CN2854595Y - Gas chromatograph for analysing tail gas of vehicle - Google Patents

Gas chromatograph for analysing tail gas of vehicle Download PDF

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Publication number
CN2854595Y
CN2854595Y CN 200520044945 CN200520044945U CN2854595Y CN 2854595 Y CN2854595 Y CN 2854595Y CN 200520044945 CN200520044945 CN 200520044945 CN 200520044945 U CN200520044945 U CN 200520044945U CN 2854595 Y CN2854595 Y CN 2854595Y
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CN
China
Prior art keywords
chromatographic column
sub
gas chromatograph
porapak
way valve
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN 200520044945
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Chinese (zh)
Inventor
方华
庄鸿涛
李建浩
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SHANGHAI HUAAI CHROMATOGRAPHIC ANALYSIS CO Ltd
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SHANGHAI HUAAI CHROMATOGRAPHIC ANALYSIS CO Ltd
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Priority to CN 200520044945 priority Critical patent/CN2854595Y/en
Application granted granted Critical
Publication of CN2854595Y publication Critical patent/CN2854595Y/en
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Expired - Fee Related legal-status Critical Current

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Abstract

A gas chromatograph in use for auto tail gas analysis comprises a sample introduction back flushing device and a column selection device. The back flushing device comprises one 10-port valve, one in use for pre-cutting back flushing 2m PORAPAK N chromatograph column; the column selection device comprises four-connection valve, one 2m 5A chromatograph column and one PORAPAK Q chromatograph column 2m in length. The utility model can be employed to measure gases comprising N<SUB>2</SUB>, NO, N<SUB>2</SUB>O, NO<SUB>2</SUB>, CO, CO<SUB>2</SUB>, etc., which is convenient in operation, cheap in price and effective to measure the auto tail gas content.

Description

Be used for the gas chromatograph that vehicle exhaust is analyzed
Technical field
The utility model belongs to a kind of gas chromatograph, is to analyze contained N in the vehicle exhaust 2, NO, NO 2, N 2O, CO, CO 2A kind of gas chromatograph Deng gas.
Technical background
Contain hydrocarbon, carbon monoxide, carbon dioxide, oxynitrides etc. in the vehicle exhaust, wherein oxynitrides is called for short NO x, the waste gas frowzy of a large amount of a kind of brown that produce when it is the big load operation of engine, the NO of 3.5ppm xEffect 1h can produce deleterious effect to the people, and the NO of 0.5ppm xEffect 1h can produce toxic action to the sensitive plant of occurring in nature.So produced some thereupon at NO x, hydrocarbon, carbon monoxide, carboloy dioxide analysis analytical instrument, measure NO xAnalytical instrument adopt chemiluminescence principle and make, the analytical instrument of measuring hydrocarbon, carbon monoxide, carbon dioxide is to adopt the nondixpersive infrared principle of absorption and make, and causes cost to increase like this, complex structure.
Summary of the invention
The utility model technical issues that need to address provide a kind of gas chromatograph that vehicle exhaust is analyzed that is used for, and this instrument cost is cheap, and is simple in structure, easy to operate.
For solving the problems of the technologies described above, the technical solution adopted in the utility model is: a kind of gas chromatograph that can be used for the vehicle exhaust analysis comprises sample introduction back-blowing device and post selecting arrangement, described sample introduction back-blowing device comprises a ten-way valve, a PORAPAK N chromatographic column that is used for cutting in advance the long 2m of blowback; Described post selecting arrangement comprises the 5A chromatographic column of a four-way valve, a long 2m and the PORAPAK Q chromatographic column of a long 2m.
Description of drawings
Fig. 1 is the working state figure that the utility model is used for the gas chromatograph of vehicle exhaust analysis;
Fig. 2 is the working state figure that the utility model is used for the gas chromatograph of vehicle exhaust analysis.
Embodiment
As shown in Figure 1, the utility model is used for the gas chromatograph that vehicle exhaust is analyzed, and mainly by sample introduction back-blowing device and post selecting arrangement, described sample introduction back-blowing device comprises a ten-way valve, a PORAPAK N chromatographic column that is used for cutting in advance the long 2m of blowback; Described post selecting arrangement comprises the 5A chromatographic column of a four-way valve, a long 2m and the PORAPAK Q chromatographic column of a long 2m.
Main flow process of gas chromatograph and operating process that the utility model is used for the vehicle exhaust analysis are:
As shown in Figure 1, systematic sampling, the sample flow process is 1-2-quantity tube-9-10, and rotation ten-way valve 60 is spent the position of accompanying drawing 2, and the flow process of carrier gas (He) 2 is 3-2-quantity tube-9-8-PORAPAKN chromatographic column-4-5-11-12-5A chromatographic column-detecting devices, N in this process 2With CO, NO and NO 2, N 2O, CO 2Separated by the PORAPAKN chromatographic column, treat NO and NO 2Do not flow out and CO flows out PORAPAK N chromatographic column also not enter the 5A chromatographic column be to switch the position of four-way to accompanying drawing 2, carrier gas 1 flow process is 14-12-5A chromatographic column-detecting device at this moment, N 2With advance detecting device one by one after CO separates again by the 5A chromatographic column, the flow process after carrier gas 2 this moment is come out from ten-way valve is a 4-5-PORAPAK Q-detecting device, NO and NO 2, N 2O, CO 2Be blown into PORAPAK Q, separate laggard detecting device again, treat CO 2Rotation ten-way valve 60 is spent the position of accompanying drawing 1 after flowing out ten-way valve PORAPAK N chromatographic column, and the flow process of carrier gas 2 is 3-4-PORAPAKN chromatographic column-8-7, and the heavy constituent blowback is gone out system.

