DE1692249C3 - Process for reducing the chlorogenic acid content in green coffee beans - Google Patents

Process for reducing the chlorogenic acid content in green coffee beans

Info

Publication number
DE1692249C3
DE1692249C3 DE1967H0063466 DEH0063466A DE1692249C3 DE 1692249 C3 DE1692249 C3 DE 1692249C3 DE 1967H0063466 DE1967H0063466 DE 1967H0063466 DE H0063466 A DEH0063466 A DE H0063466A DE 1692249 C3 DE1692249 C3 DE 1692249C3
Authority
DE
Germany
Prior art keywords
chlorogenic acid
coffee beans
green coffee
reducing
acid content
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
DE1967H0063466
Other languages
German (de)
Other versions
DE1692249B2 (en
DE1692249A1 (en
Inventor
Guenter Dr. 6600 Saarbruecken Lehmann
Otto Prof. Dr. 6650 Homburg Neunhoeffer
Wilhelm Dr.- Ing. Roselius
Otto Dr.Rer.Nat. Vitzthum
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
HAG AG 2800 BREMEN
Original Assignee
HAG AG 2800 BREMEN
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by HAG AG 2800 BREMEN filed Critical HAG AG 2800 BREMEN
Priority to DE1967H0063466 priority Critical patent/DE1692249C3/en
Publication of DE1692249A1 publication Critical patent/DE1692249A1/en
Publication of DE1692249B2 publication Critical patent/DE1692249B2/en
Application granted granted Critical
Publication of DE1692249C3 publication Critical patent/DE1692249C3/en
Expired legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23FCOFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
    • A23F5/00Coffee; Coffee substitutes; Preparations thereof
    • A23F5/16Removing unwanted substances
    • A23F5/18Removing unwanted substances from coffee extract
    • A23F5/185Removing unwanted substances from coffee extract using flocculating, precipitating, adsorbing or complex-forming agents, or ion-exchangers
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23FCOFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
    • A23F5/00Coffee; Coffee substitutes; Preparations thereof
    • A23F5/16Removing unwanted substances

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Tea And Coffee (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)

Description

Die Erfindung betrifft ein Verfahren zur Verminderung des Chorogensäuregehaltes in Rohkaffeebohnen.The invention relates to a method for reducing the chorogenic acid content in green coffee beans.

Es gibt viele Menschen, die magenempfindlich sind und nach dem Genuß von Kaffee Magenschmerzen bekommen. Die Chlorogensäure gilt u.a. als Ursache der Unbekömmlichkeit von Kaffee bei Personen, die magen- und darmempfindlich sind. Seit Jahrzehnten wird deshalb bereits nach einem brauchbaren Weg gesucht, um Chlorogensäure, die in Kaffeebohnen zu 4% enthalten ist, zu vermindern, vgl. Trill ich, »Rösten und Röstwaren« (1934), Seiten 228 und 229.There are many people who have sensitive stomachs and have stomach pain after drinking coffee receive. The chlorogenic acid is one of the reasons why coffee is unpalatable for people who are sensitive to stomach and intestines. For decades, therefore, a useful way has been found sought to reduce chlorogenic acid, which is 4% in coffee beans, see Trill I, "Roasting and Roasted Products" (1934), pages 228 and 229.

Aus der GP-PS 8 67 613 ist es bekannt. Gerb- und Bitterstoffe, wie Leucoanthocyanine, aus Getränken, z. B. Bier, Wein und Fruchtsäften, durch Behandeln mit Polyamidpulver zu entfernen. Die Filtration ist jedoch mit Nachteilen verbunden, da die Absetzgeschwindigkeit des Polyamidpulvers gering ist und die Filterplatten alsbald verstopfen. Diese Nachteile sollen gemäß FR-PS 13 68 541 durch die Verwendung von Polyamidfeinfasern überwunden werden. Polyamidfeinfasern sollen sich besser zur Klärung und Geschmacksverbesserung von Gerbstoffe enthaltenden Getränken als Polyamidpulver eignen. Als spezielle Anwendungsform für Filterpapiere und Filterschichten aus Polyamidfeinfasern wird die Geschmacksverbesserung von Kaffee- und insbesondere Teeaufgüssen angeführt. Es ist dort nicht erwähnt, daß man in dieser Weise Chlorogensäure aus dem Kaffeeaufguß entfernen kann. Das Verfahren hat den Nachteil, daß dabei auch die typischen Röstprodukt-Geschmacksstoffe entfernt werden.It is known from GP-PS 8 67 613. Tanning and Bitter substances, such as leucoanthocyanines, from beverages, e.g. B. beer, wine and fruit juices by treating with Remove polyamide powder. However, the filtration is associated with disadvantages, since the settling rate of the polyamide powder is low and the filter plates clog up immediately. These disadvantages should according to FR-PS 13 68 541 can be overcome by using fine polyamide fibers. Polyamide fine fibers are supposed to better for clarifying and improving the taste of beverages containing tannins than polyamide powder suitable. As a special form of application for filter papers and filter layers made of fine polyamide fibers the improvement of the taste of coffee and especially tea infusions is stated. It is there does not mention that chlorogenic acid can be removed from the coffee infusion in this way. The procedure has the disadvantage that the typical roasted product flavors are also removed.

Die FR-PS 13 08 673 betrifft die Entfernung von Alkaloiden aus Tabak, ohne daß andere, erwünschte Inhaltsstoffe gleichzeitig entfernt werden. Hierzu behandelt man den Tabak mit einem organischen Lösungsmittel, das gesättigt ist an denjenigen Inhaltsstoffen des Tabaks, die man im Tabak belassen will, aber eine »Sättigungslücke« in bezug auf Alkaloide aufweist In dieser Weise extrahiert man nur die Alkaloide aus dem Tabak, nicht aber die anderen Inhaltsstoffe, die man ι ο im Tabak belassen möchte.The FR-PS 13 08 673 relates to the removal of alkaloids from tobacco, without other, desired Ingredients are removed at the same time. To do this, the tobacco is treated with an organic one Solvent that is saturated with those ingredients of tobacco that you want to leave in the tobacco, but has a "saturation gap" with respect to alkaloids. In this way, only the alkaloids are extracted the tobacco, but not the other ingredients that you ι ο want to leave in the tobacco.

Gegenstand der Erfindung ist ein Verfahren zur Verminderung des Chlorogensäuregehaltes in Rohkaffeebohnen, das dadurch gekennzeichnet ist, daß man grüne Kaffeebohnen mit einem gesättigten wäßrigen Extrakt aus grünen Kaffeebohnen, dem Chlorogensäure mit aktiviertem Polyamidpulver entzogen wurde, in Berührung bringt und die an Chlorogensäure verarmten grünen Kaffeebohnen von dem Extrakt trennt.The invention relates to a method for reducing the chlorogenic acid content in green coffee beans, which is characterized in that one green coffee beans with a saturated aqueous Green coffee bean extract, from which chlorogenic acid has been removed with activated polyamide powder, in Brings contact and separates the chlorogenic acid-depleted green coffee beans from the extract.

Die Aktivierung des verwendeten Polyamidpulvers erfolgt in bekannter Weise.The polyamide powder used is activated in a known manner.

Beispielexample

10 kg Rohkaffee wurden durch Dämpfen aufgeschlossen und auf einen Wassergehalt von 40 bis 45% gebracht 251 einer 13% Feststoff enthaltenden Rohkaffee-Extraktlösung, deren Chlorogensäuregehalt zuvor durch Behandlung mit 12 kg aktiviertem Polyamidpulver von 3,9% auf 2,0% vermindert worden war, wurden 4 Stunden mit dem aufgeschlossenen Rohkaffee bei 8O0C in Berührung gebracht.10 kg of green coffee were digested by steaming and brought to a water content of 40 to 45% of a green coffee extract solution containing 13% solids, the chlorogenic acid content of which had previously been reduced from 3.9% to 2.0% by treatment with 12 kg of activated polyamide powder 4 hours have been associated with the digested raw coffee at 8O 0 C into contact.

Nach Abtrennen der Extraktlösung wurden die behandelten Bohnen auf einen Wassergehalt von 10% getrocknet.After separating the extract solution, the treated beans were heated to a water content of 10% dried.

Die analytische Untersuchung des Rohkaffees ergabThe analytical examination of the green coffee showed

ioigenae werte:ioigenae values: ExtraktgehaltExtract content
%, bezogen auf% based on
TrockenmasseDry matter
Clilorogensäure-Chlorogenic acid
gchaltgchalt
%, bezogen auf% based on
TrockenmasseDry matter
II.
RohkaffeeGreen coffee 26,3
23,7
26.3
23.7
6,2
3,7
6.2
3.7
i
i
i
i
Vor Behandlung
Nach Behandlung
Before treatment
After treatment

Demnach wurde eine 40%ige Verminderung des Chlorogensäuregehalts im Rohkaffee erzielt.According to this, a 40% reduction in the chlorogenic acid content in the green coffee was achieved.

Claims (1)

Patentanspruch:Claim: Verfahren zur Verminderung des Chlorogensäuregehaltes in Rohkaffeebohnen, dadurch gekennzeichnet, daß man grüne Kaffeebohnen mit einem gesättigten wäßrigen Extrakt aus grünen Kaffeebohnen, dem Chlorogensäure mit aktiviertem Polyamidpulver entzogen wurde, in Berührung bringt und die an Chlorogensäure verarmten grünen Kaffeebohnen von dem Extrakt trenntProcess for reducing the chlorogenic acid content in green coffee beans, characterized in that one is green coffee beans with a saturated aqueous extract from green coffee beans, the chlorogenic acid with activated Polyamide powder was withdrawn, brings into contact and the chlorogenic acid-depleted green Separates coffee beans from the extract
DE1967H0063466 1967-07-31 1967-07-31 Process for reducing the chlorogenic acid content in green coffee beans Expired DE1692249C3 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
DE1967H0063466 DE1692249C3 (en) 1967-07-31 1967-07-31 Process for reducing the chlorogenic acid content in green coffee beans

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE1967H0063466 DE1692249C3 (en) 1967-07-31 1967-07-31 Process for reducing the chlorogenic acid content in green coffee beans

Publications (3)

Publication Number Publication Date
DE1692249A1 DE1692249A1 (en) 1971-05-13
DE1692249B2 DE1692249B2 (en) 1977-09-22
DE1692249C3 true DE1692249C3 (en) 1978-05-24

Family

ID=7162322

Family Applications (1)

Application Number Title Priority Date Filing Date
DE1967H0063466 Expired DE1692249C3 (en) 1967-07-31 1967-07-31 Process for reducing the chlorogenic acid content in green coffee beans

Country Status (1)

Country Link
DE (1) DE1692249C3 (en)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CH633165A5 (en) * 1978-09-14 1982-11-30 Nestle Sa PROCESS FOR DEACIDIFYING COFFEE EXTRACT AND DEACIDIFIED EXTRACT OBTAINED.
CH637809A5 (en) * 1979-04-18 1983-08-31 Nestle Sa PROCESS FOR DEACIDIFYING COFFEE EXTRACT AND DEACIDIFIED EXTRACT OBTAINED.
EP0666033B1 (en) * 1994-02-03 1997-10-22 Kraft Foods, Inc. Process for decaffeinating aqueous caffeine-containing green coffee extracts
EP2601844B1 (en) * 2011-12-05 2015-10-21 Plantextrakt GmbH&Co. Kg Method of producing an extract enriched with trigonelline (TRIG) and/or chlorogenic acids (CQA)
US11324244B2 (en) 2013-07-03 2022-05-10 Conopco Inc. Potato derived flavour enhancing composition and method for the manufacture thereof

Also Published As

Publication number Publication date
DE1692249B2 (en) 1977-09-22
DE1692249A1 (en) 1971-05-13

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