CN2457118Y - Plasma preparing nanometer carbon tube device - Google Patents
Plasma preparing nanometer carbon tube device Download PDFInfo
- Publication number
- CN2457118Y CN2457118Y CN 00263593 CN00263593U CN2457118Y CN 2457118 Y CN2457118 Y CN 2457118Y CN 00263593 CN00263593 CN 00263593 CN 00263593 U CN00263593 U CN 00263593U CN 2457118 Y CN2457118 Y CN 2457118Y
- Authority
- CN
- China
- Prior art keywords
- electrode
- reaction tube
- tube
- crystal reaction
- cnt
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Images
Abstract
The utility model relates to a plasma device used for preparing a nanometer carbon tube. The utility model is characterized in that the anodes and the cathodes of two electrodes fixed to a sealing plug of a sealing quartz reaction tube are arranged in the quartz reaction tube; the ends of the anodes of the electrodes are made into a tip shape, and the ends of the cathodes of the electrodes are made into a platform shape the quartz reaction tube is provided with an air inlet nozzle and an air outlet nozzle. The utility model adopts the mode of plasma polymerization and creates a nanometer carbon tube with the inner diameters being 4 to 6 nm and the outer diameters being 22 to 30 nm. Needed energy does not need to be cracked by high temperature, which causes the theory conversion degree to achieve 100%. The utility model provides a new way for preparing nanometer carbon tubes.
Description
The utility model relates to preparation CNT (carbon nano-tube) device, and especially a kind of plasma body prepares the CNT (carbon nano-tube) device.
Nanotechnology is with a wide range of applications as current a kind of new high-tech material.But the technology of existing preparation CNT (carbon nano-tube) generally adopts arc discharge, heat and catalytic decomposition, chemical vapour desposition method to produce, and needs a large amount of energy and heat, the cost height.
The purpose of this utility model is to overcome the deficiency of prior art, provides a kind of simple in structure, the using plasma polymerization methods and need not any catalyzer situation under the device of preparation CNT (carbon nano-tube).
The purpose of this utility model is achieved in that
The positive and negative electrode that is packed in two electrodes on the sealing crystal reaction tube sealing plug places in the crystal reaction tube, the electrode anode end is made as pointed, the negative pole end is made as platform-like, on crystal reaction tube, be shaped on an admission piece and an outlet nozzle, admission piece is at the crystal reaction tube position of electrode anode, and outlet nozzle is built in electrode negative pole crystal reaction tube position.
Electrode anode tip diameter is 0.2-0.6mm, and electrode negative pole platform diameter is 4-12mm, and land thickness is 2mm, and the quartz reaction bore is 6-15mm; The gas that the made admission piece of crystal reaction tube feeds is the gas mixture of hydrogen and acetylene gas; The distance of electrode positive and negative electrode end is 5-25mm, and electrode is made by isometrical round brass rod or stainless steel bar.
Advantage of the present utility model and positively effect are:
The using plasma polymerization methods; at normal temperatures; produce the CNT (carbon nano-tube) of internal diameter 4-6nm, external diameter 22-30nm by corona discharge; do not need to come cracking institute energy requirement with high temperature; thereby exempted to environment and conducted heat and save energy; simultaneously also exempted the fuel that is used to provide reaction heat, made theoretical yield reach 100%, very favourable to environment protection.And it is structural good that the CNT (carbon nano-tube) of normal temperature preparation has, and the dispersity height does not use any catalyzer, for the preparation CNT (carbon nano-tube) provides a new road.
Description of drawings:
Fig. 1 is a structural representation of the present utility model;
Below in conjunction with accompanying drawing the utility model embodiment is described in further detail:
Optimum mode of operation of the present utility model is:
Battery lead rod footpath: 3mm;
Electrode anode tip diameter: 0.3mm;
Electrode negative pole platform diameter: 5mm;
Electrode negative pole land thickness: 1.5mm;
Electrode anode end and electrode anode end distance: 8mm;
Silica tube internal diameter: 8mm;
Feed acetylene gas flow: 23.8ml/min;
Feed hydrogen flowing quantity: 28.4ml/min;
Electrode voltage: 11000v; 50Hz.
Workflow of the present utility model is: feed rare gas element earlier, as Ar, after 10 minutes, feed the gas mixture of acetylene gas and hydrogen, between electrode, add dc pulse current, increase voltage gradually and lie prostrate to 6000-1300,50 hertz, produce corona discharge this moment, and the reaction times is 1-20 minute, reduces voltage gradually after reaction finishes, reduce frequency, after discharge on the positive pole, take out the cotton-shaped product between two electrodes with discharge rod, be the CNT (carbon nano-tube) of internal diameter 4-6nm, external diameter 22-30nm.
Claims (4)
1. a plasma body prepares the CNT (carbon nano-tube) device, constitute by crystal reaction tube, electrode positive and negative electrode, sealing plug, it is characterized in that: the positive and negative electrode that is packed in two electrodes on the sealing crystal reaction tube sealing plug places in the crystal reaction tube, the electrode anode end is made as pointed, the negative pole end is made as platform-like, be shaped on an admission piece and an outlet nozzle on crystal reaction tube, admission piece is at the crystal reaction tube position of electrode anode, and outlet nozzle is built in electrode negative pole crystal reaction tube position.
