CN220223603U - Yellow phosphorus refining rinsing pipe - Google Patents
Yellow phosphorus refining rinsing pipe Download PDFInfo
- Publication number
- CN220223603U CN220223603U CN202321701443.4U CN202321701443U CN220223603U CN 220223603 U CN220223603 U CN 220223603U CN 202321701443 U CN202321701443 U CN 202321701443U CN 220223603 U CN220223603 U CN 220223603U
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- Prior art keywords
- rinsing
- pipe
- tank
- yellow phosphorus
- water
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- OBSZRRSYVTXPNB-UHFFFAOYSA-N tetraphosphorus Chemical compound P12P3P1P32 OBSZRRSYVTXPNB-UHFFFAOYSA-N 0.000 title claims abstract description 53
- 238000007670 refining Methods 0.000 title claims abstract description 38
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 86
- 239000007921 spray Substances 0.000 claims abstract description 36
- 238000004062 sedimentation Methods 0.000 claims abstract description 19
- 238000003860 storage Methods 0.000 claims abstract description 13
- 239000008237 rinsing water Substances 0.000 claims abstract description 12
- 230000001105 regulatory effect Effects 0.000 claims description 20
- 238000009413 insulation Methods 0.000 claims description 6
- 238000004321 preservation Methods 0.000 claims description 4
- 238000005507 spraying Methods 0.000 claims description 4
- 238000007789 sealing Methods 0.000 claims description 2
- 238000011084 recovery Methods 0.000 abstract description 8
- 230000000694 effects Effects 0.000 abstract description 5
- 238000000034 method Methods 0.000 abstract description 5
- 230000008569 process Effects 0.000 abstract description 4
- 238000012545 processing Methods 0.000 abstract description 4
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 16
- 229910052698 phosphorus Inorganic materials 0.000 description 14
- 239000011574 phosphorus Substances 0.000 description 14
- 239000012535 impurity Substances 0.000 description 6
- 238000003756 stirring Methods 0.000 description 5
- 238000012986 modification Methods 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- 239000010802 sludge Substances 0.000 description 3
- 230000008859 change Effects 0.000 description 2
- 238000012423 maintenance Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 230000002035 prolonged effect Effects 0.000 description 2
- 238000012546 transfer Methods 0.000 description 2
- 230000007306 turnover Effects 0.000 description 2
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 230000003014 reinforcing effect Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
Landscapes
- Cleaning By Liquid Or Steam (AREA)
Abstract
The utility model relates to the technical field of yellow phosphorus recovery processing, in particular to a yellow phosphorus refining rinsing pipe, wherein a water supply pipe is arranged above a yellow phosphorus refining tank; the lower parts of the water supply pipes are respectively connected with a rinsing spray pipe through a diverter valve; the rinsing spray pipe is vertically arranged in the yellow phosphorus refining tank; the side surface of the water supply pipe is connected with an air supply pipe through a buckle; a rinsing steam pipe is vertically arranged on the side surface of the air supply pipe; an overflow port is arranged on the side surface of the top of the yellow phosphorus refining tank; the overflow port is connected with the sedimentation tank; the other end of the sedimentation tank is connected with a clean water tank; the upper part of the clean water tank is provided with a submersible pump; the submersible pump is connected with the water supply pipe; the other end of the air supply pipe is connected with a steam storage tank; a gas supply pipe at the front end of the steam storage tank is provided with a total gas valve; a plurality of water spray ports are arranged on the side surface of the rinsing water spray pipe; the side surface of the rinsing steam pipe is provided with a plurality of steam holes in a arraying way, so that the problem that the rinsing and tumbling effects are poor in the yellow phosphorus processing process, and the recovery time is too long is solved; and problems with the background art.
Description
Technical Field
The utility model relates to the technical field of yellow phosphorus recovery processing, in particular to a yellow phosphorus refining rinsing pipe.
Background
The yellow phosphorus rinsing steam has the functions of continuously keeping the temperature and speed of stirring, stirring and separating the combination of phosphorus and impurities, and the rinsing water has the functions of continuously keeping the combination of phosphorus and impurities to stir, stirring and separating the impurities and taking away the separated impurities, so that the yellow phosphorus and the sludge phosphorus are rapidly analyzed. Along with the shortage of yellow phosphorus ore resources, the quality is reduced, impurities contained in the ore are increased, the contents of associated impurities such as tar, sludge phosphorus and the like in the yellow phosphorus in the production process are high, the phosphorus quality is reduced, and the refining rinsing time is prolonged. The traditional method for refining yellow phosphorus for rinsing phosphorus adopts a stainless steel pipe to be directly inserted into the bottom of a tank, and the bottom is stirred, turned over and separated by utilizing steam temperature and water pressure; if the water and steam pressure is low, the stirring and tumbling functions are not provided, the phosphorus separation effect is poor, the period is prolonged, the rinsing time is increased by about 1 week, the phosphorus rinsing recovery can be completed, and the current production condition is not satisfied. When serious, the refining system is blocked, a large amount of mud phosphorus is rinsed and recovered without a tank, and vicious circle is caused until stopping treatment; in the prior art, (1) the pressure of steam and rinsing water is too small, phosphorus returns to a pipeline to be blocked, personnel are in the process of cleaning the blockage, so that personal injury is caused (2) in the process of recovering and rinsing the phosphorus, the water is fed from the bottom, the steam is fed, the middle part and the upper part are not stirred, overturned and rinsed, the phosphorus recovery time is increased, the efficiency is low, the consumption of the rinsing steam and the water is increased, the cost is increased, and the system is blocked and stopped.
Disclosure of Invention
The utility model aims to provide a yellow phosphorus refined rinsing pipe, which solves the problems of poor rinsing and tumbling effects and overlong recovery time in the yellow phosphorus processing process; and problems with the background art.
In order to solve the technical problems, the utility model adopts the following technical scheme:
a yellow phosphorus refining rinsing pipe comprises a yellow phosphorus refining tank, a rinsing spray pipe, a rinsing steam pipe, an overflow port, a sedimentation tank, a clean water tank, a submersible pump, a filter screen, a water supply pipe, a pressure regulating pump, a pressure regulating water bin, a flow dividing valve, a steam storage tank, a total air valve, an air supply pipe and a flow dividing air valve; a water supply pipe is arranged above the yellow phosphorus refining tank; the lower parts of the water supply pipes are respectively connected with a rinsing spray pipe through a diverter valve; the rinsing spray pipe is vertically arranged in the yellow phosphorus refining tank; the side surface of the water supply pipe is connected with an air supply pipe through a buckle; a rinsing steam pipe is vertically arranged on the side surface of the air supply pipe; an overflow port is arranged on the side surface of the top of the yellow phosphorus refining tank; the overflow port is connected with the sedimentation tank; the other end of the sedimentation tank is connected with a clean water tank; the upper part of the clean water tank is provided with a submersible pump; the submersible pump is connected with the water supply pipe; the other end of the air supply pipe is connected with a steam storage tank; a gas supply pipe at the front end of the steam storage tank is provided with a total gas valve; a plurality of water spray ports are arranged on the side surface of the rinsing water spray pipe; the side surface of the rinsing steam pipe is provided with a plurality of steam holes in a row.
Further, the water spraying port is arranged in a horn-shaped structure; the bottom of the water jet is provided with a one-way valve.
Further, the upper part of the water supply pipe is provided with a pressure regulating sump; the front end of the pressure regulating water bin is provided with a pressure regulating pump.
Further, the bottoms of the sedimentation tank and the clean water tank are respectively provided with a mud discharge port; a filter screen is obliquely arranged in the clean water tank.
Further, the rinsing steam pipe and the air supply pipe are movably connected; and connected through sealing threads.
Further, a heat preservation and insulation layer is arranged inside the rinsing steam pipe.
Further, the bottom of the rinsing spray pipe is arranged on the supporting table; the supporting table top is provided with a groove.
