CN220126176U

CN220126176U - Purification device

Info

Publication number: CN220126176U
Application number: CN202321717124.2U
Authority: CN
Inventors: 王宏伟; 臧建斌; 潘正刚
Original assignee: Xinjiang Jinshenghui Chemical Co ltd
Current assignee: Xinjiang Jinshenghui Chemical Co ltd
Priority date: 2023-07-03
Filing date: 2023-07-03
Publication date: 2023-12-05
Anticipated expiration: 2033-07-03

Abstract

The utility model discloses a purifying device, which belongs to the technical field of material purification and comprises a base and a reaction box arranged at the top end of the base, wherein a mixing paddle for accelerating the mixing speed is arranged on the vertical inner wall of the reaction box, a driving motor for providing adjusting power for the mixing paddle is arranged on the side surface of the reaction box, one end of the mixing paddle, which is far away from the driving motor, penetrates through the reaction box and is connected with a transmission shaft, the top end of the reaction box is welded with a rectangular mounting plate, the side surface of the mounting plate is connected with a driven shaft, the driven shaft is in transmission connection with the transmission shaft through a belt, the top end of the reaction box is communicated with a feed hopper, the feed hopper is arranged at a feed opening and is provided with a screw rod for controlling the feed speed, and the shaft end of the screw rod penetrates through the feed hopper and is connected with the transmission shaft. This purification device can prevent that the catalyst from piling up to shorten the reaction duration, can not influence holistic purification duration.

Description

Purification device

Technical Field

The utility model belongs to the technical field of material purification, and particularly relates to a purification device.

Background

Dimethyl disulfide is mainly used as a solvent and an intermediate of pesticides, and is also a main raw material of methylsulfonyl chloride and methylsulfonic acid products, a purification device is needed when dimethyl two streams are purified, the dimethyl two streams are purified in a mixed solution, alkaline substances in the mixed solution are needed to be treated, and the purification effect is achieved through distillation, however, when the alkaline substances are removed, the existing purification device is used for removing the alkaline substances through adding a catalyst into a reaction box to react with the mixed solution, the effect of the reaction can be achieved, but the catalyst is possibly accumulated due to the fact that the catalyst is directly added into the reaction box, so that the reaction time is long, and the integral purification duration is affected.

For example, the application number of China is 202121240230.7, a refining separation device for dimethyl disulfide safety production relates to dimethyl disulfide technical field, and comprises a box body, one side fixed mounting of box has servo motor, servo motor's output fixedly connected with dwang, the one end of dwang extends to the inner chamber of box and fixed surface has cup jointed cam and first bevel gear, the both sides of box inner chamber are all fixedly connected with mounting panel, the inside rotation of mounting panel is connected with the axis of rotation, the fixed surface of axis of rotation one end has cup jointed second bevel gear. Although the reaction effect can be achieved, the catalyst can be accumulated when the catalyst is directly added into the reaction box, so that the reaction time is longer, and the integral purification time is influenced.

Disclosure of Invention

The utility model aims to provide a purifying device for solving the problems in the background art.

In order to achieve the above purpose, the present utility model provides the following technical solutions: the utility model provides a purification device, includes the base and establishes the reaction tank on the base top, the mixing rake that accelerates the mixed speed is installed to the vertical inner wall of reaction tank, and the side-mounting of reaction tank has the driving motor that provides the regulation power to the mixing rake, the one end that driving motor was kept away from to the mixing rake runs through the reaction tank and is connected with the transmission shaft, and the top welding of reaction tank has the mounting panel of rectangle, and the mounting panel side is connected with the driven shaft, connects through belt drive between driven shaft and the transmission shaft, the top intercommunication of reaction tank has the feeder hopper, and the feeder hopper is located feed opening department and installs the screw rod of control unloading speed, and the axle head of screw rod runs through the feeder hopper and is connected with the transmission shaft.

Preferably, the bottom of the reaction box is connected with the base through a plurality of supporting legs, and the distiller for purifying subsequent operation is arranged at the top end of the base.

Preferably, two heating plates for accelerating the reaction speed are arranged on two sides of the reaction box, and a protective box is welded on the side surface of the reaction box, on which the heating plates are arranged.

Preferably, a treatment box for treating the reaction gas is arranged at the top end of the reaction box, a fan is arranged at the top end of the reaction box between the connection treatment box and the feed hopper, and an air inlet pipe of the fan is communicated with the reaction box.

Preferably, the air outlet end of the fan is communicated with the treatment box through an air conveying pipe, two through limiting grooves are formed in the inner wall of the treatment box, and springs are mounted on the inner sides of the limiting grooves.

Preferably, the inside of handling case is connected with the installing frame, and the both sides welding of installing frame have two sliders that cooperate the spacing groove to use, and the adsorption layer is installed to the inboard of installing frame.

Preferably, the side welding of processing case has the fixture block of L type, and processing case is located one side of installation fixture block and is connected with the cardboard that is used for carrying out spacing to the installing frame through the pivot.

Compared with the prior art, the utility model has the technical effects and advantages that:

this purification device benefits from driving motor and screw pole's design, rotates through starting driving motor drive mixing oar to drive the driven shaft through the transmission shaft of linkage and rotate, thereby drive the screw pole through the driven shaft and rotate, make the device mix the catalyst of adding simultaneously, effectively prevent to pile up, make mixed liquid and catalytic machine quick mixing, thereby shorten the reaction duration, can not influence holistic purification time.

Thanks to the design of fan and processing case, carry the gas that the inboard reaction of reaction case produced through the fan and extract, carry to the processing incasement, adsorb at the discharge through the adsorbed layer to can guarantee staff's health, and can effectively spacing the installing frame through installing fixture block and cardboard, and release and pop out under the elasticity of spring to the spacing of installing frame is automatic, thereby the adsorbed layer is changed to the staff of being convenient for.

This purification device can prevent that the catalyst from piling up to shorten the reaction duration, can not influence holistic purification duration.

Drawings

In order to more clearly illustrate the embodiments of the present utility model or the technical solutions in the prior art, the drawings that are needed in the description of the embodiments or the prior art will be briefly described, and it is obvious that the drawings in the description below are some embodiments of the present utility model, and other drawings can be obtained according to the drawings without inventive effort for a person skilled in the art.

FIG. 1 is a schematic diagram of the structure of the present utility model;

FIG. 2 is a cross-sectional view of the reaction chamber of FIG. 1 in the direction b-b in accordance with the present utility model;

FIG. 3 is a schematic diagram of a connection structure of a driving motor according to the present utility model;

FIG. 4 is an enlarged view of the utility model at Q in FIG. 1;

FIG. 5 is a cross-sectional view of the treatment tank of FIG. 1 in the direction a-a in accordance with the present utility model.

Reference numerals illustrate:

in the figure: 1. a base; 2. a reaction box; 3. a treatment box; 4. a driving motor; 5. a protective box; 6. a blower; 7. a feed hopper; 8. a mounting plate; 9. a distiller; 10. a driven shaft; 11. a transmission shaft; 12. a screw rod; 13. an adsorption layer; 14. mixing paddles; 15. a mounting frame; 16. a limit groove; 17. a clamping block; 18. a clamping plate; 19. a slide block; 20. and (3) a spring.

Detailed Description

In the following description, numerous specific details are set forth in order to provide a more thorough understanding of the present utility model. It will be apparent, however, to one skilled in the art that the utility model may be practiced without one or more of these details. In other instances, well-known features have not been described in detail in order to avoid obscuring the utility model.

Unless the directions indicated by the individual definitions are used, the directions of up, down, left, right, front, rear, inner and outer are all directions of up, down, left, right, front, rear, inner and outer in the drawings shown in the present utility model, and are described herein together.

The connection mode can adopt the prior modes such as bonding, welding, bolting and the like, and is based on the actual requirement.

1-5, as shown in the fig. 1-5, the vertical inner wall of reaction box 2 installs the mixing rake 14 that accelerates the mixing speed, mixing rake 14 adopts anticorrosive material, specifically according to actual conditions and decide, and the side-mounting of reaction box 2 provides driving motor 4 of adjusting power to mixing rake 14, the one end that driving motor 4 was kept away from to mixing rake 14 runs through reaction box 2 and is connected with transmission shaft 11, the design of mixing rake 14 can accelerate mixing efficiency, and the top welding of reaction box 2 has rectangular mounting panel 8, and mounting panel 8 side is connected with driven shaft 10, driven shaft 10 runs through rotation with mounting panel 8 and is connected, pass through belt transmission between driven shaft 10 and transmission shaft 11 and be connected, the top intercommunication of reaction box 2 has feeder hopper 7, feeder hopper 7 is the design of upper width down narrowly, and feeder hopper 7 is located the feed opening department and installs the hob 12 of control feed speed, the solid catalyst that just can not lead to the catalyst to revealing in the state of hob 12 refinement, and the axle head of hob 12 runs through feeder hopper 7 and transmission shaft 11.

In order to increase the practicality, the bottom of reaction box 2 is connected with base 1 through a plurality of supporting leg, and the distiller 9 that is used for the follow-up operation of purification is installed on the top of base 1, and the solution after the reaction is arranged in distiller 9, realizes the effect of purification through the distillation, and two hot plates that accelerate reaction rate are installed to the reaction box 2 both sides, and the reaction box 2 is located the side welding of installation hot plate and has a protective housing 5, and the design of protective housing 5 can prevent that staff from touching the hot plate and leading to the scald.

