CO2018008428A2 - Proceso de hidrogenación catalítico para preparar pirazoles - Google Patents

Proceso de hidrogenación catalítico para preparar pirazoles

Info

Publication number
CO2018008428A2
CO2018008428A2 CONC2018/0008428A CO2018008428A CO2018008428A2 CO 2018008428 A2 CO2018008428 A2 CO 2018008428A2 CO 2018008428 A CO2018008428 A CO 2018008428A CO 2018008428 A2 CO2018008428 A2 CO 2018008428A2
Authority
CO
Colombia
Prior art keywords
catalytic hydrogenation
hydrogenation process
pyrazoles
acids
prepare
Prior art date
Application number
CONC2018/0008428A
Other languages
English (en)
Inventor
Eric George Klauber
Michael Rack
Sebastian Soergel
Birgit Gockel
Roland Goetz
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of CO2018008428A2 publication Critical patent/CO2018008428A2/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/18—Carbon
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B01J23/42—Platinum
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/16—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of hydrazones
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C251/00—Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C251/72—Hydrazones
    • C07C251/74—Hydrazones having doubly-bound carbon atoms of hydrazone groups bound to hydrogen atoms or to acyclic carbon atoms
    • C07C251/76—Hydrazones having doubly-bound carbon atoms of hydrazone groups bound to hydrogen atoms or to acyclic carbon atoms to carbon atoms of a saturated carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D401/00—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom
    • C07D401/02—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings
    • C07D401/12—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings linked by a chain containing hetero atoms as chain links
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D403/00—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, not provided for by group C07D401/00
    • C07D403/02—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, not provided for by group C07D401/00 containing two hetero rings
    • C07D403/12—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, not provided for by group C07D401/00 containing two hetero rings linked by a chain containing hetero atoms as chain links

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

RESUMEN La presente invención se refiere a un proceso catalítico para preparar pirazoles que comprende la etapa de ciclar compuestos de carbonilo α,β-insaturados sustituidos por hidrazona mediante su reacción con hidrógeno en una mezcla de reacción que comprende como componentes (a) un catalizador de hidrogenación, (b) un ácido seleccionado de ácidos de Brønsted, sales de amonio de ácidos de Brønsted y ácidos de Lewis, (c) un solvente prótico y opcionalmente (d) un solvente aprótico.
CONC2018/0008428A 2016-02-02 2018-08-10 Proceso de hidrogenación catalítico para preparar pirazoles CO2018008428A2 (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP16153833 2016-02-02
PCT/EP2017/051524 WO2017133942A1 (en) 2016-02-02 2017-01-25 Catalytic hydrogenation process for preparing pyrazoles

Publications (1)

Publication Number Publication Date
CO2018008428A2 true CO2018008428A2 (es) 2018-08-21

Family

ID=55304873

Family Applications (1)

Application Number Title Priority Date Filing Date
CONC2018/0008428A CO2018008428A2 (es) 2016-02-02 2018-08-10 Proceso de hidrogenación catalítico para preparar pirazoles

Country Status (20)

Country Link
US (1) US10975036B2 (es)
EP (1) EP3411360B1 (es)
JP (1) JP6900400B2 (es)
KR (1) KR102651666B1 (es)
CN (1) CN108699003B (es)
AU (1) AU2017216082B2 (es)
BR (1) BR112018014357B8 (es)
CA (1) CA3010561C (es)
CL (1) CL2018002075A1 (es)
CO (1) CO2018008428A2 (es)
DK (1) DK3411360T3 (es)
ES (1) ES2795874T3 (es)
IL (1) IL260375B (es)
MX (1) MX2018009453A (es)
PE (1) PE20181539A1 (es)
PL (1) PL3411360T3 (es)
PT (1) PT3411360T (es)
RU (1) RU2733958C2 (es)
WO (1) WO2017133942A1 (es)
ZA (1) ZA201805742B (es)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TR201909606T4 (tr) 2014-07-31 2019-07-22 Basf Se Pi̇razollari hazirlamak i̇çi̇n i̇şlem
ES2856454T3 (es) 2015-05-08 2021-09-27 Basf Agro Bv Procedimiento para la preparación de epóxido de terpinoleno.
DK3294700T3 (da) 2015-05-08 2020-04-14 Basf Agro Bv Fremgangsmåde til fremstilling af limonen-4-ol
KR20230145498A (ko) 2015-05-11 2023-10-17 바스프 에스이 4-아미노-피리다진의 제조 방법
AU2017286055B2 (en) 2016-06-15 2021-07-01 BASF Agro B.V. Process for the epoxidation of a tetrasubstituted alkene
KR20190017926A (ko) 2016-06-15 2019-02-20 바스프 아그로 비.브이. 사치환된 알켄의 에폭시화 방법
CN109415280A (zh) 2016-07-07 2019-03-01 巴斯夫欧洲公司 用于制备杀虫环戊烯类化合物的Oxy-Cope重排
SI3535257T1 (sl) 2016-11-04 2021-04-30 Basf Se Proces za čiščenje prirazolpiridazinov
US10538493B2 (en) 2016-11-17 2020-01-21 Basf Se Process for the purification of 1-(4-chlorophenyl)pyrazol-3-ol
WO2018137959A1 (en) 2017-01-25 2018-08-02 Basf Se Process for preparation of benzylic amides
JP7005651B2 (ja) 2017-03-20 2022-01-21 ビーエーエスエフ ソシエタス・ヨーロピア ブロモトリクロロメタンを調製する方法
WO2019086545A1 (en) 2017-11-02 2019-05-09 Basf Se Process for preparing 4-chlorobenzyl propargyl ether

