CN2748444Y - Water distilling tower for injection - Google Patents

Water distilling tower for injection Download PDF

Info

Publication number
CN2748444Y
CN2748444Y CN 200420114085 CN200420114085U CN2748444Y CN 2748444 Y CN2748444 Y CN 2748444Y CN 200420114085 CN200420114085 CN 200420114085 CN 200420114085 U CN200420114085 U CN 200420114085U CN 2748444 Y CN2748444 Y CN 2748444Y
Authority
CN
China
Prior art keywords
heat exchanger
water
shell
tube
injection
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN 200420114085
Other languages
Chinese (zh)
Inventor
邵春林
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SHANGHAI JIUZHOU MEDICINE EQUIPMENT FACTORY
Original Assignee
SHANGHAI JIUZHOU MEDICINE EQUIPMENT FACTORY
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by SHANGHAI JIUZHOU MEDICINE EQUIPMENT FACTORY filed Critical SHANGHAI JIUZHOU MEDICINE EQUIPMENT FACTORY
Priority to CN 200420114085 priority Critical patent/CN2748444Y/en
Application granted granted Critical
Publication of CN2748444Y publication Critical patent/CN2748444Y/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Images

Landscapes

  • Heat Treatment Of Water, Waste Water Or Sewage (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

The utility model relates to a distilling tower, and the pure steam produced by the distillation tower can be used as medical water for injection. The aim of the utility model is to provide a distilling tower, and the products produced by the distilling tower can be directly used as medical water for injection. The water distilling tower for injection of the utility model comprises a tubular heat exchanger whose casing is a cylindrical structure and upper part is provided with a feeding raw material water inlet. The outside of the tubular heat exchanger is provided with an evaporator which is a hollow cylinder with a closed lower end and an opening upper end, and the upper end of the evaporator is connected with the casing of the heat exchanger. The upper part of the evaporator is provided with a pure steam outlet, and the lower part of the evaporator is provided with a concentrated water outlet. The outer surface of the casing of the heat exchanger is provided with a gas and liquid separator. The beneficial effect of the utility model is that the water for injection produced by the method has stable water quality and high purity, and the water quality of the bacterial endotoxin conforms to every quality index regulation of the water for injection of pharmacopoeia of the people's republic of china.

