CN2697459Y - Multi-atmosphere inclinable rotary furnace - Google Patents
Multi-atmosphere inclinable rotary furnace Download PDFInfo
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- CN2697459Y CN2697459Y CN 200420017540 CN200420017540U CN2697459Y CN 2697459 Y CN2697459 Y CN 2697459Y CN 200420017540 CN200420017540 CN 200420017540 CN 200420017540 U CN200420017540 U CN 200420017540U CN 2697459 Y CN2697459 Y CN 2697459Y
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- burner hearth
- turntable
- rotary furnace
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Abstract
The utility model relates to a multi-atmosphere inclinable rotary furnace which can introduce various atmosphere including hazardous gas. The rotary furnace is composed of an axial direction positioning device 1, a furnace floor end face detachable part 2, a fixed heating furnace body 3, a revolving hearth 4, an air inlet pipe 5, an electric thermocouple 6, a bearing support unit 7, a machine revolving device 8, a hearth top end face detachable part 9, an air outlet 10, a sliding sealer 11, a manometer 12, a universal stage 13, a slewing mechanism 14, a lifting appliance 15 and a base 16. The rotary furnace can introduce, protect and react to various gas. The utility model can conveniently adjust the slope angle. The utility model has the advantages of continuous revolving, homogeneous heating for materials, convenient charging and discharging, compact structure and easy maintenance. The utility model can be widely applied to the process of drying, heat decomposition, calcination, oxidation, deoxidization, carbonization and nitridation of powder stock, such as, hard alloy, structural ceramic, functional ceramic, ceramet, etc.
Description
Technical field
The utility model relates to a kind of tilting rotary furnace that can introduce the multiple atmosphere that comprises hazardous gas.
Background technology
The preparation equipment of the drying of powder stocks such as carbide alloy, structural ceramics, function ceramics, cermet, thermal decomposition, calcining, oxidation, reduction, carbonization, nitridation process is normally:
(1) fixed bed: prepare in the powder process with this equipment, because raw material does not fully contact with reaction atmosphere, cause reacting inhomogeneous, remain static owing to powder simultaneously, powder is assembled easily in course of reaction and is grown up, and the product particle that obtains is thick, composition and size distribution are all even inadequately.
(2) fluid bed: this equipment has overcome the shortcoming of fixed bed, purposes is widely arranged in powder preparation, but owing to need a large amount of use reacting gas and carrier gas, cause the powder preparation cost to increase, the powder of flow regime is taken out of by gas easily simultaneously, and it is complicated to make the preparation productive rate reduce, control.
(3) rotary furnace: this equipment is widely used in a plurality of fields such as chemical industry, metallurgy, building materials, garbage disposal, as: scrap lead melting rotary furnace (Mei Jialin, Chinese utility model patent ZL 95 2 26707.1, November 27 nineteen ninety-five); The rotary furnace grate furnace of burning away the refuse (Li Xin, Chinese utility model patent ZL on December 19th, 00253487.8,2000); Electric heating rotary furnace for ferromagnetic materials (summer gravity, Chinese invention patent ZL 97 1 01681.X, on March 17th, 1997); Wet method aluminum fluoride external-heat dehydrates rotary furnace (Li Yingwei etc., Chinese utility model patent ZL on April 19th, 992 09446.1,1999); Magnetic material sintering external-heating rotary kiln (Chen Ruisheng, Chinese utility model patent ZL on August 1st, 89205257.9,1989); Rotary kiln with resistor furnace for heating and calcining kaolin (Feng Jianming etc., Chinese invention patent ZL 01128612.1, September 19 calendar year 2001); Multi-functional rotary kiln (in Xiang, Chinese utility model patent ZL on March 26th, 96231504.4,1996); Wind and water cooling rotary kiln (Han Shiguo, Chinese utility model patent ZL on August 24th, 91223886.0,1991); Efficient rotary kiln (Chen Gengyun, Chinese utility model patent ZL on November 18th, 98242686.0,1998); Outer heating rotary kiln (Yuan Yiming etc., Chinese utility model patent ZL on May 5th, 97232399.6,1999); Automatic control compartment rotary kiln (Shen Guoxiang, China utility model patent ZL 01237607.8, on April 3rd, 2002), direct-reduction process and rotary hearth furnace (Kobe Steel Ltd, Chinese invention patent ZL on November 15th, 00105893.2,2000) or the like.