Compared with the prior art, the utility model can realize one of the following beneficial effects:
1. a water supply pipe is arranged above the yellow phosphorus refining tank; the lower parts of the water supply pipes are respectively connected with a rinsing spray pipe through a diverter valve; the rinsing spray pipe is vertically arranged in the yellow phosphorus refining tank; the side surface of the water supply pipe is connected with an air supply pipe through a buckle; a rinsing steam pipe is vertically arranged on the side surface of the air supply pipe; an overflow port is arranged on the side surface of the top of the yellow phosphorus refining tank; the overflow port is connected with the sedimentation tank; the other end of the sedimentation tank is connected with a clean water tank; the upper part of the clean water tank is provided with a submersible pump; the submersible pump is connected with the water supply pipe; the other end of the air supply pipe is connected with a steam storage tank; a gas supply pipe at the front end of the steam storage tank is provided with a total gas valve; a plurality of water spray ports are arranged on the side surface of the rinsing water spray pipe; the side surface of the rinsing steam pipe is provided with a plurality of steam holes in an arrangement manner, so that a plurality of rinsing water spray pipes and rinsing steam pipes are arranged in the yellow phosphorus refining tank, and water flow and air flow are provided in the yellow phosphorus refining tank, so that the phosphorus mud water in the yellow phosphorus refining tank is enabled to fully turn over, and the recovery efficiency of the yellow phosphorus is improved.
2. The water spraying port is arranged in a horn-shaped structure; the water jet bottom is provided with the check valve, can realize the water jet reinforcing rivers effect that sets up through loudspeaker formula structure to set up the check valve and prevent the phosphor water backward flow.
3. The upper part of the water supply pipe is provided with a pressure regulating sump; the pressure regulating pump is arranged at the front end of the pressure regulating water bin, so that the water pressure of the rinsing water spray pipe can be conveniently controlled through the arranged pressure regulating pump, and the practicability is improved.
4. Mud outlets are respectively arranged at the bottoms of the sedimentation tank and the clean water tank; the filter screen is obliquely arranged in the clean water tank, so that the sedimentation tank and the clean water tank can be cleaned conveniently through the arranged sludge discharge port, and the arranged filter screen can prevent the submersible pump from being blocked by sundries.
5. The rinsing steam pipe and the air supply pipe are arranged in a movable connection structure; and through sealed threaded connection, can realize through the swing joint rinsing steam pipe that sets up can in time change the maintenance when the steam hole is blockked up, improved the practicality.
6. The inside thermal insulation layer that keeps warm that is provided with of rinsing steam pipe can realize reducing the heat transfer that rinsing steam pipe inserted yellow phosphorus refining tank through the thermal insulation layer that sets up.
7. The bottom of the rinsing spray pipe is arranged on the supporting table; the supporting bench top is provided with the recess, can realize supporting the rinsing spray pipe through the supporting bench that sets up to make rinsing spray pipe and delivery pipe whole stable setting in yellow phosphorus refining tank.
Drawings
FIG. 1 is a schematic diagram of the structure of the present utility model.
FIG. 2 is a schematic view of a structure of a rinsing steam pipe according to the present utility model.
FIG. 3 is a schematic view of a rinse spray pipe of the present utility model.
Detailed Description
The present utility model will be described in further detail with reference to the drawings and examples, in order to make the objects, technical solutions and advantages of the present utility model more apparent. It should be understood that the specific embodiments described herein are for purposes of illustration only and are not intended to limit the scope of the utility model.