Description

The water for injection distillation tower
Technical field
Utility model relates to a kind of distillation tower, and the pure steam that this distillation tower produces can be used for water for injection medically.
Background technology
Common distillation tower is traditional shell and tube heat exchanger, and as shown in Figure 1, this shell and tube heat exchanger 1 comprises heat transfer tube 11, upper tubesheet 12, lower tubesheet 13, heat exchanger shell 14 and upper cover 15.Described heat exchanger shell 14 is a cylinder-like structure, and its underpart is provided with vapour outlet 142, and the top of housing 14 is provided with the bobbin carriage of protrusion, and a side of bobbin carriage is provided with heating steam import 141; Upper cover 15 is a spill lid, be connected by the upper tubesheet 12 of screw with heat exchanger shell 14 upper ends, lower tubesheet 13 is fixed on the bottom of shell and tube heat exchanger 14, be provided with tens of or up to a hundred heat transfer tube 11 between upper tubesheet 12 and the lower tubesheet 13, the upper end of upper cover 15 is provided with for raw water import 151; Steam through this kind structure is produced is gas-liquid mixture, can not directly use, and needs to carry out separating treatment through other equipment and just can be used as medically water for injection.
Summary of the invention
The purpose of this utility model provides a kind of distillation tower, and its product of producing can directly be used as water for injection medically.
The utility model is to be achieved by following technical scheme, and the water for injection distillation tower comprises shell and tube heat exchanger 1, and described shell and tube heat exchanger 1 comprises heat transfer tube 11, upper tubesheet 12, lower tubesheet 13, heat exchanger shell 14 and upper cover 15; Heat exchanger shell 14 is a cylinder-like structure, and its upper/lower terminal is provided with heat transfer tube 11 by upper tubesheet 12 and lower tubesheet 13 sealings between described upper tubesheet 12 and the lower tubesheet 13, and top is provided with the bobbin carriage of protrusion, and a side of bobbin carriage is provided with heating steam import 141; Upper cover 15 is the spill lid, and both sides are connected by the upper tubesheet 12 of web member with heat exchanger shell 14 upper ends, and its upper end is provided with for raw water import 151; It is characterized in that: the outside of described shell and tube heat exchanger 1 is provided with vaporizer 3, this vaporizer 3 is the hollow cylinder of bottom sealing, upper end open, and its upper end is connected with the bobbin carriage part lower end that heat exchanger shell 14 protrudes, the top of vaporizer 3 is provided with pure vapour outlet 31, and the bottom is provided with condensed water outlet 32; Outside surface at heat exchanger shell 14 is equipped with gas-liquid separator 2.
Described gas-liquid separator 2 is made up of four groups of spiral plates, every group of circumferential direction interval 90 degree, and rotation is installed on the heat exchanger shell 14.
In heat transfer tube 11 gaps of described shell and tube heat exchanger 1 preheating tube 4 is installed, this preheating tube 4 is the tubular structure of U type, its import 41 and export 42 and be installed on the heat exchanger shell 14 respectively.
The utility model is that raw water, heating steam are heating source with the purified water, adopt the principle of falling film evaporation, the water for injection that this kind method produces, water conditioning, purity height, bacterial endotoxin water quality meet that " every quality of water for injection refers to regulation in the Pharmacopoeia of the People's Republic of China.
Description of drawings
Fig. 1 is the prior art constructions synoptic diagram;
Fig. 2 is a structural representation of the present utility model.
Embodiment
Below in conjunction with accompanying drawing the utility model is carried out concrete description, as shown in Figure 2, the utility model comprises shell and tube heat exchanger 1, gas-liquid separator 2, vaporizer 3 and preheating tube 4.Described shell and tube heat exchanger 1 comprises heat transfer tube 11, upper tubesheet 12, lower tubesheet 13, heat exchanger shell 14 and upper cover 15, heat exchanger shell 14 is a cylinder-like structure, its upper/lower terminal is by upper tubesheet 12 and lower tubesheet 13 sealings, be provided with tens of or up to a hundred heat transfer tube 11 between described upper tubesheet 12 and the lower tubesheet 13, top is provided with the bobbin carriage of protrusion, and a side of bobbin carriage is provided with heating steam import 141; Upper cover 15 is the spill lid, and both sides are connected by the upper tubesheet 12 of web member with heat exchanger shell 14 upper ends, and this web member can be flange, also can be bolt or nut, and its upper end is provided with for raw water import 151.The outside of described shell and tube heat exchanger 1 is provided with vaporizer 3, and this vaporizer 3 is the hollow cylinder of bottom sealing, upper end open, and its upper end is connected with the bobbin carriage part lower end that heat exchanger shell 14 protrudes; Because the shell of vaporizer 3 places the outside of heat exchanger shell 14, after raw water heats through tubular heat exchange 1 like this, carry out flash distillation and have the space with separating.
Outside surface at heat exchanger shell 14 is equipped with gas-liquid separator 2.Gas-liquid separator 2 is made up of four groups of spiral plates, every group of circumferential direction interval 90 degree, rotation is installed on the shell 14 of interchanger 1, its effect is to make the secondary steam of evaporation generation after the gravity settling separation of process one-level, import spiral plate in the uphill process and force rotation, make secondary steam produce high speed centrifugation power, on the shell wall that the water droplet carried secretly in the secondary steam and mist are thrown to vaporizer, automatically flow into the lower liquid chamber, reach the effect of vapor-liquid separation.
In heat transfer tube 11 gaps of shell and tube heat exchanger 1 preheating tube 4 is installed, this preheating tube 4 is the tubular structure of U type, middle no splicing welding joint, its import 41 and export 42 and be installed on the heat exchanger shell 14 respectively.Play the effect of preheating material water; Because this preheating tube 4 is installed in the distillation tower, can reduce calorific loss.
Lower tubesheet 13 is provided with condensate outlet pipe 5, and passes the lower end of the housing of vaporizer 3.The upper side of vaporizer 3 is provided with pure vapour outlet 31, and the bottom is provided with condensed water outlet 32, and lower side is provided with visor 6, can observe the liquid-vapor mixture situation in the vaporizer.
During use, the raw water of this distillation tower is a purified water, and raw water flows out from preheating tube outlet 42 after being heated steam preheating in preheating tube import 41 flows into built-in U type preheating tube 4.
From the distillation tower top, the raw water import 151 of the upper cover 15 of interchanger 1 enters the tube side of tubular heat exchange 1 the raw water of process preheating.Enter then in the every heat transfer tube 11, become film like to flow downward along its tube wall.Heating steam this moment enters the shell side of shell and tube heat exchanger 1 from steam inlet 141, raw water in every heat transfer tube 11 is under the heat effect of heating steam, the rapid falling film evaporation of inwall along heat transfer tube 11, the secondary steam that evaporation produces and the mixture of water, enter the bottom evaporator room of vaporizer 3 downwards after, since the spatial sudden enlargement and sharply flash distillation be a large amount of secondary steams, after this secondary steam process one-level gravity settling separation, naturally rise with fast speeds, after running into the centrifugal gas-liquid separator 2 of spiral plate, be imported into the rotation of spiral plate generation of forced, because gas velocity is higher, high speed centrifugal force is thrown on the outer casing inner wall of vaporizer 3 the water droplet mist of carrying secretly in the secondary steam, relies on deadweight to flow to the bottom of vaporizer 3.Flow out through the pure vapour outlet 31 of the pure steam of secondary after the vapor-liquid separation,, be product-water for injection that we need through after the other condenser condenses aftertreatment from distillation tower.The spiral fluid removing system of this distillation tower can reliably be removed the bacterial endotoxin in the raw water, reaches " the requirement of " water for injection " in the Chinese pharmacopoeia 2000 editions fully.The last feed water that is not evaporated of coming out from the distillation tower tube side is because contain accumulative impurity in the still-process, so discharge from the condensed water outlet 32 of distillation tower.From the heating steam water of condensation that the distillation shell side comes out, discharge from the condensating water outlet tube 5 of vaporizer 3 bottoms.