Through anatomizing the topology discovery of above-mentioned rotary furnace (kiln), above-mentioned rotary furnace (kiln) has all adopted " straight-through structure ", promptly from an endfeed, air inlet, from other end discharging, give vent to anger, the rotary furnace of this structure (kiln) is fit to serialization production, and is easy to operate, but they have the following disadvantages: (a) because raw material is an end advances one and bring out, to react completely in order making, certainly will will to increase the length of rotary furnace, this just causes, and the rotary furnace manufacturing cost strengthens, energy consumption increases, utilization rate is not high; SUMITOMO CHEMICAL and Tokyo tungsten company have just adopted the multi-stage rotary stove to prepare tungsten-cobalt carbide powder (AsadaNobuaki, Rotary furnace, JP on April 24th, 3099192,1991); (b) reaction time of raw material is that raw material is turned back to the required time of the other end from an end, and in fact different raw material reaction asynchronism(-nization)s causes the difficulty of technology controlling and process to strengthen; (c) for batch raw material, its composition can not be fully evenly, and in most cases always have intermediate product to produce, initial feed, intermediate product and end product mix, and cause the purity of made powder not high, uneven components; (d) if make rotary furnace (kiln) keep horizontal rotation, the back discharging that reacts completely can make above-mentioned situation improve, but because powder is substantially mobile in body of heater major diameter direction, so the body of heater temperature difference still can cause the inhomogeneous of material.
Other have the researcher designed the air-flow rotary furnace (Alan W, et al., Apparatus for producing uniform, fine ceramic powder, US Pat.5110565, May 5,1992; Zhang Liying etc., a kind of Processes and apparatus for preparing tungsten carbide-nickel-iron series nanometer grade composit powder, Chinese invention patent ZL 97 1 22085.9, on June 30th, 1999), the body of heater of this air-flow rotary furnace does not rotate, but the effect that utilizes interior vane type centrifugal pump of stove and air-flow drives powder revolution in the stove, and this furnace structure is complicated, and cost is higher.
For simplifying the material powder of technological process, prepared composition and even particle size distribution, be necessary to design a kind of novel device, it can make, and raw material fully contacts with reaction atmosphere, reaction speed is accelerated, reaction temperature reduces, flouring technology parameter (input and output material, atmosphere, temperature) control is easy.A kind of many atmosphere tilting rotary furnace of the special proposition of the utility model.
Summary of the invention
In order to design a kind of carbide alloy that can be applicable to, structural ceramics, function ceramics, the drying of powder stocks such as cermet, thermal decomposition, calcining, oxidation, reduction, carbonization, the novel device of nitridation process, a kind of many atmosphere tilting rotary furnace of the special proposition of the utility model, it is by axial direction positioning device 1, burner hearth bottom end face detachable block 2, fixedly heating furnace body 3, revolution burner hearth 4, air inlet pipe 5, thermocouple 6, bearing support 7, machinery rotation device 8, roof of the furnace end face detachable block 9, gas outlet 10, dynamic sealing device 11, Pressure gauge 12, turntable 13, rotating mechanism 14, lowering or hoisting gear 15 and base 16 constitute.Wherein:
Revolution burner hearth 4 is positioned at fixedly among the heating furnace body 3, fixedly heating furnace body 3 is fixed on the turntable 13 by welding or rivet, and the rotary furnace fixedly mode of heating of heating furnace body can adopt a kind of in following: resistance wire, Elema, corundum-mullite resistance tube, fuel oil, combustion gas;
The detachable block 2 of burner hearth bottom end face is by screw thread and rotary furnace burner hearth 4 sealed attachment, there is an axial direction positioning device 1 detachable block 2 outsides of bottom end face, the tip of axial direction positioning device 1 contacts with the center of the detachable block of bottom end face 2, axial direction positioning device 1 is welded on the turntable 13, rotary furnace burner hearth 4 tops connect with support unit 7 by bearing, and machinery rotation device 8 connects with rotary furnace burner hearth 4 by gear or belt pulley; Bottom end face detachable block 2 by the revolution burner hearth can charging and discharging, and with axial direction positioning device 1 contacted place a groove is being arranged, and is convenient to support and the location; Roof of the furnace end face detachable block 9 connects by thread seal with revolution burner hearth 4, top end face detachable block 9 by the revolution burner hearth can charging and discharging, and gas outlet 10 is welded on the roof of the furnace end face detachable block 9, bearing support 7 is welded on the turntable 13, and machinery rotation device 8 is fixed on the turntable 13 by rivet;
Air inlet pipe 5 and thermocouple 6 stretch into revolution burner hearth 4 centres together, link to each other with a dynamic sealing device 11 by welding in revolution burner hearth 4 outsides; Dynamic sealing device 11 can adopt a kind of in the following movable sealing form: felt sealing, soft packing seal, float ring seal, labyrinth seal, crush seal, centrifugal seal, lip-type seal, helixseal, liquid sealing, pneumostop, piston ring sealing, mechanical seal, magnet fluid sealing;
By dynamic sealing device 11, air inlet pipe 5 links to each other with source of the gas through the air inlet of band Pressure gauge 12, and thermocouple 6 links to each other with heating control system;
Revolution burner hearth 4 inside can be introduced by air inlet pipe 5 and be comprised the following reaction of hazardous gas and protect in the required gas one or more: H
2, O
2, N
2, Ar, He, CO, CO
2, NH
3, CH
4, C
2H
2
Effect and the advantage that the utlity model has are:
1, revolution burner hearth 4 is under the effect of bearing support 7 and machinery rotation device 8, the central axis of wraparound converter thorax 4 rotation continuously, on the inwall of revolution burner hearth 4 baffle plate or well-regulated fluctuating ripple or well-regulated projection many-sided ball can also be set, be convenient to abundant, the even contact of material and gas;
2, multiple reaction and the protective gas that comprises hazardous gas can be introduced by air inlet pipe 5 in revolution burner hearth 4 inside, and tail gas is by having gas outlet 10 emptyings or the burning of ceramic porous plate or heating resisting metal porous plate or blow-back device;
3, turntable 13 is regulated the angle of inclination by rotating mechanism 14, and adjustable range is-90 °~90 °;
4, revolution burner hearth 4 internal temperatures can detect automatically and regulate by the heating control system that links to each other with thermocouple 6;
5, input and output material convenience, compact conformation, maintenance are easy;
Drying, thermal decomposition, calcining, oxidation, reduction, carbonization, the nitridation process that 6, can be widely used in powder stocks such as carbide alloy, structural ceramics, function ceramics, cermet.
Description of drawings
Fig. 1: many atmosphere tilting rotary furnace structure chart.
In Fig. 1, many atmosphere tilting rotary furnace is by axial direction positioning device 1, burner hearth bottom end face detachable block 2, fixedly heating furnace body 3, revolution burner hearth 4, air inlet pipe 5, thermocouple 6, bearing support 7, machinery rotation device 8, roof of the furnace end face detachable block 9, gas outlet 10, dynamic sealing device 11, Pressure gauge 12, turntable 13, rotating mechanism 14, lowering or hoisting gear 15 and base 16 constitute.
Wherein turning round burner hearth 4 is positioned at fixedly among the heating furnace body 3, fixedly heating furnace body 3 is fixed on the turntable 13 by rivet, the detachable block 2 of bottom end face connects by thread seal with revolution burner hearth 4, axial direction positioning device 1 tip contacts with detachable block 2 centers of bottom end face, axial direction positioning device 1 is welded on the turntable 13, roof of the furnace end face detachable block 9 passes through screw thread or rivet sealed attachment with revolution burner hearth 4, revolution burner hearth 4 connects with bearing support 7 by bearing, machinery rotation device 8 connects with revolution burner hearth 4 by gear or belt pulley, bearing support 7 is welded on the turntable 13, machinery rotation device 8 is fixed on the turntable 13 by rivet, air inlet pipe 5 and thermocouple 6 stretch into revolution burner hearth centre together, outside the revolution burner hearth, link to each other with a dynamic sealing device 11 by welding, by dynamic sealing device 11, air inlet pipe 5 links to each other with source of the gas through the air inlet of band Pressure gauge 12, and thermocouple 6 links to each other with heating control system; Turntable 13 passes through hinge-coupled with rotating mechanism 14, turntable 13 is regulated the angle of inclination by rotating mechanism 14, adjustable range is-90 °~90 °, it is fixing after adjusting finishes with lowering or hoisting gear 15, lowering or hoisting gear 15 can move at base 16, and rotating mechanism 14 is fixed on the base 16 by welding or rivet.
The specific embodiment
Embodiment 1:
Many atmosphere of the utility model tilting rotary furnace is by axial direction positioning device 1 (diameter 60mm, long 300mm, 60 ° of drift angles), burner hearth bottom end face detachable block 2 (diameter 180mm, thick 15mm), fixing heating furnace body 3 (internal diameter 220mm, external diameter 370mm, long 1000mm, the resistance wire heating), revolution burner hearth 4 (external diameter 200mm, wall thickness 10mm, long 1500mm, material is a 1Cr25Ni20Si2 heat resisting steel), air inlet pipe 5 (external diameter 12mm, wall thickness 2mm, long 1500mm), thermocouple 6 (platinum rhodium-platinum thermocouples, long 1500mm), bearing support 7,8 (the gear drives of machinery rotation device, power 3kW), roof of the furnace end face detachable block 9 (diameter 180mm, thick 10mm), gas outlet 10 (external diameter 10mm, wall thickness 2mm), dynamic sealing device 11 (employing mechanical dynamic seal), Pressure gauge 12, turntable 13, rotating mechanism 14, lowering or hoisting gear 15 and base 16 constitute.Wherein turning round burner hearth 4 is positioned at fixedly among the heating furnace body 3, fixedly heating furnace body 3 is fixed on the turntable 13 by rivet, the detachable block 2 of bottom end face connects by thread seal with revolution burner hearth 4, axial direction positioning device 1 tip contacts with detachable block 2 centers of bottom end face, axial direction positioning device 1 is welded on the turntable 13, roof of the furnace end face detachable block 9 passes through the rivet sealed attachment with revolution burner hearth 4, revolution burner hearth 4 connects with bearing support 7 by bearing, machinery rotation device 8 connects with revolution burner hearth 4 by gear, bearing support 7 is welded on the turntable 13, machinery rotation device 8 is fixed on the turntable 13 by rivet, air inlet pipe 5 and thermocouple 6 stretch into revolution burner hearth centre together, outside the revolution burner hearth, link to each other with a dynamic sealing device 11 by welding, by dynamic sealing device 11, air inlet pipe 5 links to each other with source of the gas through the air inlet of band Pressure gauge 12, and thermocouple 6 links to each other with heating control system; Turntable 13 passes through hinge-coupled with rotating mechanism 14, turntable 13 is regulated the angle of inclination by rotating mechanism 14, and adjustable range is-90 °~90 °, and it is fixing with lowering or hoisting gear 15 to regulate the back that finishes, lowering or hoisting gear 15 can move at base 16, and rotating mechanism 14 is fixed on the base 16 by rivet.