Example 1
A yellow phosphorus refining rinsing pipe comprises a yellow phosphorus refining tank 1, a rinsing spray pipe 2, a rinsing steam pipe 3, an overflow port 4, a sedimentation tank 5, a clean water tank 6, a submersible pump 7, a filter screen 8, a water supply pipe 9, a pressure regulating pump 10, a pressure regulating water sump 11, a flow dividing valve 12, a steam storage tank 13, a main air valve 14, an air supply pipe 15 and a flow dividing air valve 16; a water supply pipe 9 is arranged above the yellow phosphorus refining tank 1; the lower parts of the water supply pipes 9 are respectively connected with a rinsing spray pipe 2 through a diverter valve 12; the rinsing spray pipe 2 is vertically arranged in the yellow phosphorus refining tank 1; the side surface of the water supply pipe 9 is connected with an air supply pipe 15 through a buckle 22; a rinsing steam pipe 3 is vertically arranged on the side surface of the air supply pipe 15; an overflow port 4 is arranged on the side surface of the top of the yellow phosphorus refining tank 1; the overflow port 4 is connected with a sedimentation tank 5; the other end of the sedimentation tank 5 is connected with a clean water tank 6; the upper part of the clean water tank 6 is provided with a submersible pump 7; the submersible pump 7 is connected with a water supply pipe 9; the other end of the air supply pipe 15 is connected with the steam storage tank 13; a gas supply pipe 15 at the front end of the steam storage tank 13 is provided with a total gas valve 14; a plurality of water spray ports 20 are arranged on the side surface of the rinsing water spray pipe 2; the side surface of the rinsing steam pipe 3 is provided with a plurality of steam holes 17, so that the purpose that the yellow phosphorus recovery efficiency is improved by arranging a plurality of rinsing water spray pipes and rinsing steam pipes in the yellow phosphorus refining tank and providing water flow and air flow in the yellow phosphorus refining tank to enable the phosphorus mud in the yellow phosphorus refining tank to fully turn over can be achieved.
Example 2
On the basis of the embodiment 1, the water spraying ports 20 are arranged in a horn-shaped structure; the bottom of the water jet 20 is provided with a one-way valve 21, so that the water jet enhanced water jet effect through the horn-shaped structure can be realized, and the one-way valve is arranged to prevent the backflow of the phosphor water.
Example 3
On the basis of the embodiment 1, the upper part of the water supply pipe 9 is provided with a pressure regulating water bin 11; the pressure regulating pump 10 is arranged at the front end of the pressure regulating water bin 11, so that the water pressure of the rinsing water spray pipe can be conveniently controlled through the arranged pressure regulating pump, and the practicability is improved.
Example 4
On the basis of the embodiment 1, the bottoms of the sedimentation tank 5 and the clean water tank 6 are respectively provided with a mud discharge port 19; the filter screen 8 is obliquely arranged in the clean water tank 6, so that the sedimentation tank and the clean water tank can be cleaned conveniently through the arranged mud discharging port, and the arranged filter screen can prevent the submersible pump from being blocked by sundries.
Example 5
On the basis of the embodiment 1, the rinsing steam pipe 3 and the air supply pipe 15 are arranged in a movable connection structure; and through sealed screw 24 connection, can realize through the swing joint rinsing steam pipe that sets up can in time change the maintenance when the steam hole is blockked up, improved the practicality.
Example 6
On the basis of the embodiment 1, the heat preservation and insulation layer 18 is arranged inside the rinsing steam pipe 3, so that the heat transfer of the rinsing steam pipe inserted into the yellow phosphorus refining tank can be reduced through the arranged heat preservation and insulation layer.
Example 7
On the basis of the embodiment 1, the bottom of the rinsing spray pipe 2 is arranged on a supporting table 23; the supporting bench 23 top is provided with the recess, can realize supporting the rinsing spray pipe through the supporting bench that sets up to make rinsing spray pipe and delivery pipe whole stable setting in yellow phosphorus refining tank.
Although the utility model has been described herein with reference to a number of illustrative embodiments thereof, it should be understood that numerous other modifications and embodiments can be devised by those skilled in the art that will fall within the scope and spirit of the principles of this disclosure. More specifically, various variations and modifications may be made to the component parts and/or arrangements of the subject combination arrangement within the scope of the disclosure, drawings and claims of this application. In addition to variations and modifications in the component parts and/or arrangements, other uses will be apparent to those skilled in the art.
