CN85101482A - Tobacco composition and preparation method thereof - Google Patents
Tobacco composition and preparation method thereof Download PDFInfo
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- CN85101482A CN85101482A CN 85101482 CN85101482A CN85101482A CN 85101482 A CN85101482 A CN 85101482A CN 85101482 CN85101482 CN 85101482 CN 85101482 A CN85101482 A CN 85101482A CN 85101482 A CN85101482 A CN 85101482A
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Abstract
The tobacco composition that contains bluish dogbane, bluish dogbane additive wherein can be a Folium Apocyni Veneti, can be apocynum extract also, smoke cigarette, cigar and the pipe tobacco made by the tobacco composition that contains bluish dogbane and can improve, treat chronic bronchitis by caused by smoking.
Description
The present invention relates to tobacco composition that contains bluish dogbane and preparation method thereof, say more properly, the present invention relates to contain apocynum extract or contain the new tobacco composition of Folium Apocyni Veneti that it has and reduces phlegm, cough-relieving slows down, improves usefulness such as chronic bronchitis and PFT.
Since the sixties, Britain and U.S. government announced that Smoking is harmful to your health, all carried out the research of the theoretical and practice of safe tobacco in the world wide.Developed at present and established and improved burning condition, reduced main flow flue gas in tobacco tar, nicotine, the industrial process of carbon monoxide content.This comprises the ventilated cigarettes production technology, manually synthetic low tar tabacco technology, expanding tobacco technology, and the technology that applies additive in tobacco.
Apply the existing a lot of report of technology of additive in tobacco, the additive major part is a chemical addition agent, for example: Metal Palladium or its esters, nitrate, silicate, and carbohydrate etc.Referring to: United States Patent (USP) 3338246; 2429567; 4248251; German patent specification 817717; Above-mentioned various additive all improves the result of combustion of tobacco condition, reduces main flume tar, and nicotine and carbon monoxide content have certain effect.
The present invention relates to use extract of Chinese herb bluish dogbane or Folium Apocyni Veneti to be tobacco additive agent, the preparation tobacco composition.The bluish dogbane tobacco composition removes to have to be alleviated and opposing main flume tar, outside the effect of nicotine and carbon monoxide content, have also that cost is low, technical process simply, be easy to industrial characteristics.In addition, main is that this tobacco composition has clearing phlegm and relieving cough, improves, treats by the chronic bronchitis of caused by smoking and the usefulness of PFT.
The chronic bronchitis that is caused by smoking also is smoking to one of main harm of human body; And the research to this disease is very few in the world at present, yet there are no any successful report.
Research of safety low-poison tobacco and production are the urgent task that present World tobacco industry faces.Its purpose mainly is in order to slow down or to prevent and treat diseases such as the lung cancer that caused by smoking, coronary heart disease.Yet the patient of the chronic bronchitis that our discovery is caused by smoking occupies the first place that smoking is caused a disease.This class patient accounts for bronochitic's 50～80%.The present invention just is being based on above reason and is developing the tobacco composition that contains apocynum extract or Folium Apocyni Veneti with preventing phlegm from forming and stopping coughing effect.Tool novelty of the present invention belongs to original invention.
Bluish dogbane is a Chinese herb.It contains Quercetin, phytosterin compound, multiple components such as anthraquinone, amino acid through chemical analysis.The pharmacological testing proof is nontoxic.Chinese Pharmacopoeia (1977) is on the books to it.Quercetin chemical constitution in the bluish dogbane is clear, and chemical name is: 3,5,7,3 ' 4 '-pentahydroxyflavone.It has eliminates the phlegm, antibechic, flat effect such as coughs.
First aspect of the present invention relates to new being used to and makes cigarette, the tobacco composition that contains apocynum extract of cigar and pipe tobacco, and this mixture comprises:
A) tobacco;
B) at least 0.1% apocynum extract is in the weight of its butt, tobacco composition.
Second aspect of the present invention relates to new being used to and makes cigarette, the Folium Apocyni Veneti of cigar and pipe tobacco and the mixture of tobacco, and this mixture comprises:
A) tobacco;
B) at least 1% Folium Apocyni Veneti is in the weight of its butt, tobacco composition.
