DE3013152C2 - Verfahren zur Herstellung von Granulaten mit gegen Verbacken geschützter Oberfläche - Google Patents

Verfahren zur Herstellung von Granulaten mit gegen Verbacken geschützter Oberfläche

Info

Publication number: DE3013152C2
Authority: DE; Germany
Prior art keywords: granules; soap; caking; grains; stearate
Prior art date: 1979-04-06
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

DE3013152A

Other languages

German (de)

English (en)

Other versions

DE3013152A1 (de

Inventor

Hans-Gerhard Klippan Grunert

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Individual

Original Assignee

Individual

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1979-04-06

Filing date

1980-04-03

Publication date

1987-02-26

1980-04-03 Application filed by Individual filed Critical Individual

1980-10-16 Publication of DE3013152A1 publication Critical patent/DE3013152A1/de

1987-02-26 Application granted granted Critical

1987-02-26 Publication of DE3013152C2 publication Critical patent/DE3013152C2/de

Status Expired legal-status Critical Current

Links

239000008187 granular material Substances 0.000 title claims description 17
238000000034 method Methods 0.000 title claims description 9
239000000344 soap Substances 0.000 claims description 21
239000007788 liquid Substances 0.000 claims description 15
QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 10
239000003337 fertilizer Substances 0.000 claims description 10
239000003795 chemical substances by application Substances 0.000 claims description 9
ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 8
229910052700 potassium Inorganic materials 0.000 claims description 8
239000011591 potassium Substances 0.000 claims description 8
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 7
229910052708 sodium Inorganic materials 0.000 claims description 7
239000011734 sodium Substances 0.000 claims description 7
125000004432 carbon atom Chemical group C* 0.000 claims description 2
150000001732 carboxylic acid derivatives Chemical class 0.000 claims description 2
150000001735 carboxylic acids Chemical class 0.000 claims description 2
239000000203 mixture Substances 0.000 claims description 2
239000000126 substance Substances 0.000 claims description 2
235000014113 dietary fatty acids Nutrition 0.000 description 12
239000000194 fatty acid Substances 0.000 description 12
229930195729 fatty acid Natural products 0.000 description 12
150000004665 fatty acids Chemical class 0.000 description 9
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 6
-1 fatty acid amines Chemical class 0.000 description 5
HQKMJHAJHXVSDF-UHFFFAOYSA-L magnesium stearate Chemical compound [Mg+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O HQKMJHAJHXVSDF-UHFFFAOYSA-L 0.000 description 5
239000000843 powder Substances 0.000 description 5
238000007127 saponification reaction Methods 0.000 description 5
239000003784 tall oil Substances 0.000 description 5
239000002253 acid Substances 0.000 description 4
238000006243 chemical reaction Methods 0.000 description 4
239000002245 particle Substances 0.000 description 4
229940114930 potassium stearate Drugs 0.000 description 4
ANBFRLKBEIFNQU-UHFFFAOYSA-M potassium;octadecanoate Chemical compound [K+].CCCCCCCCCCCCCCCCCC([O-])=O ANBFRLKBEIFNQU-UHFFFAOYSA-M 0.000 description 4
239000002344 surface layer Substances 0.000 description 4
VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 description 3
DCXXMTOCNZCJGO-UHFFFAOYSA-N Glycerol trioctadecanoate Natural products CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC DCXXMTOCNZCJGO-UHFFFAOYSA-N 0.000 description 3
229910021529 ammonia Inorganic materials 0.000 description 3
238000004821 distillation Methods 0.000 description 3
230000000694 effects Effects 0.000 description 3
235000019359 magnesium stearate Nutrition 0.000 description 3
239000000463 material Substances 0.000 description 3
239000002904 solvent Substances 0.000 description 3
XOOUIPVCVHRTMJ-UHFFFAOYSA-L zinc stearate Chemical compound [Zn+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O XOOUIPVCVHRTMJ-UHFFFAOYSA-L 0.000 description 3
RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 2
241001465754 Metazoa Species 0.000 description 2
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
235000021355 Stearic acid Nutrition 0.000 description 2
HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 2
229910017052 cobalt Inorganic materials 0.000 description 2
239000010941 cobalt Substances 0.000 description 2
GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 2
150000001875 compounds Chemical class 0.000 description 2
229910052802 copper Inorganic materials 0.000 description 2
239000010949 copper Substances 0.000 description 2
239000010410 layer Substances 0.000 description 2
239000011777 magnesium Substances 0.000 description 2
229910052749 magnesium Inorganic materials 0.000 description 2
150000002736 metal compounds Chemical class 0.000 description 2
QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 2
OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 2
239000000243 solution Substances 0.000 description 2
239000008117 stearic acid Substances 0.000 description 2
150000005846 sugar alcohols Polymers 0.000 description 2
239000011701 zinc Substances 0.000 description 2
229910052725 zinc Inorganic materials 0.000 description 2
WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 1
RSWGJHLUYNHPMX-UHFFFAOYSA-N 1,4a-dimethyl-7-propan-2-yl-2,3,4,4b,5,6,10,10a-octahydrophenanthrene-1-carboxylic acid Chemical compound C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 description 1
LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 1
BTXXTMOWISPQSJ-UHFFFAOYSA-N 4,4,4-trifluorobutan-2-one Chemical compound CC(=O)CC(F)(F)F BTXXTMOWISPQSJ-UHFFFAOYSA-N 0.000 description 1
JXSRRBVHLUJJFC-UHFFFAOYSA-N 7-amino-2-methylsulfanyl-[1,2,4]triazolo[1,5-a]pyrimidine-6-carbonitrile Chemical compound N1=CC(C#N)=C(N)N2N=C(SC)N=C21 JXSRRBVHLUJJFC-UHFFFAOYSA-N 0.000 description 1
QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 1
QUUCYKKMFLJLFS-UHFFFAOYSA-N Dehydroabietan Natural products CC1(C)CCCC2(C)C3=CC=C(C(C)C)C=C3CCC21 QUUCYKKMFLJLFS-UHFFFAOYSA-N 0.000 description 1
NFWKVWVWBFBAOV-UHFFFAOYSA-N Dehydroabietic acid Natural products OC(=O)C1(C)CCCC2(C)C3=CC=C(C(C)C)C=C3CCC21 NFWKVWVWBFBAOV-UHFFFAOYSA-N 0.000 description 1
PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 1
KGMSWPSAVZAMKR-UHFFFAOYSA-N Me ester-3, 22-Dihydroxy-29-hopanoic acid Natural products C1CCC(C(O)=O)(C)C2C1(C)C1CCC(=C(C)C)C=C1CC2 KGMSWPSAVZAMKR-UHFFFAOYSA-N 0.000 description 1
KGMSWPSAVZAMKR-ONCXSQPRSA-N Neoabietic acid Chemical compound [C@H]1([C@](CCC2)(C)C(O)=O)[C@@]2(C)[C@H]2CCC(=C(C)C)C=C2CC1 KGMSWPSAVZAMKR-ONCXSQPRSA-N 0.000 description 1
ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 1
239000005642 Oleic acid Substances 0.000 description 1
239000004698 Polyethylene Substances 0.000 description 1
RSWGJHLUYNHPMX-ONCXSQPRSA-N abietic acid Chemical compound C([C@@H]12)CC(C(C)C)=CC1=CC[C@@H]1[C@]2(C)CCC[C@@]1(C)C(O)=O RSWGJHLUYNHPMX-ONCXSQPRSA-N 0.000 description 1
150000007513 acids Chemical class 0.000 description 1
229940088990 ammonium stearate Drugs 0.000 description 1
239000007864 aqueous solution Substances 0.000 description 1
JPNZKPRONVOMLL-UHFFFAOYSA-N azane;octadecanoic acid Chemical compound [NH4+].CCCCCCCCCCCCCCCCCC([O-])=O JPNZKPRONVOMLL-UHFFFAOYSA-N 0.000 description 1
239000011230 binding agent Substances 0.000 description 1
AMFIJXSMYBKJQV-UHFFFAOYSA-L cobalt(2+);octadecanoate Chemical compound [Co+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O AMFIJXSMYBKJQV-UHFFFAOYSA-L 0.000 description 1
239000013078 crystal Substances 0.000 description 1
NFWKVWVWBFBAOV-MISYRCLQSA-N dehydroabietic acid Chemical compound OC(=O)[C@]1(C)CCC[C@]2(C)C3=CC=C(C(C)C)C=C3CC[C@H]21 NFWKVWVWBFBAOV-MISYRCLQSA-N 0.000 description 1
229940118781 dehydroabietic acid Drugs 0.000 description 1
239000003085 diluting agent Substances 0.000 description 1
238000005194 fractionation Methods 0.000 description 1
229910052742 iron Inorganic materials 0.000 description 1
150000002506 iron compounds Chemical class 0.000 description 1
FRVCGRDGKAINSV-UHFFFAOYSA-L iron(2+);octadecanoate Chemical compound [Fe+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O FRVCGRDGKAINSV-UHFFFAOYSA-L 0.000 description 1
QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 1
229910052748 manganese Inorganic materials 0.000 description 1
239000011572 manganese Substances 0.000 description 1
WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
SZINCDDYCOIOJQ-UHFFFAOYSA-L manganese(2+);octadecanoate Chemical compound [Mn+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O SZINCDDYCOIOJQ-UHFFFAOYSA-L 0.000 description 1
235000013379 molasses Nutrition 0.000 description 1
239000002052 molecular layer Substances 0.000 description 1
ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
239000012188 paraffin wax Substances 0.000 description 1
229920000058 polyacrylate Polymers 0.000 description 1
229920000573 polyethylene Polymers 0.000 description 1
229920000193 polymethacrylate Polymers 0.000 description 1
159000000001 potassium salts Chemical class 0.000 description 1
150000003141 primary amines Chemical class 0.000 description 1
239000011347 resin Chemical class 0.000 description 1
229920005989 resin Chemical class 0.000 description 1
150000003839 salts Chemical class 0.000 description 1
239000000377 silicon dioxide Substances 0.000 description 1
RYYKJJJTJZKILX-UHFFFAOYSA-M sodium octadecanoate Chemical compound [Na+].CCCCCCCCCCCCCCCCCC([O-])=O RYYKJJJTJZKILX-UHFFFAOYSA-M 0.000 description 1
229940080350 sodium stearate Drugs 0.000 description 1
238000004381 surface treatment Methods 0.000 description 1
239000000454 talc Substances 0.000 description 1
229910052623 talc Inorganic materials 0.000 description 1
239000003760 tallow Substances 0.000 description 1
235000013311 vegetables Nutrition 0.000 description 1
239000001993 wax Substances 0.000 description 1

Classifications

- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
- B01J2/30—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic using agents to prevent the granules sticking together; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/30—Anti-agglomerating additives; Anti-solidifying additives
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/30—Layered or coated, e.g. dust-preventing coatings

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Life Sciences & Earth Sciences (AREA)
Pest Control & Pesticides (AREA)
Chemical Kinetics & Catalysis (AREA)
Fertilizers (AREA)

DE3013152A 1979-04-06 1980-04-03 Verfahren zur Herstellung von Granulaten mit gegen Verbacken geschützter Oberfläche Expired DE3013152C2 (de)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
SE7903066A SE421492B (sv)	1979-04-06	1979-04-06	Forfarande for framstellning av mot sammanbakning ytbehandlade granuler, korn eller dylikt av hydrofila och hygroskopiska material

Publications (2)

Publication Number	Publication Date
DE3013152A1 DE3013152A1 (de)	1980-10-16
DE3013152C2 true DE3013152C2 (de)	1987-02-26

Family

ID=20337744

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
DE3013152A Expired DE3013152C2 (de)	1979-04-06	1980-04-03	Verfahren zur Herstellung von Granulaten mit gegen Verbacken geschützter Oberfläche

Country Status (2)

Country	Link
DE (1)	DE3013152C2 (fr)
SE (1)	SE421492B (fr)

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
FR2339663A1 (fr) *	1976-01-29	1977-08-26	Ppg Ind Canada Ltd	Composition antiagglutinante de faible viscosite et son procede de preparation

1979
- 1979-04-06 SE SE7903066A patent/SE421492B/sv not_active IP Right Cessation
1980
- 1980-04-03 DE DE3013152A patent/DE3013152C2/de not_active Expired

Also Published As

Publication number	Publication date
DE3013152A1 (de)	1980-10-16
SE7903066L (sv)	1980-10-07
SE421492B (sv)	1982-01-04

Legal Events

Date	Code	Title	Description
1986-05-07	8110	Request for examination paragraph 44
1986-09-11	8128	New person/name/address of the agent	Representative=s name: KUHNEN, R., DIPL.-ING. WACKER, P., DIPL.-ING. DIPL
1987-02-26	D2	Grant after examination
1987-08-20	8364	No opposition during term of opposition
1990-04-12	8339	Ceased/non-payment of the annual fee

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CH676980A5 (fr)	1991-03-28
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DE19608000B4 (de)	2004-09-02	Verfahren zur Herstellung von körnigem Natriumpercarbonat
DE2334542A1 (de)	1974-01-24	Korrosionsinhibierendes pigment und verfahren zur herstellung desselben
DE2136978A1 (de)	1972-02-17	Verfahren zur Verhinderung des Zu sammenbackens von Teilchen aus einem Kernmaterial mit einem Überzug
DE1592655C2 (de)	1972-03-30	Düngemittelgranulat mit kontollierter Nährstoffabgabe
DE3013152C2 (de)	1987-02-26	Verfahren zur Herstellung von Granulaten mit gegen Verbacken geschützter Oberfläche
DE2515425A1 (de)	1975-10-16	Brikettiertes duengemittel fuer die waldduengung und verfahren zu seiner herstellung
EP0230299A1 (fr)	1987-07-29	Procédé pour l'application de dicyandiamide finement divisé sur des engrais contenant des groupes ammonium et sulfate
DE1544697C3 (de)	1978-09-07	Staubfreie Stabilisatoren-Gleitmittel-Kombination für halogenhaltige Polymere
EP1340738B1 (fr)	2012-08-29	Méthode pour préparer les engrais minéraux
DE2136973C3 (de)	1979-06-21	Nicht zusammenbackendes Natriumpropionat
DE2360851C3 (de)	1979-10-25	Verfahren zur Verminderung der Backneigung eines anorganischen Düngesalzes
EP0431091B1 (fr)	1997-04-02	Procede antipoussiere pour granules d'engrais
DE3223139C2 (de)	1985-02-07	Verfahren zur Herstellung von Harnstoff als Hauptbestandteil enthaltenden Düngemittelkörnern
DE3811913C1 (fr)	1989-10-12
DE1300134B (de)	1969-07-31	Verfahren zur Herstellung lagerfaehiger, mit einem Mineraloelprodukt ueberzogener, nitrathaltiger NPK-Duengemittel
DE69911544T2 (de)	2004-08-05	Molybdänseifen enthaltende metallseifen und verfahren zu ihrer herstellung
DE2155924C3 (de)	1985-12-05	Beschichtetes Düngemittelgranulat
DE3020255C2 (de)	1983-12-22	Verfahren zum Herstellen von nichtstaubenden, gleitmittelarmen basischen und/oder neutralen Metallsalzen und/oder -seifen
DE2122890A1 (en)	1972-11-23	Improving surface properties of granules - by impregnating with polyoxyalkylene and hydrophobising agents
DE1916089A1 (de)	1969-12-18	Nichtzusammenballende Harnstoff-Zusammensetzung
DE3403621A1 (de)	1984-08-02	Verfahren zur herstellung von metallseifen
DE2910896A1 (de)	1979-10-04	Rostschutzmittel und verfahren zu dessen herstellung
DE4209924A1 (de)	1993-09-30	Stabilisiertes Percarbonat (II)