DE429272C - Process for the representation of bodies similar to fatty acids - Google Patents
Process for the representation of bodies similar to fatty acidsInfo
- Publication number
- DE429272C DE429272C DEM75493D DEM0075493D DE429272C DE 429272 C DE429272 C DE 429272C DE M75493 D DEM75493 D DE M75493D DE M0075493 D DEM0075493 D DE M0075493D DE 429272 C DE429272 C DE 429272C
- Authority
- DE
- Germany
- Prior art keywords
- representation
- fatty acids
- bodies similar
- bodies
- until
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title claims description 8
- 235000014113 dietary fatty acids Nutrition 0.000 title 1
- 229930195729 fatty acid Natural products 0.000 title 1
- 239000000194 fatty acid Substances 0.000 title 1
- 150000004665 fatty acids Chemical class 0.000 title 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 4
- 229910052739 hydrogen Inorganic materials 0.000 claims description 4
- 239000001257 hydrogen Substances 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 3
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 239000011347 resin Substances 0.000 claims description 2
- 229920005989 resin Polymers 0.000 claims description 2
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 2
- 235000011152 sodium sulphate Nutrition 0.000 claims description 2
- 230000009965 odorless effect Effects 0.000 claims 1
- 238000005984 hydrogenation reaction Methods 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 239000007858 starting material Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 239000003784 tall oil Substances 0.000 description 3
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000012043 crude product Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 229910052763 palladium Inorganic materials 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 239000012265 solid product Substances 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- PHYFQTYBJUILEZ-IUPFWZBJSA-N triolein Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCC(OC(=O)CCCCCCC\C=C/CCCCCCCC)COC(=O)CCCCCCC\C=C/CCCCCCCC PHYFQTYBJUILEZ-IUPFWZBJSA-N 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09F—NATURAL RESINS; FRENCH POLISH; DRYING-OILS; OIL DRYING AGENTS, i.e. SICCATIVES; TURPENTINE
- C09F1/00—Obtaining purification, or chemical modification of natural resins, e.g. oleo-resins
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
Verfahren zur Darstellung fettsäureartiger Körper. Das Hauptpatent schützt ein Verfahren zur Darstellung fettsäureartiger Körper, nach welchem man das beim Natronsulfatv erfahren entstehende flüssige Harz der Einwirkung von Wasserstoff unterwirft.Process for the preparation of fatty acid-like bodies. The main patent protects a process for the preparation of fatty acid-like bodies, according to which one the liquid resin produced by the action of hydrogen in the sodium sulfate process subject.
Nach diesem Verfahren sollen vor allem Stoffe hergestellt werden, die zur Herstellung von Seifen bzw. seifenartigen Produkten verwendet werden.This process is primarily intended to produce substances which are used to make soaps or soap-like products.
Es hat sich nun gezeigt - und das bildet den Gegenstand der Erfindung -, daß es nicht erforderlich ist, die Hydrierung des Ausgangsstoffes so weit zu treiben, bis feste oder halbfeste Produkte entstehen, sondern daß es zwecks Herstellung technisch verwendbarer Stoffe genügt, das Ausgangsmaterial nur einer gelinden Hydrierung zu untern erfen, indem man es mit Wasserstoff nur so hinge behandelt, bis es seinen Geruch verloren hat. Das entstehende Produkt ist alsdann noch flüssig, unterscheidet sich aber von dem Ausgangsmaterial dadurch, daß es nicht mehr übelriechend ist. Das Produkt kann für eine Reihe von Verwendungszwecken Benutzung finden, beispielsweise kann es in der Textilindustrie als Ersatz für Olein verwendet werden.It has now been shown - and that forms the subject of the invention - That it is not necessary to hydrogenate the starting material so far drift until solid or semi-solid products arise, but that it is for the purpose of production Technically usable substances are sufficient, the starting material only a mild hydrogenation to be undertaken by treating it with hydrogen just until it is Has lost smell. The resulting product is then still liquid, differentiates but differs from the starting material in that it is no longer malodorous. The product can find use for a number of purposes, for example it can be used in the textile industry as a substitute for olein.
Das Verfahren verläuft im übrigen genau so, wie es das Hauptpatent beschreibt, es wird lediglich die Einwirkung des Wasser-Stoffes nur so lange fortgesetzt, bis das Öl seinen typischen Geruch verloren hat, ohne in Festen Zustand überzugehen.The procedure is otherwise exactly as it is the main patent describes that the action of the water substance is only continued as long as until the oil has lost its typical smell without changing into a solid state.
Das Tallöl kann auch vor der Hydrierung einer Destillation unterworfen werden, wie es Patent 37i55 beschreibt. Es kann auch vor oder nach der Hydrierung eine Raffination oder Behandlung mit Wasserdampf erfolgen. Ausführungsbeispiel ioo kg Tallöl, und zwar entweder das Rohprodukt oder die aus Tallöl durch Destillation erhaltenen niedrigsiedenden Anteile werden reit i kg Nickelkatalysator oder ioo g Palladiumkatalysator «im Autoklav en in der gewöhnlichen Weise einige Stunden lang hydriert, und zwar so lange, bis etwa i cbm Wasserstoff aufgenommen worden ist. Der Katalysator wird dann durch Filtrieren in bekannter Weise entfernt.The tall oil can also be subjected to distillation prior to hydrogenation as described in patent 37i55. It can also be done before or after the hydrogenation refining or treatment with steam. Embodiment ioo kg of tall oil, either the crude product or that from tall oil by distillation The low-boiling fractions obtained are just 1 kg of nickel catalyst or 100% g palladium catalyst in the autoclave in the usual way for a few hours hydrogenated for a long time, until about 1 cbm of hydrogen has been absorbed is. The catalyst is then removed by filtration in a known manner.
Claims (1)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEM75493D DE429272C (en) | 1921-10-22 | 1921-10-22 | Process for the representation of bodies similar to fatty acids |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEM75493D DE429272C (en) | 1921-10-22 | 1921-10-22 | Process for the representation of bodies similar to fatty acids |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE429272C true DE429272C (en) | 1926-05-31 |
Family
ID=7316375
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEM75493D Expired DE429272C (en) | 1921-10-22 | 1921-10-22 | Process for the representation of bodies similar to fatty acids |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE429272C (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE914884C (en) * | 1951-03-13 | 1954-07-12 | Thoerl S Vereinigte Harburger | Process for refining tallow oil and the distillates, raffinates and fractions obtained from it |
-
1921
- 1921-10-22 DE DEM75493D patent/DE429272C/en not_active Expired
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE914884C (en) * | 1951-03-13 | 1954-07-12 | Thoerl S Vereinigte Harburger | Process for refining tallow oil and the distillates, raffinates and fractions obtained from it |
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