The 3rd aspect of the present invention relates to the preparation method of the tobacco composition that contains apocynum extract that is used to make cigarette, cigar and pipe tobacco.
Unless otherwise indicated, the proportioning of the tobacco composition that this paper is related is all with its butt, and percentage by weight is a benchmark.
The present invention mixes apocynum extract or Folium Apocyni Veneti with tobacco, make cigarette, cigar and pipe tobacco, the smoker inhale the combustion they the time, the fumicants that contains the bluish dogbane effective ingredient will act on the upper respiratory tract, reach and slow down, improve the purpose of smoker's chronic bronchitis.The effect of foregoing invention has been carried out pharmacology, clinical verification by the authoritative health service unit of China.
The tobacco composition that preparation contains bluish dogbane can be divided into two kinds of methods.
1) tobacco that will be used to make cigarette, cigar and pipe tobacco and general a small amount of tobacco additive agent mix mutually with by fermentation Folium Apocyni Veneti.Be at least 1% with the amount of the Folium Apocyni Veneti of tobacco composition, be generally 1～50%, in the weight of its butt, tobacco composition.
When making cigarette and pipe tobacco with the above-mentioned tobacco composition that contains Folium Apocyni Veneti, wherein the content of Folium Apocyni Veneti with account for tobacco composition 20～40% for good, be that the suction flavor and the curative effect of 15～25% o'clock tobacco compositions is the best with its content especially.
When making cigar with the above-mentioned tobacco composition that contains Folium Apocyni Veneti, the content with Folium Apocyni Veneti is that suction in 25～35% o'clock is distinguished the flavor of and curative effect is the best especially.
2) use polar solvent, for example water, ethanol etc. extract bluish dogbane or Folium Apocyni Veneti, and extract is concentrated, and drying makes apocynum extract, and the drug effect of its 1 gram approximates the Folium Apocyni Veneti of 10 grams greatly.Apocynum extract is mixed with a small amount of general tobacco additive agent earlier, then be used to make cigarette, the tobacco mixing of cigar and pipe tobacco.Apocynum extract can be a dry, also can be the aqueous solution.The apocynum extract that mixes with tobacco is at least 0.1%, is generally 0.1～10%, with its butt, and the weight meter of tobacco composition.
When making cigarette and pipe tobacco with above-mentioned tobacco composition, its apocynum extract is good to account for 0.5～4% of tobacco composition, is the best with 0.5～1.5% especially.When making cigar with above-mentioned tobacco composition, its apocynum extract is good to account for 0.5～4% of tobacco composition, is best especially with 2-4%.When the amount of apocynum extract is 4% when following of tobacco composition, tobacco composition has the curative effect of treatment tracheitis, and does not influence and inhale flavor.
The solvent that extracts apocynum extract is best with water, because water is pollution-free, residues in the tobacco composition and has no side effect, and need not reclaim.
Be that the method that solvent prepares apocynum extract is with water: place one to have in the equipment of stirring clean bluish dogbane or Folium Apocyni Veneti, the water that adds q.s, available heater, also can directly spray into steam in it, boiling 0.5～4 hour is filtered then, decompression distillation, temperature is not higher than 80 ℃, and under vacuum, temperature is not higher than about 1 hour of 80 ℃ of dryings at last.Generally can get the extract of Folium Apocyni Veneti amount 1/10.The apocynum extract that is equipped with gained through last legal system has following feature:
Color: brown.
Taste: little puckery.
Quercetin content: 0.1～1.5%.
Solubility test: dry apocynum extract mixes by 1: 20 with hot water, should all dissolve at 80 ℃, and precipitation must not be arranged.
To use polar solvent, particularly mix with tobacco as follows with the form of the dry or the aqueous solution as the apocynum extract that solvent makes, be used to make cigarette, cigar and pipe tobacco with water.
Apocynum extract and other general tobacco additive agent are mixed, add the water of q.s, in the equipment that steam jacket or other heater are arranged, heat and boil, and stir.Mix, stop heating, be cooled to 45～60 ℃, filter, filtrate is added on the tobacco leaf surface of the softness of warming and humidifying., stored under 60～75% relative humidity 2～48 hours at 25～35 ℃ through the tobacco leaf of above-mentioned reinforced processing.As requested it further is processed into cigarette then, cigar or pipe tobacco.The apocynum extract that adds in said method is at least 0.1%, is generally 0.1～10%, and optimum amount is 0.5～4% to decide according to the kind of institute's tobacco curing product.
Prepare the mixture of Folium Apocyni Veneti and tobacco with above-mentioned method, be processed into cigarette then, the patient of the chronic bronchitis that 100 examples are caused by smoking treats.The patient at first smokes the cigarette of being made by the tobacco composition that contains 40% Folium Apocyni Veneti, every day 10 times, each 2, continuous 15 days.And then smoke the cigarette of making by the tobacco composition that contains 20% Folium Apocyni Veneti.Be no more than 20 every day, connect and inhaled 30 days.Curative effect is as follows:
| The treatment number | Produce effects | Take a turn for the better | Invalid | Total effective rate % |
| 100 | 42 | 40 | 18 | 82 |
Prepare the mixture of Folium Apocyni Veneti and tobacco with preceding method, be processed into cigar then, the patient that 106 examples are suffered with chronic bronchitis treats.Patient's smoke a cigar is made by 30% Folium Apocyni Veneti and 70% tobacco.Be no more than 5 for each person every day, each half, it is as follows to inhale 30 days (size of cigar is about a times of regular-size cigarette) curative effect continuously:
| The treatment number | Produce effects | Take a turn for the better | Invalid | Total effective rate |
| 106 | 34 | 67 | 5 | 95.3 |
Prepare the tobacco composition that contains 1% bluish dogbane water extract with preceding method, make cigarette with this mixture, the patient that 43 examples are suffered with chronic bronchitis treats.10～20 of smokings for each person every day amount to smoking 60 days.Curative effect is as follows:
| Clinic control | Produce effects | Take a turn for the better | Invalid | Total effective rate |
| 11.4% | 54.5% | 27.3% | 6.8% | 93.2% |
More than the diagnosis of each efficacy determination and tracheitis all judge it with " Chinese chronic bronchitis diagnosis typing and curative effect determinate standard ".
The bluish dogbane tobacco composition is except that having the bronchitic obvious curative effects of above-mentioned treatment, and test confirms that also it has following effect through the authoritative medical science unit of China:
1, the more similar carbon monoxide content low 15% that does not contain the cigarette of bluish dogbane of cigarette that makes with the tobacco composition that contains 1% apocynum extract.
2, the cigarette smoke that makes with the tobacco composition that contains 1.5% apocynum extract carries out toxicity test to white mouse, record the white mouse median lethal dose with contrast cigarette smog contrast test, the result shows that the comparison of bluish dogbane cigarette smoke toxicity is little by 23% according to cigarette smoke toxicity.
3, compare with other cigarette, the cigarette that suction contains bluish dogbane is minimum to influence of Pulmonary Function, wherein residual gas accounts for total lung capacity percentage average annual growth value and 25% and breathes all identical with normal non-smoking people of lung capacity flow velocity, has confirmed to spread out cigarette many than other cigarette safety.
4, the result of TA98 mutagenicity test shows that the cigarette mutagenesis ability that contains bluish dogbane is lower than the cigarette that does not contain bluish dogbane, confirms that this cigarette has the mutation effect of pressing down.
5, the platelet aggregation of inhaling the cigarette person contain bluish dogbane makes moderate progress.
Through evidence, apocynum extract contains Quercetin, and calculating its content with flavonoids is 0.1～1.5%, and Quercetin has expelling phlegm and arresting coughing usefulness.
The present invention further describes in detail and is illustrated by the following examples, but embodiment not delimit the scope of the invention.
Embodiment 1
The preparation of bluish dogbane water extract
Folium Apocyni Veneti places one to have in the reflecting device of agitating device for 100 kilograms, adds 1000 kilograms of entry, and heating was stirred 2 hours under slight boiling condition.Cooling final vacuum suction filtration gets 830 kilograms of filtrates.Concentrate 80 ℃ of decompressions, get 18 kilograms of concentrates.80 ℃ of dryings are 1 hour under vacuum condition, obtain 10 kilograms of dry apocynum extracts.
Feature is as follows:
Color: brown.
Taste: little puckery.
Quercetin content: 0.98%(is in flavonoids).
Solubility test: dry bluish dogbane water extract mixes with hot water at 1: 20,80 ℃ of all dissolvings.
Embodiment 2
Contain the preparation of the tobacco composition of 0.5% bluish dogbane water extract
(1) with 49.1 kilograms of prescription tobacco leaves uniformly that are mixed, the economy-combat leaf goes to carry out the reinforced processing of leaves moisting behind the stalk, and is in the leaves moisting tube that tobacco leaf is loose, and heats to 50 ℃ with the cycling hot humid air;
(2) the dry bluish dogbane water extract that will make with the method for embodiment 1 places in the mini-plant for 0.25 kilogram, adds 0.5 kilogram of glucose, 0.025 kilogram of liquorice beverage extract, and 0.125 kilogram of liquor mixes.Add an amount of water, be heated to little boiling, filter, be cooled to 50 ℃;
(3) will be sprayed onto by on the finished tobacco of step (1) surface by steam jet with the mixed liquor that step (2) make, make the wet eventually amount of tobacco leaf reach 20%,, under relative humidity 70% condition above-mentioned tobacco composition was stored 4 hours at last at 30 ℃.Make cigarette with common process, cigar and pipe tobacco.
Embodiment 3
Contain the preparation of the tobacco composition of 4% bluish dogbane water extract
(1) the prescription tobacco leaves uniformly that are mixed of 46.4 kilograms after the economy-combat leaf is gone to obstruct carry out that leaves moisting is reinforced to be handled.In the leaves moisting tube that tobacco leaf is loose, and with cycling hot humid air humidification to 60 ℃;
(2) the dry bluish dogbane water extract that will make with the method for embodiment 1 places in the mini-plant for 2 kilograms, adds 1 kilogram of glucose, 0.1 kilogram of licorice, and 0.25 kilogram of red date tincture, liquor mixes for 0.25 kilogram.Add an amount of water, be heated to little boiling, filter, be cooled to 60 ℃;
(3) the mixed liquor compressed air that step (2) is made is that carrier gas is sprayed onto by on the finished tobacco leaf surface of step (1).The whole water capacity of tobacco leaf is 18%.At 35 ℃, under relative humidity 80% condition above-mentioned tobacco composition was stored 8 hours at last.Require to make cigarette, cigar, and pipe tobacco with common process then.
Embodiment 4
Contain the preparation of the tobacco composition of 1% bluish dogbane water extract
(1) 12 kilograms of offals is sent into spiral and steamed the hot and humid processing of stalk machine, and add the dry bluish dogbane water extract of 0.15 kilogram of powdery.Stalk moisture content after reinforced the processing is 28%, 75 ℃ of humidity, and cooling was subsequently stored 6 hours.
(2) the bluish dogbane water extract with 0.35 kilogram of drying places in the mini-plant, adds 1 kilogram of glucose, 0.05 kilogram of licorice, and 0.25 kilogram of liquor stirs, and mixes.Add an amount of water, be heated to little boiling, filter and to be cooled to 50 ℃, it is sprayed onto on 36.2 kilograms the tobacco leaf (this tobacco leaf through and embodiment 2, the identical step process of step (1) is crossed).
(3) tobacco leaf and the offal with above-mentioned treated mistake mixes, and stores to be used to make cigarette after 4 hours, cigar, and pipe tobacco.
Embodiment 5
Contain the preparation of the tobacco composition of 20% Folium Apocyni Veneti
40 kilograms of uniform tobacco leaves that are mixed are made be the blade of 12.5mm more than 80%, subsequently 10 kilograms of Folium Apocyni Venetves of handling by fermentation are with tobacco leaf in the preceding batching of leaves moisting tube and are evenly mixed, press the reinforced processing of conventional method then, make cigarette, cigar, and pipe tobacco.