Claims (4)

1, a kind of gas chromatograph that is used for the tails assay of automobile tail comprises sample introduction back-blowing device and post selecting arrangement, it is characterized in that: described sample introduction back-blowing device comprises a ten-way valve, a PORAPAK N chromatographic column that is used for cutting in advance the long 2m of blowback.
2, according to the described gas chromatograph that is used for the analysis of vehicle exhaust thing of claim 1, it is characterized in that: the two ends of described PORAPAKN chromatographic column link to each other with the 8th binding post with the 4th binding post of described ten-way valve respectively.
3, a kind of gas chromatograph that is used for the vehicle exhaust analysis comprises sample introduction back-blowing device and post selecting arrangement, and it is characterized in that: described post selecting arrangement comprises the PORAPAK Q chromatographic column of a four-way valve, a long 2m 5A chromatographic column and a long 2m.
4, be used for the gas chromatograph that the vehicle exhaust thing is analyzed according to claim 3 is described, it is characterized in that: the two ends after described 5A chromatographic column and the described PORAPAK Q chromatographic column serial connection link to each other with two diametrical connection terminals of described four-way valve respectively.
CN 200520044945 2005-09-12 2005-09-12 Gas chromatograph for analysing tail gas of vehicle Expired - Fee Related CN2854595Y (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 200520044945 CN2854595Y (en) 2005-09-12 2005-09-12 Gas chromatograph for analysing tail gas of vehicle

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 200520044945 CN2854595Y (en) 2005-09-12 2005-09-12 Gas chromatograph for analysing tail gas of vehicle

Publications (1)

Publication Number Publication Date
CN2854595Y true CN2854595Y (en) 2007-01-03

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Family Applications (1)

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CN 200520044945 Expired - Fee Related CN2854595Y (en) 2005-09-12 2005-09-12 Gas chromatograph for analysing tail gas of vehicle

Country Status (1)

Country Link
CN (1) CN2854595Y (en)

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101251517B (en) * 2008-04-01 2011-01-19 南京特种气体厂有限公司 Method and equipment for chromatographic analysis minim argon, nitrogen impurity in oxygen
CN102621251A (en) * 2011-01-31 2012-08-01 中国石油化工股份有限公司 Trace helium, neon and hydrogen gas analysis method and device
CN103776910A (en) * 2012-10-23 2014-05-07 中国石油化工股份有限公司 Analysis system for nitrogen oxides in exhaust gas
CN105181851A (en) * 2015-10-13 2015-12-23 神华集团有限责任公司 Method for testing oxynitride in environment
CN106124676A (en) * 2016-09-08 2016-11-16 国网上海市电力公司 A kind of for measuring the gas chromatograph of solution gas in transformer oil
CN107014940A (en) * 2017-05-09 2017-08-04 上海大学 Rapid analysis method when carbon monoxide, carbon dioxide and nitrous oxide coexist
CN107941930A (en) * 2017-11-03 2018-04-20 南京信息工程大学 A kind of quickly VOCs gas multicomponent chromatographic separation devices
CN109975449A (en) * 2017-12-28 2019-07-05 内蒙古伊泰煤基新材料研究院有限公司 The Gas Chromatographic Method of hydrogen sulfide and carbonyl sulfur in a kind of crude synthesis gas
CN111323525A (en) * 2020-04-10 2020-06-23 苏州天蓝分析仪器有限公司 Non-methane total hydrocarbon and benzene series concentration on-line analysis and detection device

Cited By (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101251517B (en) * 2008-04-01 2011-01-19 南京特种气体厂有限公司 Method and equipment for chromatographic analysis minim argon, nitrogen impurity in oxygen
CN102621251A (en) * 2011-01-31 2012-08-01 中国石油化工股份有限公司 Trace helium, neon and hydrogen gas analysis method and device
CN103776910A (en) * 2012-10-23 2014-05-07 中国石油化工股份有限公司 Analysis system for nitrogen oxides in exhaust gas
CN103776910B (en) * 2012-10-23 2015-06-17 中国石油化工股份有限公司 Analysis system for nitrogen oxides in exhaust gas
CN105181851A (en) * 2015-10-13 2015-12-23 神华集团有限责任公司 Method for testing oxynitride in environment
CN106124676B (en) * 2016-09-08 2017-08-29 国网上海市电力公司 A kind of gas chromatograph for being used to determine solution gas in transformer oil
CN106124676A (en) * 2016-09-08 2016-11-16 国网上海市电力公司 A kind of for measuring the gas chromatograph of solution gas in transformer oil
CN107014940A (en) * 2017-05-09 2017-08-04 上海大学 Rapid analysis method when carbon monoxide, carbon dioxide and nitrous oxide coexist
CN107941930A (en) * 2017-11-03 2018-04-20 南京信息工程大学 A kind of quickly VOCs gas multicomponent chromatographic separation devices
CN107941930B (en) * 2017-11-03 2020-11-27 南京信息工程大学 Quick gaseous multicomponent chromatographic fractionation device of VOCs
CN109975449A (en) * 2017-12-28 2019-07-05 内蒙古伊泰煤基新材料研究院有限公司 The Gas Chromatographic Method of hydrogen sulfide and carbonyl sulfur in a kind of crude synthesis gas
CN111323525A (en) * 2020-04-10 2020-06-23 苏州天蓝分析仪器有限公司 Non-methane total hydrocarbon and benzene series concentration on-line analysis and detection device
CN111323525B (en) * 2020-04-10 2022-06-14 苏州天蓝分析仪器有限公司 Non-methane total hydrocarbon and benzene series concentration on-line analysis and detection device

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20070103

Termination date: 20140912

EXPY Termination of patent right or utility model