CN219942848U - Sarcosine and hydrazine hydrate reaction device - Google Patents

Abstract

The utility model relates to the technical field of sarcosine and hydrazine hydrate reaction devices, in particular to a sarcosine and hydrazine hydrate reaction device which comprises a bottom plate, wherein an L-shaped vertical rod is arranged on the bottom plate, a liquid separation barrel is arranged on the side face of a fixed plate, a piston plate is arranged at the bottom end of a screw rod, a graduated scale is vertically arranged on the L-shaped vertical rod, the other end of the connecting rod is bent to form a right angle, a lifting block is arranged at the other end of the connecting rod, the graduated scale is arranged in a through hole in a penetrating manner, a connecting pipe is arranged at the upper part of the outer wall of the liquid separation barrel, the screw rod drives the piston plate at the bottom end of the liquid separation barrel to move upwards when moving, liquid at the upper part of the piston plate can be upwards extruded upwards when moving, the lifting block slides on the graduated scale through the through hole when moving, the lifting block controls the quantity of the liquid extruded upwards according to the ascending height of the graduated scale, the effect of controlling flow and injection quantity is achieved in a matching manner, the effect of the liquid injection is effectively avoided, the reaction effect is influenced by too fast or too much, and compared with the traditional reaction device, the liquid mixing reaction effect is better.

Description

Sarcosine and hydrazine hydrate reaction device

Technical Field

The utility model relates to the technical field of reaction devices for sarcosine and hydrazine hydrate, in particular to a reaction device for sarcosine and hydrazine hydrate.

Background

The hydrazine hydrate is an inorganic compound, is colorless transparent fuming liquid, has light ammonia smell, emits smoke in wet air, has strong alkalinity and hygroscopicity, and the creatine is prepared by decomposing caffeine by barium hydroxide or reacting formaldehyde, sodium cyanide and methylamine, is used for synthesizing an enzyme inhibitor, can also be used for synthesizing a biochemical reagent, and needs to be mixed and reacted to obtain a new substance or test reaction effect when the experiment is needed.

One patent with publication number of CN106975429A discloses a liquid mixing reaction device for chemical experiments, which comprises a reaction base, a heating pipe is embedded in the reaction base through a heating controller, the inner heat collecting base is arranged at the upper end edge of the reaction base, a hydraulic controller is arranged at the upper end of a supporting frame, a hydraulic telescopic rod is connected with the hydraulic controller and a mixing rotor, a splash-proof cover is arranged on a sealing sleeve and a movable cover is arranged on a mixing container, and the effect of heating and stirring chemical liquid is achieved through cooperation so as to meet the reaction conditions of the chemical experiments.

The existing reaction device cannot accurately control the injection speed and injection quantity of reactants, so that the reaction effect and the observation data of the mixture can be influenced due to too fast or too much injection, and the observation data is wrong; therefore, a reaction apparatus for sarcosine and hydrazine hydrate is proposed to solve the above problems.

Disclosure of Invention

In order to make up the defects of the prior art, the utility model provides a reaction device for sarcosine and hydrazine hydrate, aiming at the problems in the prior art.

The technical scheme adopted for solving the technical problems is as follows: the utility model discloses a sarcosine and hydrazine hydrate reaction device, which comprises a bottom plate, wherein an L-shaped vertical rod is arranged on the bottom plate, a fixing plate is arranged on the side surface of the L-shaped vertical rod, a liquid separation barrel is arranged on the side surface of the fixing plate, a fixing block is arranged at the end part of the vertical section of the L-shaped vertical rod, a threaded hole is formed in the fixing block in a penetrating manner, a screw rod is arranged in the threaded hole in a penetrating manner, a piston plate is arranged at the bottom end of the screw rod, the piston plate is positioned in the liquid separation barrel, a rotating disc is arranged at the top end of the screw rod, an annular limiting strip is arranged at the inner edge of an opening at the upper part of the liquid separation barrel, a scale is vertically arranged on the L-shaped vertical rod, a connecting rod is rotatably arranged on the rotating disc, a lifting block is arranged at the other end of the connecting rod in a right angle in a penetrating manner, a through hole is formed in the lifting block in a penetrating manner, a connecting pipe is arranged at the upper part of the outer wall of the liquid separation barrel, the connecting pipe is arranged at the connecting pipe, the mounting position is positioned under the annular limiting strip, the effect of controlling flow and excessive injection quantity is achieved in a matching manner, the effect is effectively avoided, and the liquid injection is too fast or the effect is better compared with the traditional reaction device.

Preferably, two L-shaped vertical rods are symmetrically arranged on the bottom plate, the upper members of the two L-shaped vertical rods are identical, the other ends of the connecting pipes on the liquid separation barrel are symmetrically and inwards provided with a mixing barrel, the connecting pipes are arranged on the upper part of the mixing barrel, the effect of liquid mixing is achieved through cooperation, and the normal use of the reaction device is ensured.

Preferably, the liquid separation barrel is located under the vertical section of the L-shaped vertical rod, the vertical section of the L-shaped vertical rod is parallel to the bottom plate, the central line axis of the screw rod and the piston plate is collinear with the central axis of the liquid separation barrel, and the air holes are formed in the inner bottom of the liquid separation barrel in a penetrating manner, so that the piston plate can move upwards in the liquid separation barrel in a matched manner, and liquid in the liquid separation barrel is extruded upwards.

Preferably, two backup pads are installed on the bottom plate symmetry, install the blending tank in two backup pads, be provided with the motor under the blending tank, the stirring vane is installed to the motor output shaft running through the blending tank, and the cooperation has reached the effect of mixing with higher speed.

Preferably, the motor is located between two backup pads, the mixing drum side runs through and is provided with the heating rod, install heating controller on the mixing drum outer wall, just the heating rod is connected on heating controller, and the cooperation has reached the effect of accelerating the liquid reaction, makes the reaction unit in this scheme can be suitable for different liquid mixing experiment requirements.

Preferably, the motor is arranged on the bottom plate, a discharging pipe is arranged at the outer bottom of the mixing drum, and a valve is arranged on the discharging pipe to realize the effect of discharging mixed liquid in a matched mode.

The utility model has the advantages that:

1. according to the utility model, two liquids are respectively poured into the two liquid separation barrels, the screw rod moves vertically upwards when rotating, the piston plate at the bottom end of the screw rod is driven to move upwards when moving, the liquid at the upper part of the piston plate is extruded upwards when the piston plate moves upwards, the liquid in the liquid separation barrel flows into the mixing barrel through the connecting pipe when the liquid level rises to the connecting pipe, the lifting block slides on the graduated scale through the through hole when moving, the quantity of the liquid extruded upwards by the piston plate is controlled according to the rising height of the lifting block on the graduated scale, the effects of controlling the flow and the injection quantity are achieved in cooperation, the effect that the liquid injection is too fast or too much influences the reaction effect is effectively avoided, and compared with the traditional reaction device, the liquid mixing reaction effect is better.

2. According to the utility model, after liquid enters the mixing barrel, the stirring blades stir and accelerate the mixing of the liquid in the mixing barrel when rotating, the heating controller is matched to control the heating rod to heat the mixed liquid in the mixing barrel, so that the reaction efficiency is improved, the valve is opened after the experiment is completed, the mixed liquid in the mixing barrel can be discharged, the effect of improving the reaction speed is achieved, and the mixing experiment requirements of different liquids can be met.

Drawings

In order to more clearly illustrate the embodiments of the utility model or the technical solutions of the prior art, the drawings which are used in the description of the embodiments or the prior art will be briefly described, it being obvious that the drawings in the description below are only some embodiments of the utility model, and that other drawings can be obtained from these drawings without inventive faculty for a person skilled in the art.

FIG. 1 is a schematic view of a first three-dimensional main body structure;

FIG. 2 is an enlarged schematic view, partially in section, of the body structure of the volume control assembly;

FIG. 3 is an enlarged schematic view of a portion of the main body of the implant volume display device;

FIG. 4 is an enlarged schematic view of the main body structure of the lifting block assembly;

FIG. 5 is an enlarged schematic view in partial cutaway of the main body structure of the dispensing barrel assembly;

fig. 6 is an enlarged schematic view of a portion of the main structure of the mixing drum assembly.

In the figure: 1. a bottom plate; 2. an L-shaped upright rod; 3. a fixing plate; 4. a liquid separating barrel; 401. ventilation holes; 5. a fixed block; 6. a screw; 7. a piston plate; 8. a rotating disc; 9. an annular limit bar; 10. a graduated scale; 11. a connecting rod; 12. a lifting block; 13. a through hole; 14. a support plate; 15. a mixing drum; 16. a connecting pipe; 17. a motor; 18. stirring blades; 19. a heating rod; 20. a heating controller; 21. a discharge pipe; 22. and (3) a valve.

Detailed Description

The following description of the embodiments of the present utility model will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present utility model, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the utility model without making any inventive effort, are intended to be within the scope of the utility model.

Referring to fig. 1-6, a reaction device for sarcosine and hydrazine hydrate comprises a bottom plate 1, an L-shaped vertical rod 2 is installed on the bottom plate 1, a fixed plate 3 is installed on the side surface of the L-shaped vertical rod 2, a liquid separation barrel 4 is installed on the side surface of the fixed plate 3, a through hole is formed in the end part of a vertical section of the L-shaped vertical rod 2, a screw rod 6 is arranged in the through hole in a penetrating manner in the fixed block 5, a piston plate 7 is installed at the bottom end of the screw rod 6, the piston plate 7 is positioned in the liquid separation barrel 4, a rotary disk 8 is installed at the top end of the screw rod 6, an annular limiting strip 9 is installed at the inner edge of an opening at the upper part of the liquid separation barrel 4, a graduated scale 10 is vertically installed on the L-shaped vertical rod 2, a connecting rod 11 is rotatably installed on the rotary disk 8, a lifting block 12 is installed at a right angle in a bending manner at the other end of the connecting rod 11, a through hole 13 is formed in a penetrating manner on the lifting block 12, a threaded hole is formed in the through hole 13 in a penetrating manner, a threaded hole 16 is formed in the upper part of the outer wall of the liquid separation barrel 4, a connecting pipe 16 is arranged in a penetrating manner, the bottom plate 9 is installed at the bottom plate 6, two symmetrical vertical rods 1 are arranged in the same position as the bottom plate 1, two vertical rod sections are arranged in the vertical rod 4, two vertical rod sections are arranged in the vertical rod 4, and are arranged in the same side 1, and are arranged in the vertical rod 4, and are arranged in the same side, and 2, and the vertical rod 4 is arranged in the vertical rod 4, and the vertical rod 2 is perpendicular to the vertical rod 2.

During operation, because the injection speed and the injection volume of reactant can not be accurately controlled by the existing reaction device, pour into too fast or too much reaction effect and the observation data that can influence the mixture into, lead to observing data mistake, in this scheme, piston plate 7 is located the bottom in dividing liquid bucket 4 under through initial condition, elevating block 12 is located the bottom of calibrated scale 10, pour into two kinds of liquids respectively in dividing liquid bucket 4, pour into two kinds of liquids into after the back and can be located the piston plate 7 upper portion in two dividing liquid bucket 4 respectively, when needs are mixed, twist rotary disk 8, can drive screw rod 6 rotatory when rotary disk 8, and screw rod 6 runs through the threaded hole that sets up at fixed block 5, can vertically upwards move when screw rod 6 rotatory, and drive the piston plate 7 of its bottom and upwards move when moving, can upwards extrude the liquid of its upper portion when piston plate 7 upwards move, will divide liquid in liquid bucket 4 will flow into mixing bucket 15 through connecting pipe 16 when the liquid level rises to connecting pipe 16 department, and can not follow the piston plate 11 tip when rotary disk 8 rotates and can not rotate because of calibrated scale 10, can not drive screw rod 6 and can be moved up through the rotation block 12, can reach the effect of the high-efficient flow rate through the control through the elevating block 12 when the mixed scale 10, the volume of liquid is compared with traditional elevating block 12, can be reached, the effect of controlling the flow rate of liquid is up-flowing through the up through the elevating block 12, and can be more accurate and can be realized through the control device, the up through the elevating block is more than can be realized, the slider is more efficient when the volume is compared with the volume is 12, and has been moved, can be compared with the device.

Referring to fig. 6, the base plate 1 is symmetrically provided with two support plates 14, the two support plates 14 are provided with a mixing drum 15, a motor 17 is arranged under the mixing drum 15, an output shaft of the motor 17 penetrates through the mixing drum 15 to be provided with a stirring blade 18, the motor 17 is positioned between the two support plates 14, a side surface of the mixing drum 15 is provided with a heating rod 19 in a penetrating manner, the outer wall of the mixing drum 15 is provided with a heating controller 20, the heating rod 19 is connected to the heating controller 20, the motor 17 is arranged on the base plate 1, the outer bottom of the mixing drum 15 is provided with a discharging pipe 21, and the discharging pipe 21 is provided with a valve 22.

During operation, for guaranteeing the normal use of reaction unit in this scheme, can be suitable for different liquid mixing experiment requirements, promote mixing efficiency, in this scheme, through liquid in getting into mixing drum 15 after, cooperation starter motor 17, motor 17 starts and can drive stirring vane 18 rotation, can stir the mixed liquid in the mixing drum 15 when stirring vane 18 rotates and accelerate mixing, the cooperation is through heating controller 20 control heating rod 19 to the mixed liquid in the mixing drum 15 heating, and then promote reaction efficiency, open valve 22 after the experiment is accomplished, can discharge the mixed liquid in the mixing drum 15, the cooperation has reached the effect that promotes reaction rate, the realization can be suitable for different liquid mixing experiment requirements.

In the working principle, as the existing reaction device can not accurately control the injection speed and injection amount of reactants, the injection is too fast or too much to influence the reaction effect and observation data of a mixture, and the observation data is wrong, in the scheme, through the fact that a piston plate 7 is positioned at the bottom in a liquid separation barrel 4 in an initial state, a lifting block 12 is positioned at the lowest position of a graduated scale 10, two liquids are respectively poured into the two liquid separation barrels 4, the two liquids are respectively positioned at the upper parts of the piston plates 7 in the two liquid separation barrels 4 after being poured, when the two liquids are required to be mixed, a rotating disk 8 is screwed, a screw rod 6 is driven to rotate when the rotating disk 8 rotates, the screw rod 6 penetrates through a threaded hole formed in a fixed block 5, the screw rod 6 is vertically upwards moved when rotating, and simultaneously drives a piston plate 7 at the bottom end of the screw rod 6 to upwards move, when the piston plate 7 upwards moves, the liquid at the upper part of the piston plate 7 is upwards extruded and lifted, when the liquid level rises to the connecting pipe 16, liquid in the liquid separation barrel 4 flows into the mixing barrel 15 through the connecting pipe 16, the end part of the connecting rod 11 can not follow rotation under the limit of the graduated scale 10 when the rotating disk 8 rotates, the lifting block 12 can be driven to move upwards through the connecting rod 11 when the rotating disk 8 moves upwards, the lifting block 12 can slide on the graduated scale 10 through the through hole 13 when moving, the quantity of the liquid which is extruded upwards by the piston plate 7 is controlled according to the rising height of the lifting block 12 on the graduated scale 10, the flow rate of the liquid flowing to the mixing barrel 15 can be accurately controlled through screwing the lifting piston plate 7 of the screw rod 6, the effect of controlling the flow rate and the injection quantity is achieved in cooperation, the reaction effect is effectively avoided, and compared with the traditional reaction device, the liquid mixing reaction effect is better.

