DE10341615A1 - Process for the preparation of xylylenediamine - Google Patents
Process for the preparation of xylylenediamine Download PDFInfo
- Publication number
- DE10341615A1 DE10341615A1 DE2003141615 DE10341615A DE10341615A1 DE 10341615 A1 DE10341615 A1 DE 10341615A1 DE 2003141615 DE2003141615 DE 2003141615 DE 10341615 A DE10341615 A DE 10341615A DE 10341615 A1 DE10341615 A1 DE 10341615A1
- Authority
- DE
- Germany
- Prior art keywords
- xylylenediamine
- preparation
- nmp
- hydrogenation
- pyrrolidone
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/44—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers
- C07C209/48—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers by reduction of nitriles
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Verfahren zur Herstellung von Xylylendiamin durch Hydrierung von Phthalodinitril in Gegenwart eines Heterogenkatalysators, wobei die Hydrierung in Gegenwart von N-Methyl-2-pyrrolidon (NMP) als Lösungsmittel durchgeführt wird.A process for the preparation of xylylenediamine by hydrogenating phthalonitrile in the presence of a heterogeneous catalyst, wherein the hydrogenation is carried out in the presence of N-methyl-2-pyrrolidone (NMP) as solvent.
Priority Applications (15)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE2003141615 DE10341615A1 (en) | 2003-09-10 | 2003-09-10 | Process for the preparation of xylylenediamine |
PCT/EP2004/009882 WO2005026101A1 (en) | 2003-09-10 | 2004-09-04 | Method for producing xylylenediamine |
EP04764998A EP1663947B1 (en) | 2003-09-10 | 2004-09-09 | Method for the production of diaminoxylene by continuous hydrogenation of liquid phthalonitrile |
PCT/EP2004/010062 WO2005026098A1 (en) | 2003-09-10 | 2004-09-09 | Method for the production of diaminoxylene by continuous hydrogenation of liquid phthalonitrile |
AT04764997T ATE380788T1 (en) | 2003-09-10 | 2004-09-09 | METHOD FOR PRODUCING XYLYLENEDIAMINE BY CONTINUOUS HYDROGENATION OF LIQUID PHTHALODINITRILE |
PCT/EP2004/010063 WO2005026099A1 (en) | 2003-09-10 | 2004-09-09 | Method for the production of diaminoxylene by continuous hydrogenation of liquid phthalonitrile |
DE502004005718T DE502004005718D1 (en) | 2003-09-10 | 2004-09-09 | METHOD FOR THE PRODUCTION OF XYLYLENDIAMINE BY CONTINUOUS HYDROGENATION OF LIQUID PHTHALODINITRILE |
US10/570,099 US7339080B2 (en) | 2003-09-10 | 2004-09-09 | Method for the production of diaminoxylene by continuous hydrogenation of liquid phthalonitrile |
JP2006525765A JP4406645B2 (en) | 2003-09-10 | 2004-09-09 | Process for the production of xylylenediamine by continuous hydrogenation of liquid phthalonitrile |
EP04764997A EP1663946B1 (en) | 2003-09-10 | 2004-09-09 | Method for the production of diaminoxylene by continuous hydrogenation of liquid phthalonitrile |
DE502004005974T DE502004005974D1 (en) | 2003-09-10 | 2004-09-09 | METHOD FOR THE PRODUCTION OF XYLYLENDIAMINE BY CONTINUOUS HYDROGENATION OF LIQUID PHTHALODINITRILE |
KR1020067004871A KR101106334B1 (en) | 2003-09-10 | 2004-09-09 | Method for the production of diaminoxylene by continuous hydrogenation of liquid phthalonitrile |
AT04764998T ATE384037T1 (en) | 2003-09-10 | 2004-09-09 | METHOD FOR PRODUCING XYLYLENEDIAMINE BY CONTINUOUS HYDROGENATION OF LIQUID PHTHALODINITRILE |
KR1020067004869A KR101103220B1 (en) | 2003-09-10 | 2004-09-09 | Method for the production of diaminoxylene by continuous hydrogenation of liquid phthalonitrile |
JP2006525766A JP4495730B2 (en) | 2003-09-10 | 2004-09-09 | Process for the production of xylylenediamine by continuous hydrogenation of liquid phthalodinitrile |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE2003141615 DE10341615A1 (en) | 2003-09-10 | 2003-09-10 | Process for the preparation of xylylenediamine |
Publications (1)
Publication Number | Publication Date |
---|---|
DE10341615A1 true DE10341615A1 (en) | 2005-04-28 |
Family
ID=34305634
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE2003141615 Withdrawn DE10341615A1 (en) | 2003-09-10 | 2003-09-10 | Process for the preparation of xylylenediamine |
Country Status (2)
Country | Link |
---|---|
DE (1) | DE10341615A1 (en) |
WO (1) | WO2005026101A1 (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US7339080B2 (en) | 2003-09-10 | 2008-03-04 | Basf Aktiengesellschaft | Method for the production of diaminoxylene by continuous hydrogenation of liquid phthalonitrile |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE10341613A1 (en) | 2003-09-10 | 2005-04-14 | Basf Ag | Process for the preparation of xylylenediamine |
KR100613404B1 (en) * | 2005-03-24 | 2006-08-17 | 한국과학기술연구원 | Preparation of xylylenediamine using imidazole as a solvent |
KR20080033480A (en) | 2005-08-02 | 2008-04-16 | 바스프 에스이 | Process for preparing xylylenediamine by continuous hydrogenation of phthalonitrile |
DE602006004279D1 (en) | 2005-09-09 | 2009-01-29 | Mitsubishi Gas Chemical Co | A process for the preparation of amino compounds having an aromatic ring using a shell catalyst |
US8142618B2 (en) | 2006-02-01 | 2012-03-27 | Basf Aktiengesellschaft | Processes for preparing pure xylylenediamine |
DE602007003135D1 (en) | 2006-05-18 | 2009-12-24 | Mitsubishi Gas Chemical Co | Process for the preparation of xylylenediamine |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
BE700877A (en) * | 1966-07-04 | 1967-12-18 | ||
DE2153693A1 (en) * | 1971-10-28 | 1973-05-03 | Dynamit Nobel Ag | PROCESS FOR PRODUCING 1,4 DIAMINOPHTHALAZINE |
US4539189A (en) * | 1984-01-23 | 1985-09-03 | Chevron Research Company | Method for removing sulfides from industrial gas |
DE3935112A1 (en) * | 1989-10-21 | 1991-04-25 | Basf Ag | METHOD FOR PRODUCING AMINES |
DE10056840A1 (en) * | 2000-11-16 | 2002-05-23 | Basf Ag | Continuous hydrogenation of nitrites to primary amines over activated Raney catalyst, involves hydrogenating nitrites in absence of ammonia and basic alkali or alkaline earth metal compounds |
JP5017756B2 (en) * | 2001-07-16 | 2012-09-05 | 三菱瓦斯化学株式会社 | Method for producing high purity metaxylylenediamine |
-
2003
- 2003-09-10 DE DE2003141615 patent/DE10341615A1/en not_active Withdrawn
-
2004
- 2004-09-04 WO PCT/EP2004/009882 patent/WO2005026101A1/en active Application Filing
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US7339080B2 (en) | 2003-09-10 | 2008-03-04 | Basf Aktiengesellschaft | Method for the production of diaminoxylene by continuous hydrogenation of liquid phthalonitrile |
Also Published As
Publication number | Publication date |
---|---|
WO2005026101A1 (en) | 2005-03-24 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
8130 | Withdrawal |