2. plasma body according to claim 1 prepares the CNT (carbon nano-tube) device, it is characterized in that: electrode anode tip diameter is 0.2-0.6mm, and electrode negative pole platform diameter is 4-12mm, and land thickness is 2mm, and the quartz reaction bore is 6-15mm.
3. plasma body according to claim 1 prepares the CNT (carbon nano-tube) device, it is characterized in that: the gas that the made admission piece of crystal reaction tube feeds is the gas mixture of hydrogen and acetylene gas.
4. prepare the CNT (carbon nano-tube) device according to claim 1,2 described plasma bodys, it is characterized in that: the distance of electrode positive and negative electrode end is 5-25mm, and electrode is made by isometrical round brass rod or stainless steel bar.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 00263593 CN2457118Y (en) | 2000-12-07 | 2000-12-07 | Plasma preparing nanometer carbon tube device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 00263593 CN2457118Y (en) | 2000-12-07 | 2000-12-07 | Plasma preparing nanometer carbon tube device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN2457118Y true CN2457118Y (en) | 2001-10-31 |
Family
ID=33618545
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 00263593 Expired - Fee Related CN2457118Y (en) | 2000-12-07 | 2000-12-07 | Plasma preparing nanometer carbon tube device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN2457118Y (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101857218A (en) * | 2010-06-11 | 2010-10-13 | 垦利三合新材料科技有限责任公司 | Method for preparing nano carbon spheres |
| WO2013097545A1 (en) * | 2011-12-28 | 2013-07-04 | 温州医学院 | Modification method for reducing cytotoxicity of carbon nano-tubes |
| CN107779236A (en) * | 2017-11-10 | 2018-03-09 | 李明 | A kind of black petroleum products deep processing prepares the preparation method of high perofmrnace lubricating oils additive |
-
2000
- 2000-12-07 CN CN 00263593 patent/CN2457118Y/en not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101857218A (en) * | 2010-06-11 | 2010-10-13 | 垦利三合新材料科技有限责任公司 | Method for preparing nano carbon spheres |
| WO2013097545A1 (en) * | 2011-12-28 | 2013-07-04 | 温州医学院 | Modification method for reducing cytotoxicity of carbon nano-tubes |
| CN107779236A (en) * | 2017-11-10 | 2018-03-09 | 李明 | A kind of black petroleum products deep processing prepares the preparation method of high perofmrnace lubricating oils additive |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103179772B (en) | Produce method and the special purpose device thereof of DC Atmospheric Pressure Glow Discharge | |
| CN102610398B (en) | Device and method for preparing electrode of vertical graphene double electric layer capacitor at constant voltage | |
| CN100415643C (en) | Cathode gas film microarc discharging method for preparing carbon nanometer material in solution | |
| CN2457118Y (en) | Plasma preparing nanometer carbon tube device | |
| CN100515935C (en) | Carbon nano-tube growth apparatus and method | |
| KR100468845B1 (en) | Method of fabricating carbon nano tube | |
| CN1188073A (en) | Method for preparing Fullerenes carbon material and its use in battery electrode material | |
| CN1248248C (en) | Technology and equipment for preparing magnetic carbon nanometer tube by plasma | |
| CN105236352A (en) | Direct coupling microwave liquid-phase plasma alcohol hydrogen production device and method | |
| CN114294130B (en) | Plasma-based ammonia catalytic hydrogen production-ignition integrated system and method | |
| CN103981531A (en) | Preparation method of fluorescent carbon dots | |
| CN104725271A (en) | Method for preparing aminoacetonitrile and N,N-dimethylcyanamide from methane and ammonia gas through plasma synthesis | |
| CN115029021A (en) | Preparation method of large-particle-size low-structure soft carbon black | |
| CN205419766U (en) | Direct coupling microwave liquid phase plasma alcohols hydrogen plant | |
| CN103086406A (en) | Preparation method of magnesium oxide nanobelt-carbon nanotube composite material | |
| CN1837028A (en) | Generating device and method for producing hydrogen by using nonequilibrium plasma | |
| CN211436164U (en) | Device for simultaneously preparing hydrogen-rich synthesis gas and carbon nanoparticles | |
| CN203070938U (en) | Device used for preparing electrode of vertical graphene double electric layer capacitor at atmospheric pressure | |
| CN206071754U (en) | A kind of vehicle-mounted online fuel modifying device | |
| CN207903908U (en) | A kind of Combined type low-temperature plasma reactor | |
| CN201284231Y (en) | Serial connected ceramic ozone generating device | |
| CN217511839U (en) | Plasma natural gas cracking device | |
| CN110841577A (en) | Device for simultaneously preparing hydrogen-rich synthesis gas and carbon nanoparticles | |
| CN1216019C (en) | High-frequency plasma natural gas cracking process of synthesizing C2 hydrocarbon | |
| CN200990473Y (en) | Needle array electrode bipolar discharger |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C19 | Lapse of patent right due to non-payment of the annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |