DE2118282A1 - - Google Patents

Info

Publication number: DE2118282A1
Authority: DE; Germany
Prior art keywords: acetic acid; diacetylethylenediamine; ethylenediamine; continuously; distilled
Prior art date: 1971-04-15
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Granted

Application number

DE19712118282

Other languages

German (de)

English (en)

Other versions

DE2118282C3 (de

DE2118282B2 (de

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1971-04-15

Filing date

1971-04-15

Publication date

1972-11-02

1971-04-15 Application filed filed Critical

1971-04-15 Priority to DE2118282A priority Critical patent/DE2118282C3/de

1972-03-22 Priority to CH428472A priority patent/CH564520A5/xx

1972-04-12 Priority to BE781995A priority patent/BE781995A/xx

1972-04-12 Priority to IT49563/72A priority patent/IT954430B/it

1972-04-12 Priority to FR7212778A priority patent/FR2136341A5/fr

1972-04-12 Priority to NL7204898A priority patent/NL7204898A/xx

1972-04-13 Priority to SE04809/72A priority patent/SE368198B/xx

1972-04-14 Priority to AT325772A priority patent/AT314492B/de

1972-04-14 Priority to GB1726172A priority patent/GB1383583A/en

1972-11-02 Publication of DE2118282A1 publication Critical patent/DE2118282A1/de

1974-02-07 Publication of DE2118282B2 publication Critical patent/DE2118282B2/de

1974-10-03 Application granted granted Critical

1974-10-03 Publication of DE2118282C3 publication Critical patent/DE2118282C3/de

Status Expired legal-status Critical Current

Links

QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 66
PIICEJLVQHRZGT-UHFFFAOYSA-N Ethylenediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 claims description 13
WNYIBZHOMJZDKN-UHFFFAOYSA-N n-(2-acetamidoethyl)acetamide Chemical compound CC(=O)NCCNC(C)=O WNYIBZHOMJZDKN-UHFFFAOYSA-N 0.000 claims description 12
238000000034 method Methods 0.000 claims description 9
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
239000000155 melt Substances 0.000 claims description 5
239000003795 chemical substances by application Substances 0.000 claims description 3
238000010924 continuous production Methods 0.000 claims description 3
238000006243 chemical reaction Methods 0.000 description 15
WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical compound CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 description 9
239000007858 starting material Substances 0.000 description 4
239000006227 byproduct Substances 0.000 description 2
238000010438 heat treatment Methods 0.000 description 2
238000000746 purification Methods 0.000 description 2
239000000126 substance Substances 0.000 description 2
VWSLLSXLURJCDF-UHFFFAOYSA-N 2-methyl-4,5-dihydro-1h-imidazole Chemical compound CC1=NCCN1 VWSLLSXLURJCDF-UHFFFAOYSA-N 0.000 description 1
241001550224 Apha Species 0.000 description 1
239000000654 additive Substances 0.000 description 1
230000000996 additive effect Effects 0.000 description 1
150000003863 ammonium salts Chemical class 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
150000003857 carboxamides Chemical class 0.000 description 1
150000001735 carboxylic acids Chemical class 0.000 description 1
239000003599 detergent Substances 0.000 description 1
238000004821 distillation Methods 0.000 description 1
238000004519 manufacturing process Methods 0.000 description 1
238000002844 melting Methods 0.000 description 1
230000008018 melting Effects 0.000 description 1
239000000203 mixture Substances 0.000 description 1
HMSINBTULZNZRC-UHFFFAOYSA-N n-acetyl-n-(2-aminoethyl)acetamide Chemical compound CC(=O)N(C(C)=O)CCN HMSINBTULZNZRC-UHFFFAOYSA-N 0.000 description 1
239000011541 reaction mixture Substances 0.000 description 1
FRPJTGXMTIIFIT-UHFFFAOYSA-N tetraacetylethylenediamine Chemical compound CC(=O)C(N)(C(C)=O)C(N)(C(C)=O)C(C)=O FRPJTGXMTIIFIT-UHFFFAOYSA-N 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C231/00—Preparation of carboxylic acid amides
- C07C231/02—Preparation of carboxylic acid amides from carboxylic acids or from esters, anhydrides, or halides thereof by reaction with ammonia or amines
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C233/00—Carboxylic acid amides
- C07C233/01—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
- C07C233/34—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by amino groups
- C07C233/35—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by amino groups with the substituted hydrocarbon radical bound to the nitrogen atom of the carboxamide group by an acyclic carbon atom
- C07C233/36—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by amino groups with the substituted hydrocarbon radical bound to the nitrogen atom of the carboxamide group by an acyclic carbon atom having the carbon atom of the carboxamide group bound to a hydrogen atom or to a carbon atom of an acyclic saturated carbon skeleton

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

DE2118282A 1971-04-15 1971-04-15 Verfahren zur kontinuierlichen Herstellung von N.N'-Diacetyläthylendiamin Expired DE2118282C3 (de)

Priority Applications (9)

Application Number	Priority Date	Filing Date	Title
DE2118282A DE2118282C3 (de)	1971-04-15	1971-04-15	Verfahren zur kontinuierlichen Herstellung von N.N'-Diacetyläthylendiamin
CH428472A CH564520A5 (it)	1971-04-15	1972-03-22
IT49563/72A IT954430B (it)	1971-04-15	1972-04-12	Produzione continua di n n diaceti lendiammina
FR7212778A FR2136341A5 (it)	1971-04-15	1972-04-12
BE781995A BE781995A (fr)	1971-04-15	1972-04-12	Preparation en continu du diaceto-ethylenediamide
NL7204898A NL7204898A (it)	1971-04-15	1972-04-12
SE04809/72A SE368198B (it)	1971-04-15	1972-04-13
AT325772A AT314492B (de)	1971-04-15	1972-04-14	Verfahren zur kontinuierlichen Herstellung von N,N'-Diacetyläthylendiamin
GB1726172A GB1383583A (en)	1971-04-15	1972-04-14	Continuous production of n,n-diacetylethylenediamine

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
DE2118282A DE2118282C3 (de)	1971-04-15	1971-04-15	Verfahren zur kontinuierlichen Herstellung von N.N'-Diacetyläthylendiamin

Publications (3)

Publication Number	Publication Date
DE2118282A1 true DE2118282A1 (it)	1972-11-02
DE2118282B2 DE2118282B2 (de)	1974-02-07
DE2118282C3 DE2118282C3 (de)	1974-10-03

Family

ID=5804802

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
DE2118282A Expired DE2118282C3 (de)	1971-04-15	1971-04-15	Verfahren zur kontinuierlichen Herstellung von N.N'-Diacetyläthylendiamin

Country Status (9)

Country	Link
AT (1)	AT314492B (it)
BE (1)	BE781995A (it)
CH (1)	CH564520A5 (it)
DE (1)	DE2118282C3 (it)
FR (1)	FR2136341A5 (it)
GB (1)	GB1383583A (it)
IT (1)	IT954430B (it)
NL (1)	NL7204898A (it)
SE (1)	SE368198B (it)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
EP0027208A1 (de) *	1979-10-10	1981-04-22	Hoechst Aktiengesellschaft	Verfahren zur kontinuierlichen Herstellung von Di-acetyl-ethylendiamin
EP0042096A1 (de) *	1980-06-12	1981-12-23	BASF Aktiengesellschaft	Verfahren zur Herstellung von N,N'-Diacetylethylendiamin

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE2828765A1 (de) *	1978-06-30	1980-01-10	Hoechst Ag	Verfahren zur herstellung von n,n'-diacetylethylendiamin
DE2832021A1 (de) *	1978-07-21	1980-01-31	Basf Ag	Verfahren zur herstellung von tetraacetylaethylendiamin
DK12887A (da) *	1987-01-12	1988-07-13	Cheminova As	Fremgangsmaade til fremstilling af n,n'-diacetylethylendiamin

1971
- 1971-04-15 DE DE2118282A patent/DE2118282C3/de not_active Expired
1972
- 1972-03-22 CH CH428472A patent/CH564520A5/xx not_active IP Right Cessation
- 1972-04-12 FR FR7212778A patent/FR2136341A5/fr not_active Expired
- 1972-04-12 BE BE781995A patent/BE781995A/xx not_active IP Right Cessation
- 1972-04-12 NL NL7204898A patent/NL7204898A/xx not_active Application Discontinuation
- 1972-04-12 IT IT49563/72A patent/IT954430B/it active
- 1972-04-13 SE SE04809/72A patent/SE368198B/xx unknown
- 1972-04-14 GB GB1726172A patent/GB1383583A/en not_active Expired
- 1972-04-14 AT AT325772A patent/AT314492B/de not_active IP Right Cessation

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
EP0027208A1 (de) *	1979-10-10	1981-04-22	Hoechst Aktiengesellschaft	Verfahren zur kontinuierlichen Herstellung von Di-acetyl-ethylendiamin
EP0042096A1 (de) *	1980-06-12	1981-12-23	BASF Aktiengesellschaft	Verfahren zur Herstellung von N,N'-Diacetylethylendiamin

Also Published As

Publication number	Publication date
NL7204898A (it)	1972-10-17
DE2118282C3 (de)	1974-10-03
AT314492B (de)	1974-04-10
IT954430B (it)	1973-08-30
CH564520A5 (it)	1975-07-31
DE2118282B2 (de)	1974-02-07
FR2136341A5 (it)	1972-12-22
BE781995A (fr)	1972-10-12
GB1383583A (en)	1974-02-12
SE368198B (it)	1974-06-24

Legal Events

Date	Code	Title
1974-10-03	C3	Grant after two publication steps (3rd publication)
1977-12-31	E77	Valid patent as to the heymanns-index 1977
1984-09-13	8330	Complete renunciation

Publication	Publication Date	Title
DE2118282A1 (it)	1972-11-02
DE3106476C2 (de)	1984-01-05	Verfahren zur Herstellung von Trioxan
DE1493815B2 (de)	1976-11-04	Verfahren zur gewinnung von reinem 2,2-(4,4' - dihydroxydiphenyl) - propan
DE2341743B2 (de)	1981-02-19	Verfahren zur Herstellung einer Mischung aus Brenzkatechin und Hydrochinon
EP0026291B1 (de)	1983-02-09	Verfahren zur Herstellung von Terephthalaldehyd bzw. Isophthalaldehyd
DE1518647A1 (de)	1969-02-13	Verfahren zur Herstellung von Tetrabromphthalsaeureanhydrid
DE1468428A1 (de)	1969-03-27	Verfahren zur Herstellung von ungesaettigten Carbonsaeuren
DE2313386A1 (de)	1974-09-19	Verfahren zur herstellung von succinimid
DE2165858C3 (de)	1974-11-28	Verfahren zur Herstellung von höhermolekularen, aliphatischen Monocarbonsäuren
DE2938163C2 (it)	1988-08-11
DE1808389C3 (de)	1977-11-24	Verfahren zur Herstellung von Resorcin durch Säurehydrolyse von m-Phenylendiamin
DE1030836B (de)	1958-05-29	Verfahren zur Herstellung von 2, 2-Bis-(p-oxyphenyl)-propan
DE2341738A1 (de)	1974-02-28	Verfahren zur behandlung von rohem adiponitril
DE2233489C3 (de)	1981-12-03	Verfahren zur Herstellung von Octachlordipropyläther
DE586445C (de)	1933-10-25	Verfahren zum Aufarbeiten der rohen, bei der Herstellung von Benzylcellulose anfallenden Laugen
AT272332B (de)	1969-07-10	Verfahren zur Herstellung von Cumarin
DE621913C (de)	1935-11-15	Verfahren zur Herstellung von o-Dicarbonsaeurechloriden der Benzolreihe
DE1493815C3 (de)	1977-06-16	Verfahren zur Gewinnung von reinem 2,2-(4,4' - Dihydroxydiphenyl) - propan
DE1926538A1 (de)	1970-11-26	Verfahren zur kontinuierlichen Herstellung von Sorbinsaeure
DE2165219C3 (de)	1982-03-25	Verfahren zur Herstellung von Sorbinsäure
DE2145308C3 (de)	1977-12-15	Verfahren zur Herstellung von 4-(4-Hydroxyphenyl)-butan-2-on
DE2759151C2 (de)	1979-10-25	Verfahren zur Herstellung von 5-Cyan-3-pentensäuren
DE1007319B (de)	1957-05-02	Verfahren zur Herstellung von Acetylenalkoholen
DE1670240A1 (de)	1972-03-02	Verfahren zur Herstellung von N-Methylpiperazin
DE2261616A1 (de)	1973-06-28	Verfahren zur herstellung von organischen aldehyden

DE2118282A1 - - Google Patents

Info

Links

Classifications

Landscapes

Priority Applications (9)

Applications Claiming Priority (1)

Publications (3)

Family

ID=5804802

Family Applications (1)

Country Status (9)

Cited By (2)

Families Citing this family (3)

Cited By (2)

Also Published As

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Legal Events