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JP2007326784A (ja) * 2006-06-06 2007-12-20 Sagami Chem Res Center １−置換−５−フルオロアルキルピラゾール−４−カルボン酸エステルの製造方法
US20110189167A1 (en) 2007-04-20 2011-08-04 Flynn Daniel L Methods and Compositions for the Treatment of Myeloproliferative Diseases and other Proliferative Diseases
US20080269267A1 (en) * 2007-04-20 2008-10-30 Deciphera Pharmaceuticals, Llc Kinase inhibitors useful for the treatment of myleoprolific diseases and other proliferative diseases
RU2516290C2 (ru) 2007-08-27 2014-05-20 Басф Се Пиразольные соединения и их использование в способе борьбы с беспозвоночными вредителями, в способе защиты материала размножения растений, в способе лечения или защиты животных от инвазии или инфицирования, в материале размножения растений и сельскохозяйственные композиции, содержащие пиразольные соединения
WO2009068652A1 (en) * 2007-11-30 2009-06-04 Smithkline Beecham Corporation 2, 6-disubstituted pyridines and 2, 4-disubstituted pyrimidines as soluble guanylate cyclase activators
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EP2236505A1 (de) 2009-04-03 2010-10-06 Bayer CropScience AG Acylierte Aminopyridine und - pyridazine als Insektizide
AR076984A1 (es) 2009-06-08 2011-07-20 Merck Serono Sa Derivados de pirazol oxadiazol
KR102168241B1 (ko) 2011-04-12 2020-10-22 써메디컬, 인코포레이티드 유체 강화 절제에서 요법을 성형하기 위한 장치 및 방법
BR112013024708B1 (pt) * 2011-04-21 2018-10-09 Basf Se compostos de pirazol,composições, métodos para combater ou controlar pragas invertebradas e para proteger plantas em crescimento, processo para proteger sementes e uso dos compostos
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TR201909606T4 (tr) * 2014-07-31 2019-07-22 Basf Se Pi̇razollari hazirlamak i̇çi̇n i̇şlem
KR20230145498A (ko) 2015-05-11 2023-10-17 바스프 에스이 4-아미노-피리다진의 제조 방법

Also Published As

Publication number Publication date
CN108699003B (zh) 2023-02-03
ES2795874T3 (es) 2020-11-25
BR112018014357B1 (pt) 2022-08-16
DK3411360T3 (da) 2020-06-08
AU2017216082A1 (en) 2018-07-26
CN108699003A (zh) 2018-10-23
US10975036B2 (en) 2021-04-13
CA3010561A1 (en) 2017-08-10
RU2733958C2 (ru) 2020-10-08
ZA201805742B (en) 2019-11-27
WO2017133942A1 (en) 2017-08-10
EP3411360A1 (en) 2018-12-12
AU2017216082B2 (en) 2020-12-03
RU2018130339A3 (es) 2020-03-19
JP6900400B2 (ja) 2021-07-07
CL2018002075A1 (es) 2018-09-14
PE20181539A1 (es) 2018-09-26
EP3411360B1 (en) 2020-03-11
IL260375B (en) 2021-03-25
BR112018014357B8 (pt) 2022-09-06
KR102651666B1 (ko) 2024-03-26
BR112018014357A2 (pt) 2018-12-18
KR20180104743A (ko) 2018-09-21
PT3411360T (pt) 2020-06-01
US20190055200A1 (en) 2019-02-21
RU2018130339A (ru) 2020-03-04
CA3010561C (en) 2024-04-16
JP2019504883A (ja) 2019-02-21
MX2018009453A (es) 2018-09-21
PL3411360T3 (pl) 2020-08-24

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