Embodiment 6
Contain the preparation of the tobacco composition of 30% Folium Apocyni Veneti
35 kilograms of uniform tobacco leaves that are mixed are made be the blade of 12.5mm more than 80%, subsequently 15 kilograms of Folium Apocyni Venetves of handling by fermentation are with tobacco leaf in the preceding batching of leaves moisting tube and are evenly mixed, press the reinforced processing of conventional method then, make cigarette, cigar, and pipe tobacco.
Claims (17)
1, the tobacco composition that contains tobacco and tobacco additive agent commonly used is characterized in that this mixture contains at least 0.1% apocynum extract in addition, in the weight of tobacco composition.
2,, it is characterized in that apocynum extract wherein is 0.1～10%, in the weight of tobacco composition according to claim 1 described tobacco composition.
3,, it is characterized in that apocynum extract wherein is 0.5～4%, in the weight of tobacco composition according to claim 2 described tobacco compositions.
4, according to claim 3 described tobacco compositions when being used to make cigarette and pipe tobacco, it is characterized in that apocynum extract wherein is 0.5～1.5%, in the weight of tobacco composition.
5, according to claim 2 described tobacco compositions when being used to make cigar, it is characterized in that apocynum extract wherein is 2-4%, in the weight of tobacco composition.
6,, it is characterized in that apocynum extract wherein can be a dry according to claim 1 described tobacco composition.Also can be the aqueous solution.
7,, it is characterized in that apocynum extract wherein extracts from bluish dogbane or Folium Apocyni Veneti according to claim 1 described tobacco composition.
8,, it is characterized in that apocynum extract wherein contains 0.1～1.5% Quercetin, in the weight of apocynum extract according to claim 1 described tobacco composition.
9, the tobacco composition that contains tobacco and tobacco additive agent commonly used is characterized in that this mixture contains at least 1% Folium Apocyni Veneti in addition, in the weight of tobacco composition.
10,, it is characterized in that Folium Apocyni Veneti wherein is 1～50%, in the weight of tobacco composition according to claim 9 described tobacco compositions.
11, according to claim 10 described tobacco compositions when being used to make cigarette and pipe tobacco, it is characterized in that Folium Apocyni Veneti wherein is 15～25%, in the weight of tobacco composition.
12, according to claim 10 described tobacco compositions when being used to make cigar, it is characterized in that Folium Apocyni Veneti wherein is 25～35%, in the weight of tobacco composition.
13, preparation contains the method for the tobacco composition of apocynum extract, it is characterized in that:
A, the water that will spread out extract and other tobacco additive agent and q.s boil in firing equipment, and fully mix;
B, with said mixture cooling, filter;
C, above-mentioned filtrate added to heat, on the tobacco surface of humidification, and careful the mixing.
14,, it is characterized in that apocynum extract wherein is 0.1% at least, in the weight of tobacco composition according to the claim 13 described methods that prepare tobacco composition.
15, according to the claim 13 described methods that prepare tobacco composition, it is characterized in that apocynum extract wherein is 0.1～10%, in the weight of tobacco composition.
16, according to the claim 13 described methods that prepare tobacco composition, it is characterized in that apocynum extract wherein is 0.5～4%, in the weight of tobacco composition.