Claims (3)

1. the water for injection distillation tower comprises shell and tube heat exchanger (1), and described shell and tube heat exchanger (1) comprises heat transfer tube (11), upper tubesheet (12), lower tubesheet (13), heat exchanger shell (14) and upper cover (15); Heat exchanger shell (14) is a cylinder-like structure, its upper/lower terminal is by upper tubesheet (12) and lower tubesheet (13) sealing, be provided with heat transfer tube (11) between described upper tubesheet (12) and the lower tubesheet (13), top is provided with the bobbin carriage of protrusion, and a side of bobbin carriage is provided with heating steam import (141); Upper cover (15) is the spill lid, and both sides are connected by the upper tubesheet (12) of web member with heat exchanger shell (14) upper end, and its upper end is provided with for raw water import (151); It is characterized in that: the outside of described shell and tube heat exchanger (1) is provided with vaporizer (3), this vaporizer (3) is the hollow cylinder of bottom sealing, upper end open, and its upper end is connected with the bobbin carriage part lower end that heat exchanger shell (14) protrudes, the top of vaporizer (3) is provided with pure vapour outlet (31), and the bottom is provided with condensed water outlet (32); At heat exchanger shell (14) outside surface gas-liquid separator (2) is installed.
2. according to the described water for injection distillation tower of claim 1, it is characterized in that: described gas-liquid separator (2) is made up of four groups of spiral plates, every group of circumferential direction interval 90 degree, and rotation is installed on the heat exchanger shell (14).
3. according to claim 1 or 2 described water for injection distillation towers, it is characterized in that: preheating tube (4) is installed in the heat transfer tube gap of described shell and tube heat exchanger (1), this preheating tube (4) is the tubular structure of U type, and its import (41) and outlet (42) are being installed on the heat exchanger shell (14) respectively.
CN 200420114085 2004-12-13 2004-12-13 Water distilling tower for injection Expired - Fee Related CN2748444Y (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 200420114085 CN2748444Y (en) 2004-12-13 2004-12-13 Water distilling tower for injection