Claims (7)
1. A yellow phosphorus refining rinsing pipe is characterized in that: the device comprises a yellow phosphorus refining tank (1), a rinsing water spray pipe (2), a rinsing steam pipe (3), an overflow port (4), a sedimentation tank (5), a clean water tank (6), a submersible pump (7), a filter screen (8), a water supply pipe (9), a pressure regulating pump (10), a pressure regulating water bin (11), a diverter valve (12), a steam storage tank (13), a total air valve (14), an air supply pipe (15) and a diverter air valve (16); a water supply pipe (9) is arranged above the yellow phosphorus refining tank (1); the lower parts of the water supply pipes (9) are respectively connected with a rinsing spray pipe (2) through a diverter valve (12); the rinsing spray pipe (2) is vertically arranged in the yellow phosphorus refining tank (1); the side surface of the water supply pipe (9) is connected with an air supply pipe (15) through a buckle (22); a rinsing steam pipe (3) is vertically arranged on the side surface of the air supply pipe (15); an overflow port (4) is arranged on the side surface of the top of the yellow phosphorus refining tank (1); the overflow port (4) is connected with the sedimentation tank (5); the other end of the sedimentation tank (5) is connected with a clean water tank (6); the upper part of the clean water tank (6) is provided with a submersible pump (7); the submersible pump (7) is connected with the water supply pipe (9); the other end of the air supply pipe (15) is connected with a steam storage tank (13); a gas supply pipe (15) at the front end of the steam storage tank (13) is provided with a total gas valve (14); a plurality of water spray ports (20) are arranged on the side surface of the rinsing water spray pipe (2); the side surface of the rinsing steam pipe (3) is provided with a plurality of steam holes (17) in a row.
2. A yellow phosphorus refined rinse tube as claimed in claim 1, wherein: the water spraying port (20) is arranged in a horn-shaped structure; the bottom of the water jet (20) is provided with a one-way valve (21).
3. A yellow phosphorus refined rinse tube as claimed in claim 1, wherein: the upper part of the water supply pipe (9) is provided with a pressure regulating water bin (11); the front end of the pressure regulating water bin (11) is provided with a pressure regulating pump (10).
4. A yellow phosphorus refined rinse tube as claimed in claim 1, wherein: mud outlets (19) are respectively formed in the bottoms of the sedimentation tank (5) and the clean water tank (6); a filter screen (8) is obliquely arranged in the clean water tank (6).
5. A yellow phosphorus refined rinse tube as claimed in claim 1, wherein: the rinsing steam pipe (3) and the air supply pipe (15) are arranged in a movable connection structure; and connected by means of a sealing thread (24).
6. A yellow phosphorus refined rinse tube as claimed in claim 1, wherein: the rinsing steam pipe (3) is internally provided with a heat preservation and insulation layer (18).
7. A yellow phosphorus refined rinse tube as claimed in claim 1, wherein: the bottom of the rinsing spray pipe (2) is arranged on the supporting table (23); the top of the supporting table (23) is provided with a groove.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321701443.4U CN220223603U (en) | 2023-06-30 | 2023-06-30 | Yellow phosphorus refining rinsing pipe |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321701443.4U CN220223603U (en) | 2023-06-30 | 2023-06-30 | Yellow phosphorus refining rinsing pipe |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN220223603U true CN220223603U (en) | 2023-12-22 |
Family
ID=89183507
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202321701443.4U Active CN220223603U (en) | 2023-06-30 | 2023-06-30 | Yellow phosphorus refining rinsing pipe |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN220223603U (en) |
-
2023
- 2023-06-30 CN CN202321701443.4U patent/CN220223603U/en active Active
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20240503 Address after: 650000 Production Area of Xiaohaikou Zhongqing Yilan (Group) Co., Ltd., Xishan District, Kunming City, Yunnan Province Patentee after: Kunming Baozhuo Chemical Co.,Ltd. Country or region after: China Patentee after: Yunnan Jinning yellow phosphorus Co.,Ltd. Address before: 650000 Production Area of Xiaohaikou Zhongqing Yilan (Group) Co., Ltd., Xishan District, Kunming City, Yunnan Province Patentee before: Kunming Baozhuo Chemical Co.,Ltd. Country or region before: China |