In order to guarantee the normal use of reaction unit in this scheme, can be suitable for different liquid mixing experiment requirements, promote mixing efficiency, in this scheme, through liquid in getting into mixing drum 15 after, cooperation starter motor 17, motor 17 starts and can drive stirring vane 18 rotation, can stir the mixed liquid in the mixing drum 15 when stirring vane 18 rotates and accelerate mixing, the cooperation is through heating controller 20 control heating rod 19 to the mixed liquid in the mixing drum 15, and then promote reaction efficiency, open valve 22 after the experiment is accomplished, can discharge the mixed liquid in the mixing drum 15, the cooperation has reached the effect that promotes reaction rate, the realization can be suitable for different liquid mixing experiment requirements.

In the description of the present specification, the descriptions of the terms "one embodiment," "example," "specific example," and the like, mean that a particular feature, structure, material, or characteristic described in connection with the embodiment or example is included in at least one embodiment or example of the present utility model. In this specification, schematic representations of the above terms do not necessarily refer to the same embodiments or examples. Furthermore, the particular features, structures, materials, or characteristics described may be combined in any suitable manner in any one or more embodiments or examples.

The foregoing has shown and described the basic principles, principal features and advantages of the utility model. It will be understood by those skilled in the art that the present utility model is not limited to the embodiments described above, and that the above embodiments and descriptions are merely illustrative of the principles of the present utility model, and various changes and modifications may be made without departing from the spirit and scope of the utility model, which is defined in the appended claims.

Claims (6)

1. A sarcosine and hydrazine hydrate reaction device is characterized in that: including bottom plate (1), install L shape pole setting (2) on bottom plate (1), L shape pole setting (2) side-mounting has fixed plate (3), fixed plate (3) side-mounting has divide liquid bucket (4), fixed block (5) are installed to L shape pole setting (2) vertical section tip, it sets up threaded hole to run through on fixed block (5), threaded hole runs through and is provided with screw rod (6), piston plate (7) are installed to screw rod (6) bottom, and piston plate (7) are located divides liquid bucket (4), rotary disk (8) are installed on screw rod (6) top, divide liquid bucket (4) upper portion opening inward flange to install annular spacing (9), vertical install scale (10) on L shape pole setting (2), rotate on rotary disk (8) and install connecting rod (11), the other end of connecting rod (11) is right angle and installs lifter (12), it has through-hole (13) to run through on lifter (12), scale (10) run through setting up in through-hole (13), install annular connecting pipe (16) and be located annular connecting pipe (16) position (16) on the connecting pipe.

2. The reaction device for sarcosine and hydrazine hydrate according to claim 1, wherein: two L-shaped vertical rods (2) are symmetrically arranged on the bottom plate (1), the upper components of the two L-shaped vertical rods (2) are identical, a mixing barrel (15) is symmetrically and inwards arranged at the other end of a connecting pipe (16) on the liquid separation barrel (4), and the connecting pipe (16) is arranged on the upper part of the mixing barrel (15).

3. The reaction device for sarcosine and hydrazine hydrate according to claim 1, wherein: the liquid separation barrel (4) is positioned under the vertical section of the L-shaped vertical rod (2), the vertical section of the L-shaped vertical rod (2) is parallel to the bottom plate (1), the central line axis of the screw (6) and the piston plate (7) is collinear with the central axis of the liquid separation barrel (4), and the air holes (401) are formed in the inner bottom of the liquid separation barrel (4) in a penetrating manner.

4. A sarcosine and hydrazine hydrate reaction device according to claim 3, wherein: two backup pads (14) are installed on bottom plate (1) symmetry, install mixing drum (15) on two backup pads (14), be provided with motor (17) under mixing drum (15), stirring vane (18) are installed in motor (17) output shaft run through mixing drum (15).

5. The reaction device for sarcosine and hydrazine hydrate according to claim 4, wherein: the motor (17) is located between the two support plates (14), a heating rod (19) penetrates through the side face of the mixing barrel (15), a heating controller (20) is installed on the outer wall of the mixing barrel (15), and the heating rod (19) is connected to the heating controller (20).

6. The reaction device for sarcosine and hydrazine hydrate according to claim 5, wherein: the motor (17) is arranged on the bottom plate (1), a discharging pipe (21) is arranged at the outer bottom of the mixing drum (15), and a valve (22) is arranged on the discharging pipe (21).