17, according to the claim 13 described methods that prepare tobacco composition, it is characterized in that apocynum extract wherein extracts with polar solvent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 85101482 CN85101482A (en) | 1985-04-01 | 1985-04-01 | Tobacco composition and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 85101482 CN85101482A (en) | 1985-04-01 | 1985-04-01 | Tobacco composition and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN85101482A true CN85101482A (en) | 1986-08-20 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 85101482 Pending CN85101482A (en) | 1985-04-01 | 1985-04-01 | Tobacco composition and preparation method thereof |
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| CN (1) | CN85101482A (en) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102273731A (en) * | 2011-07-06 | 2011-12-14 | 南宁乙翔生物科技有限公司 | Method for degrading harm of tobacco toxin by utilizing bluish dogbane extract |
| CN102796204A (en) * | 2012-08-27 | 2012-11-28 | 福建中烟工业有限责任公司 | Extraction method of tremella polysaccharide and application of tremella polysaccharide in tobaccos |
| CN103315384A (en) * | 2007-02-23 | 2013-09-25 | 美国无烟烟草有限责任公司 | Novel tobacco compositions and methods of making |
| CN103813725A (en) * | 2011-10-12 | 2014-05-21 | 日本烟草产业株式会社 | Method for augmenting component providing smoking flavor for tobacco product, tobacco raw material, cigarette, and cigar |
| CN104738805A (en) * | 2015-01-30 | 2015-07-01 | 广东中烟工业有限责任公司 | Method for manufacturing reconstituted tobacco paper base with apocynum venetum and obtained reconstituted tobacco paper base |
| CN104738806A (en) * | 2015-01-30 | 2015-07-01 | 广东中烟工业有限责任公司 | Method for manufacturing reconstituted tobacco paper base with apocynum venetum and tobacco stems mixed and obtained reconstituted tobacco paper base |
| CN107467709A (en) * | 2017-08-25 | 2017-12-15 | 四川中烟工业有限责任公司 | Chinese style style pipe tobacco process for making |
| CN110250562A (en) * | 2019-06-19 | 2019-09-20 | 山西伟润诚戒烟品科技有限公司 | A kind of bluish dogbane health cigarette and preparation method thereof |
-
1985
- 1985-04-01 CN CN 85101482 patent/CN85101482A/en active Pending
Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9629334B2 (en) | 2007-02-23 | 2017-04-25 | U.S. Smokeless Tobacco Company Llc | Tobacco compositions and methods of making |
| CN103315384A (en) * | 2007-02-23 | 2013-09-25 | 美国无烟烟草有限责任公司 | Novel tobacco compositions and methods of making |
| US9173371B2 (en) | 2007-02-23 | 2015-11-03 | U.S. Smokeless Tobacco Company | Tobacco compositions and methods of making |
| CN103315384B (en) * | 2007-02-23 | 2016-04-06 | 美国无烟烟草有限责任公司 | Novel tobacco compositions and preparation method |
| CN102273731A (en) * | 2011-07-06 | 2011-12-14 | 南宁乙翔生物科技有限公司 | Method for degrading harm of tobacco toxin by utilizing bluish dogbane extract |
| CN103813725A (en) * | 2011-10-12 | 2014-05-21 | 日本烟草产业株式会社 | Method for augmenting component providing smoking flavor for tobacco product, tobacco raw material, cigarette, and cigar |
| CN103813725B (en) * | 2011-10-12 | 2016-08-17 | 日本烟草产业株式会社 | The method of taste useful component, tobacco material, medicated cigarette and cigar is inhaled for strengthening the fragrant of tobacco product |
| CN102796204A (en) * | 2012-08-27 | 2012-11-28 | 福建中烟工业有限责任公司 | Extraction method of tremella polysaccharide and application of tremella polysaccharide in tobaccos |
| CN104738805A (en) * | 2015-01-30 | 2015-07-01 | 广东中烟工业有限责任公司 | Method for manufacturing reconstituted tobacco paper base with apocynum venetum and obtained reconstituted tobacco paper base |
| CN104738806A (en) * | 2015-01-30 | 2015-07-01 | 广东中烟工业有限责任公司 | Method for manufacturing reconstituted tobacco paper base with apocynum venetum and tobacco stems mixed and obtained reconstituted tobacco paper base |
| CN107467709A (en) * | 2017-08-25 | 2017-12-15 | 四川中烟工业有限责任公司 | Chinese style style pipe tobacco process for making |
| CN107467709B (en) * | 2017-08-25 | 2019-03-22 | 四川中烟工业有限责任公司 | Chinese style style pipe tobacco process for making |
| CN110250562A (en) * | 2019-06-19 | 2019-09-20 | 山西伟润诚戒烟品科技有限公司 | A kind of bluish dogbane health cigarette and preparation method thereof |
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