Before the rotary furnace operation, the detachable block 9 with the roof of the furnace end face unloads earlier, adds the CoWO of 2000g
4/ WO
3Refill behind the material (press the WC-10wt%Co proportioning, make with spray pyrolysis), the angle of inclination of regulating turntable 13 is 30 °, and the back that finishes is fixing with lowering or hoisting gear 15, feeds N
2(flow is 6000ml/min) connects the fixedly power supply of heating furnace body 3 and the electrical source of power of machinery rotation device 8, begins to heat and make to turn round burner hearth 4 with 10 rev/mins rotating speed uniform rotation, and heating rate is 10 ℃/min, feeds H after being warming up to 550 ℃
2(flow is 6000ml/min) lights tail gas, and heating rate is 10 ℃/min, feeds CH after being warming up to 950 ℃
4(flow is 600ml/min) begins insulation, is incubated and closes CH after 4 hours
4, beginning cooling, rate of temperature fall is 10 ℃/min, feeds CO after being cooled to 750 ℃
2(flow is 500ml/min), insulation is closed the fixedly power supply of heating furnace body 3 after half an hour, cool off with stove, temperature is closed hydrogen after reducing to 200 ℃, closes the electrical source of power of mechanical slewing equipment 8 simultaneously, cool to room temperature with the furnace after, cut off all sources of the gas, the angle of inclination of regulating turntable 13 be-60 °, unloads the detachable block 9 of roof of the furnace end face, can be with the WC-10Co composite powder taking-up of the 1500g that makes.
Claims (5)
1, a kind of many atmosphere tilting rotary furnace, it is characterized in that rotary furnace is by axial direction positioning device 1, burner hearth bottom end face detachable block 2, fixedly heating furnace body 3, revolution burner hearth 4, air inlet pipe 5, thermocouple 6, bearing support 7, machinery rotation device 8, roof of the furnace end face detachable block 9, gas outlet 10, dynamic sealing device 11, Pressure gauge 12, turntable 13, rotating mechanism 14, lowering or hoisting gear 15 and base 16 constitute, wherein turning round burner hearth 4 is positioned at fixedly among the heating furnace body 3, fixedly heating furnace body 3 is fixed on the turntable 13 by welding or rivet, the detachable block 2 of bottom end face connects by thread seal with revolution burner hearth 4, axial direction positioning device 1 tip contacts with detachable block 2 centers of bottom end face, axial direction positioning device 1 is welded on the turntable 13, roof of the furnace end face detachable block 9 passes through screw thread or rivet sealed attachment with revolution burner hearth 4, revolution burner hearth 4 connects with bearing support 7 by bearing, machinery rotation device 8 connects with revolution burner hearth 4 by gear or belt pulley, bearing support 7 is welded on the turntable 13, machinery rotation device 8 is fixed on the turntable 13 by rivet, air inlet pipe 5 and thermocouple 6 stretch into revolution burner hearth centre together, outside the revolution burner hearth, link to each other with a dynamic sealing device 11 by welding, by dynamic sealing device 11, air inlet pipe 5 links to each other with source of the gas through the air inlet of band Pressure gauge 12, thermocouple 6 links to each other with heating control system, turntable 13 passes through hinge-coupled with rotating mechanism 14, turntable 13 is regulated the angle of inclination by rotating mechanism 14, adjustable range is-90 °~90 °, it is fixing after adjusting finishes with lowering or hoisting gear 15, lowering or hoisting gear 15 can move at base 16, and rotating mechanism 14 is fixed on the base 16 by welding or rivet.
2, require described many atmosphere tilting rotary furnace according to right 1, it is characterized in that can charging and discharging by the bottom end face detachable block 2 of revolution burner hearth, and with axial direction positioning device 1 contacted place a groove is being arranged, and is convenient to support and the location.
3, require described many atmosphere tilting rotary furnace according to right 1, it is characterized in that can charging and discharging by the top end face detachable block 9 of revolution burner hearth, and gas outlet 10 is positioned on the roof of the furnace end face detachable block 9.
4, require described many atmosphere tilting rotary furnace according to right 1, it is characterized in that gas outlet 10 can have ceramic porous plate or heating resisting metal porous plate or blow-back device;
5, require described many atmosphere tilting rotary furnace according to right 1, it is characterized in that turning round on the inwall of burner hearth 4 baffle plate or well-regulated fluctuating ripple or well-regulated projection many-sided ball can be set, be convenient to material and gas fully, even contact.
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