In order to handle reaction gas, the processing box 3 that is used for handling reaction gas is installed on the top of reaction box 2, and fan 6 is installed on the top that reaction box 2 is located between connection processing box 3 and the feeder hopper 7, fan 6 is carried the gas that reaction box 2 inboard reaction produced and is extracted, in carrying to processing box 3, adsorb in the discharge through adsorbed layer 13, can guarantee staff's health, and the intake pipe and the reaction box 2 intercommunication of fan 6, the air-out end of fan 6 passes through the air-delivery line and communicates with processing box 3, and the inner wall of processing box 3 is equipped with two spacing grooves 16 of through-type, and spring 20 is installed to the inboard of spacing groove 16, can pop out the installation frame 15 voluntarily under the elasticity of spring 20, the inboard of processing box 3 is connected with installation frame 15, and the both sides welding of installation frame 15 have two sliders 19 that cooperate spacing groove 16 to use, and the inboard of installation frame 15 installs adsorbed layer 13, the material of adsorbed layer 13 is according to actual conditions.

The clamping block 17 of L type has been welded to the side of handling case 3, and the handling case 3 is located one side of installation clamping block 17 and is connected with the cardboard 18 that is used for spacing to installing frame 15 through the pivot, and installation clamping block 17 and cardboard 18 can effectively spacing to installing frame 15, and the side of handling case 3 is equipped with the air exit.

The driving motor 4, the fan 6 and the distiller 9 are all conventional instruments, the working principle, the size and the model are irrelevant to the functions of the utility model, so the functions are not described more, and the functions are controlled by a remote control switch.

Principle of operation

This purification device, when using, be connected with external 220V commercial power with the electronic device of device, connect and accomplish, through in adding the feeder hopper 7 with the catalyst, through driving motor 4 drive mixing paddle 14 rotate, thereby drive driven shaft 10 through the transmission shaft 11 of linkage and rotate, thereby drive hob 12 through driven shaft 10 and rotate, make the device mix and add the catalyst simultaneously, the mixing is accomplished, the heating plate is started and is heated to appointed temperature, make mixed liquor react with the catalyst, and start the gas that produces through fan 6 with the inboard reaction of reaction tank 2 and extract, carry in the treatment tank 3, adsorb reaction gas through adsorbed layer 13, gas discharge after adsorbing through the gas vent after the adsorption treatment, and the solution that the reaction is accomplished is carried to distiller 9 and is distilled the purification can.

It should be noted that relational terms such as one and two are used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Moreover, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus. Without further limitation. The term "comprising" an element defined by the term "comprising" does not exclude the presence of other identical elements in a process, method, article or apparatus that comprises the element.

Although embodiments of the present utility model have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made therein without departing from the principles and spirit of the utility model, the scope of which is defined in the appended claims and their equivalents.

Claims

1. The utility model provides a purification device, includes base (1) and establishes reaction box (2) on base (1) top, its characterized in that: the vertical inner wall of reaction box (2) is installed and is accelerated mixed oar (14), and the side-mounting of reaction box (2) has drive motor (4) to mixed oar (14) provide regulation power, the one end that drive motor (4) was kept away from to mixed oar (14) runs through reaction box (2) and is connected with transmission shaft (11), and the top welding of reaction box (2) has mounting panel (8) of rectangle, and mounting panel (8) side-mounting has driven shaft (10), is connected through belt drive between driven shaft (10) and transmission shaft (11), the top intercommunication of reaction box (2) has feeder hopper (7), and feeder hopper (7) are located feed opening department and install control unloading speed's hob (12), and the axle head of hob (12) runs through feeder hopper (7) and is connected with transmission shaft (11).

2. A purification apparatus according to claim 1, wherein: the bottom of the reaction box (2) is connected with the base (1) through a plurality of supporting legs, and a distiller (9) for purifying subsequent operations is arranged at the top end of the base (1).

3. A purification apparatus according to claim 2, wherein: two heating plates for accelerating the reaction speed are arranged on two sides of the reaction box (2), and a protective box (5) is welded on the side surface of the reaction box (2) where the heating plates are arranged.

4. A purification apparatus according to claim 3, wherein: the top of reaction box (2) is installed and is used for handling reaction gas's processing box (3), and fan (6) are installed on the top that reaction box (2) are located between connection processing box (3) and feeder hopper (7), and the intake pipe and the reaction box (2) intercommunication of fan (6).

5. A purification apparatus according to claim 4, wherein: the air outlet end of the fan (6) is communicated with the treatment box (3) through an air delivery pipe, two through limiting grooves (16) are formed in the inner wall of the treatment box (3), and springs (20) are arranged on the inner sides of the limiting grooves (16).

6. A purification apparatus according to claim 5, wherein: the inside of processing case (3) is connected with installing frame (15), and the both sides welding of installing frame (15) have slider (19) that two cooperation spacing groove (16) used, and adsorption layer (13) are installed to the inboard of installing frame (15).

7. A purification apparatus according to claim 6, wherein: the side welding of processing case (3) has fixture block (17) of L type, and processing case (3) are located one side of installation fixture block (17) and are connected with cardboard (18) that are used for carrying out spacing to installing frame (15) through the pivot.