)iminodiacetic acid Chemical compound OC(=O)CN(CC(O)=O)CP(O)(O)=O AZIHIQIVLANVKD-UHFFFAOYSA-N 0.000 title 1
238000007254 oxidation reaction Methods 0.000 title 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
- C07F9/3804—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)] not used, see subgroups
- C07F9/3808—Acyclic saturated acids which can have further substituents on alkyl
- C07F9/3813—N-Phosphonomethylglycine; Salts or complexes thereof
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Health & Medical Sciences (AREA)
Life Sciences & Earth Sciences (AREA)
Biochemistry (AREA)
General Health & Medical Sciences (AREA)
Molecular Biology (AREA)
Catalysts (AREA)
Agricultural Chemicals And Associated Chemicals (AREA)
Preparation Of Compounds By Using Micro-Organisms (AREA)

DE69114610T 1990-03-12 1991-03-12 Herstellung von n-phosphonomethylglyzin durch oxydation von n-phosphonomethyliminodiessigsäure. Expired - Fee Related DE69114610T2 (de)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
ES9000732A ES2021229A6 (es)	1990-03-12	1990-03-12	Perfeccionamientos introducidos en un procedimiento de obtencion de n-fosfonometilglicina por oxidacion de n-fosfonometiliminodiacetico.
PCT/ES1991/000013 WO1991013893A1 (es)	1990-03-12	1991-03-12	Preparacion de n-fosfonometilglicina por oxidacion de acido n-fosfonometiliminodiacetico

Publications (2)

Publication Number	Publication Date
DE69114610D1 DE69114610D1 (de)	1995-12-21
DE69114610T2 true DE69114610T2 (de)	1996-05-02

Family

ID=8266371

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
DE69114610T Expired - Fee Related DE69114610T2 (de)	1990-03-12	1991-03-12	Herstellung von n-phosphonomethylglyzin durch oxydation von n-phosphonomethyliminodiessigsäure.

Country Status (9)

Country	Link
US (1)	US5179228A (de)
EP (1)	EP0472693B1 (de)
KR (1)	KR920701215A (de)
AU (1)	AU637896B2 (de)
DE (1)	DE69114610T2 (de)
DK (1)	DK0472693T3 (de)
ES (1)	ES2021229A6 (de)
GR (1)	GR3018731T3 (de)
WO (1)	WO1991013893A1 (de)