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 200420114085 CN2748444Y (en) 2004-12-13 2004-12-13 Water distilling tower for injection

Publications (1)

Publication Number Publication Date
CN2748444Y true CN2748444Y (en) 2005-12-28

Family

ID=35719936

Family Applications (1)

Application Number Title Priority Date Filing Date
CN 200420114085 Expired - Fee Related CN2748444Y (en) 2004-12-13 2004-12-13 Water distilling tower for injection

Country Status (1)

Country Link
CN (1) CN2748444Y (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102491572A (en) * 2011-12-20 2012-06-13 浙江晶泉水处理设备有限公司 Device for preparing injection water by using reverse osmosis ultrafiltration combined membrane method
CN107008024A (en) * 2017-05-02 2017-08-04 上海济俭工业设备有限公司 A kind of process structure for the integrated evaporating column that can save energy effective acquisition clean steam
CN107670316A (en) * 2017-10-31 2018-02-09 江阴市九鑫节能设备科技有限公司 MVR evaporation structures with integral type vapor-liquid separating structure

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102491572A (en) * 2011-12-20 2012-06-13 浙江晶泉水处理设备有限公司 Device for preparing injection water by using reverse osmosis ultrafiltration combined membrane method
CN107008024A (en) * 2017-05-02 2017-08-04 上海济俭工业设备有限公司 A kind of process structure for the integrated evaporating column that can save energy effective acquisition clean steam
CN107670316A (en) * 2017-10-31 2018-02-09 江阴市九鑫节能设备科技有限公司 MVR evaporation structures with integral type vapor-liquid separating structure
CN107670316B (en) * 2017-10-31 2023-09-15 江阴市吉瑞机械制造有限公司 MVR evaporator structure with integrated gas-liquid separation structure

Similar Documents

Publication Publication Date Title
JP5483226B2 (en) Method and apparatus for producing pure water vapor
CA2494564C (en) Method and device for the production of purified steam
CN205730426U (en) A kind of rectifying column
CN109096140A (en) Energy-saving dimethyl acetamide rectification and purification Processes and apparatus
CN101213004B (en) A rectification apparatus using a heat pump
CN2748444Y (en) Water distilling tower for injection
CN102266677B (en) High vacuum distillation purification device
CN106582054A (en) Condensed steam source heat pump driven multi-effect horizontal pipe falling film distillation column
CN202155061U (en) High vacuum distillation purification device
CN101780343A (en) Dynamic purification regenerator of harmful solvent and application thereof
CN216890737U (en) Caprolactam high-efficient gasification piece-rate system
CN102512833A (en) Horizontal-pipe falling-film evaporation method coupling distillation and device thereof
CN200948243Y (en) Device for concentrating Chinese traditional medicine
CN206995904U (en) Condensing source heat pump driving multiple-effect horizontal tube falling film destilling tower
CN214809891U (en) Pervaporation membrane device for isopropanol concentration
CN100395190C (en) Method and device for treating water
KR100243518B1 (en) A distillation apparatus for high purity distilled water manufacture
JPS63252501A (en) Distillation column for distilling plant
CN106730960A (en) A kind of high-efficiency steam recycling type triple effect falling film evaporator
CN205516593U (en) Evaporate and separate formula condensing equipment
CN220412940U (en) Multi-effect evaporation device for medical intermediate wastewater
CN213347825U (en) Supergravity solvent purification recovery system
CN220724071U (en) Cosmetic vegetable oil purification and precipitation device
CN221206833U (en) Rectifying and separating device for chloroethane
CN105521617A (en) Evaporative separation type condensing unit

Legal Events

Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
C17 Cessation of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20051228

Termination date: 20100113