Families Citing this family (33)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US6232494B1 (en) *	1998-02-12	2001-05-15	Monsanto Company	Process for the preparation of N-(phosphonomethyl)glycine by oxidizing N-substituted N-(phosphonomethyl)glycine
EP1716923A1 (de) *	1998-02-12	2006-11-02	Monsanto Technology, LLC	Oxidationskatalysator zur Herstellung von Glyphosat
US6417133B1 (en)	1998-02-25	2002-07-09	Monsanto Technology Llc	Deeply reduced oxidation catalyst and its use for catalyzing liquid phase oxidation reactions
US5962729A (en) *	1998-05-14	1999-10-05	Calgon Carbon Corporation	Method for the manufacture of N-phosphonomethylglycine from N-phosphonomethyliminodiacetic acid using a catalytic carbon
US5942643A (en) *	1998-05-14	1999-08-24	Calgon Carbon Corporation	Method for the manufacture of N-phosphonomethylglycine from N-phosphonomethyliminodiacetic acid using a low temperature catalytic carbon
IL140488A0 (en) *	1998-07-06	2002-02-10	Syngenta Participations Ag	Preparation of n-phosphonomethylglycine salts
IES980552A2 (en)	1998-07-09	1999-08-11	Agritech Chemical Ltd	Improved process for preparing N-phosphonomethyl iminodiacetic acid
AU6024599A (en) *	1998-09-08	2000-03-27	Hampshire Chemical Corp.	Synthesis of phosphonomethyliminodiacetic acid with reduced effluent
ES2195929T3 (es)	1999-07-23	2003-12-16	Basf Ag	Procedimiento para la obtencion de glifosatos o de una sal de los mismos.
IL150354A0 (en)	1999-12-21	2002-12-01	Monsanto Technology Llc	Use of a supplemental promoter in conjunction with a carbon-supported, noble-metal containing catalyst in liquid phase oxidation reactions
DE10007702A1 (de) *	2000-02-19	2001-08-23	Sueddeutsche Kalkstickstoff	Verfahren zur Herstellung von N-(Phosphonomethyl)glycin
US6376708B1 (en)	2000-04-11	2002-04-23	Monsanto Technology Llc	Process and catalyst for dehydrogenating primary alcohols to make carboxylic acid salts
CN100354256C (zh) *	2000-05-15	2007-12-12	孟山都技术有限责任公司	以单乙醇胺为原料制备亚氨基二乙酸化合物
US6927304B2 (en)	2000-05-22	2005-08-09	Monsanto Technology Llc	De-oxygenation treatment for noble metal on carbon catalysts used in liquid phase oxidation reactions
ATE310009T1 (de)	2000-05-22	2005-12-15	Monsanto Technology Llc	Reaktionssysteme zur herstellung von n- (phosphonomethyl)glyzin verbindungen
US6818450B2 (en)	2001-05-22	2004-11-16	Monsanto Technology Llc	Use of infrared spectroscopy for on-line process control and endpoint detection
CN1729052A (zh)	2001-10-18	2006-02-01	孟山都技术公司	用于伯醇脱氢以制备羧酸盐的方法和催化剂
US7390920B2 (en) *	2002-02-14	2008-06-24	Monsanto Technology Llc	Oxidation catalyst and process
CA2476255C (en) *	2002-02-14	2012-07-31	Monsanto Technology Llc	Oxidation catalyst and process for its preparation and process for oxidation using it
US6921834B2 (en)	2002-05-22	2005-07-26	Dow Agrosciences Llc	Continuous process for preparing N-phosphonomethyl glycine
JP4202047B2 (ja) *	2002-05-24	2008-12-24	富士通株式会社	ヘッド位置制御方法及びデイスク記憶装置
WO2004002622A1 (en) *	2002-06-28	2004-01-08	Monsanto Technology Llc	Use of tellurium in carbon-supported, noble metal-containing catalysts for liquid phase oxidation reactions
EP1684900B1 (de)	2003-08-14	2013-02-27	Monsanto Technology LLC	Verfahren zur Oxidation von N-(phosphonomethyl)iminodiessigsäure oder Salz davon
BRPI0414464A (pt) *	2003-09-17	2006-11-21	Monsanto Technology Llc	processo para recuperação de um produto cristalino a partir de uma solução
US8703639B2 (en) *	2004-09-15	2014-04-22	Monsanto Technology Llc	Oxidation catalyst and its use for catalyzing liquid phase oxidation reactions
AR054096A1 (es) *	2004-11-12	2007-06-06	Monsanto Technology Llc	Recuperacion de metales nobles de corrientes de proceso acuosas y proceso de preparacion de n-(fosfonometil)-glicina
CA2598013C (en)	2005-02-17	2014-11-25	Monsanto Technology Llc	Transition metal-containing catalysts and catalyst combinations including transition metal-containing catalysts and processes for their preparation and use as oxidation catalysts
MX2007012239A (es)	2005-04-01	2007-12-07	Monsanto Technology Llc	Control de la conversion de acido n-(fosfonometil) iminodiacetico en la fabricacion de glifosato.
CA2642226A1 (en) *	2006-02-17	2007-08-30	Monsanto Technology Llc	Transition metal-containing catalysts and processes for their preparation and use as fuel cell catalysts
US7771494B2 (en) *	2007-01-31	2010-08-10	Monsanto Technology Llc	Process for selective removal of water and impurities from N-(phosphonomethyl)glycine
US8252953B2 (en)	2008-05-01	2012-08-28	Monsanto Technology Llc	Metal utilization in supported, metal-containing catalysts
CN104058495B (zh)	2009-05-18	2016-04-20	孟山都技术公司	含水废物流中磷有用成分和盐杂质的回收
US11279644B2 (en)	2017-06-26	2022-03-22	Monsanto Technology Llc	Phosphorus control for waste streams from glyphosate manufacturing processes

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US3950402A (en) *	1972-05-31	1976-04-13	Monsanto Company	Process for producing N-phosphonomethyl glycine
MX4703E (es) *	1976-12-20	1982-08-04	Monsanto Co	Procedimiento mejorado para la preparacion de mono y disales de n-fosfonometilglicina
US4582650A (en) *	1985-02-11	1986-04-15	Monsanto Company	Oxidation with encapsulated co-catalyst
US4579689A (en) *	1985-02-11	1986-04-01	Monsanto Company	Oxidation with coated catalyst
US4853159A (en) *	1987-10-26	1989-08-01	Monsanto Company	Process for producing N-phosphonomethylglycine
US4952723A (en) *	1989-07-31	1990-08-28	Monsanto Company	Process for producing N-phosphonomethylglycine

1990
- 1990-03-12 ES ES9000732A patent/ES2021229A6/es not_active Expired - Lifetime
1991
- 1991-03-12 WO PCT/ES1991/000013 patent/WO1991013893A1/es active IP Right Grant
- 1991-03-12 EP EP91905864A patent/EP0472693B1/de not_active Expired - Lifetime
- 1991-03-12 AU AU74973/91A patent/AU637896B2/en not_active Ceased
- 1991-03-12 KR KR1019910701582A patent/KR920701215A/ko not_active Application Discontinuation
- 1991-03-12 DK DK91905864.4T patent/DK0472693T3/da active
- 1991-03-12 DE DE69114610T patent/DE69114610T2/de not_active Expired - Fee Related
- 1991-03-12 US US07/778,842 patent/US5179228A/en not_active Expired - Fee Related
1996
- 1996-01-18 GR GR960400118T patent/GR3018731T3/el unknown

Also Published As

Publication number	Publication date
GR3018731T3 (en)	1996-04-30
AU7497391A (en)	1991-10-10
ES2021229A6 (es)	1991-10-16
KR920701215A (ko)	1992-08-11
DK0472693T3 (da)	1996-01-02
DE69114610D1 (de)	1995-12-21
AU637896B2 (en)	1993-06-10
US5179228A (en)	1993-01-12
EP0472693A1 (de)	1992-03-04
WO1991013893A1 (es)	1991-09-19
EP0472693B1 (de)	1995-11-15

Legal Events

Date	Code	Title	Description
1996-12-12	8364	No opposition during term of opposition
2000-05-11	8339	Ceased/non-payment of the annual fee

Publication	Publication Date	Title
DE69114610T2 (de)	1996-05-02	Herstellung von n-phosphonomethylglyzin durch oxydation von n-phosphonomethyliminodiessigsäure.
ATE72660T1 (de)	1992-03-15	Herstellung von zeolith-l.
DE69201934D1 (de)	1995-05-11	Verfahren zur Herstellung von Sonnenschutzmitteln.
DE3872495T2 (de)	1993-01-28	Herstellung von 3,3,3-trifluoropropen.
ATE131185T1 (de)	1995-12-15	Herstellung von peroxidhaltigen perfluorpolyethern.
DE69018071T2 (de)	1995-07-27	Herstellung von peroxysäuren.
DE3482982D1 (de)	1990-09-20	Herstellung von l-aminosaeuren durch transaminierung.
ATE116961T1 (de)	1995-01-15	Herstellung von zitronensäure.
DE69010963T2 (de)	1995-01-19	Herstellung von Adipinsäure aus Laktonen.
DE3875281D1 (de)	1992-11-19	Herstellung von pseudoiononen.
DE3773028D1 (de)	1991-10-24	Herstellung von zimtsaeuren.
ATE2685T1 (de)	1986-03-15	Herstellung von 2-keto-l-gulonsaeure.
DE69108740D1 (de)	1995-05-11	Herstellung von peroxidzusammensetzungen.
DE69001071T2 (de)	1993-06-17	Verfahren zur herstellung von n-alkyl-carbaminsaeurearylestern.
DE59204060D1 (de)	1995-11-23	Verfahren zur Herstellung von 1-Fluor-cyclopropan-1-carbonsäure.
DE3888307T2 (de)	1994-06-16	Verfahren zur Herstellung von Ascorbinsäure-2-phosphat.
DE3869465D1 (de)	1992-04-30	Herstellung von 4-pentenoat durch isomerisation.
ATE73765T1 (de)	1992-04-15	Verfahren zur herstellung von 2-nitro-5-phenoxy-n-alkylsulfonylbenzamiden durch nitrierung.
DE59104571D1 (de)	1995-03-23	Verfahren zur Herstellung von Vinylphosphonsäurederivaten.
DE69004199D1 (de)	1993-12-02	Herstellung von Cymenol durch direkte Dehydrogenierung.
DE3886786T2 (de)	1994-06-01	Verfahren zur Herstellung von Cimetidin.
DE69109953D1 (de)	1995-06-29	Alfa-fluorocarbonsäurederivate als Zwischenprodukte zur Herstellung von Fungiziden.
DE3766873D1 (de)	1991-02-07	Herstellung von substituierten dichlormethylpyridinen.
DE3862402D1 (de)	1991-05-23	Verfahren zur herstellung von 2,3,5,6-tetrafluorbenzoesaeure.
DE3486091T2 (de)	1993-09-16	Herstellung von butandicarboxylsaeureestern.