CN218411794U

CN218411794U - Continuous neutralization apparatus of thick sec-octanol

Info

Publication number: CN218411794U
Application number: CN202221640140.1U
Authority: CN
Inventors: 左康会; 王保平
Original assignee: Shandong Juye Youbang Industry Co ltd
Current assignee: Shandong Juye Youbang Industry Co ltd
Priority date: 2022-06-29
Filing date: 2022-06-29
Publication date: 2023-01-31
Anticipated expiration: 2032-06-29

Abstract

The utility model discloses a continuous neutralization device for crude sec-octanol, which comprises a continuous neutralization device body, wherein the continuous neutralization device body comprises a continuous neutralization tower and a middle tank connected with the continuous neutralization tower, the right side of the bottom of the middle tank is communicated and fixed with a sampling detection port, and the bottom end of the sampling detection port is provided with a self-sealing sampling mechanism; the self-sealing sampling mechanism comprises a round box fixedly connected to the bottom end of the sampling and detecting port, the bottom of the round box is provided with an opening, and a communicating hole communicated with the sampling and detecting port is formed in the inner wall of the top of the round box. The utility model discloses be convenient for through simple extruded mode quick sample, be convenient for after the sample automatic close the shutoff of sample detection mouth fast, can effectively avoid forgetting the shutoff due to personnel's carelessness and close the extravagant phenomenon that leads to thick octanol to flow in a large number, and be convenient for shelter from the shutoff in the bottom that does not use the circle box, the phenomenon that causes the pollution in the dust gets into the circle box in a large number when preventing not using satisfies the user demand.

Description

Continuous neutralization apparatus of thick sec-octanol

Technical Field

The utility model relates to a continuous neutralization equipment technical field especially relates to a thick sec-octanol continuous neutralization device.

Background

When the sebacic acid is produced by castor oil, the secondary octanol is a byproduct, is obtained by recovery, is insoluble in water, can be mixed and dissolved with organic solvents such as alcohol, ether, chloroform and the like, has low toxicity, has certain stimulation effect on skin and mucosa, and is mainly used for producing plasticizers, emulsifiers, solvents, organic synthetic raw materials and the like; the acid value of the crude secondary octanol is high, and the crude secondary octanol contains too many impurity components, so that the application of the crude secondary octanol in downstream products is influenced, and the crude secondary octanol needs to be subjected to a neutralization reaction;

in view of the above, in the prior art, no. CN212549562U discloses a continuous neutralization apparatus for crude sec-octanol, which comprises a continuous neutralization tower, wherein the upper part of the continuous neutralization tower is connected with an alkali liquor feeding pipe, and the alkali liquor feeding pipe is communicated with an alkali liquor tank; the lower part of the continuous neutralization tower is connected with a crude alcohol raw material feeding pipe which is communicated with a raw material tank; a crude alcohol discharging pipe is arranged at the upper part of the continuous neutralization tower and is communicated with the intermediate tank; a material conveying pipe and a first material returning pipe are communicated with the intermediate tank, and the material conveying pipe is communicated with the finished product tank; the first return pipe is communicated with the raw material tank; the bottom of the continuous neutralization tower is connected with an alkali liquor discharging pipe which is communicated with the separation tank; the utility model can realize the continuity of the neutralization process of the coarse sec-octanol, shorten the reaction time and improve the production efficiency; the water consumption for neutralization and washing can be reduced, the wastewater amount is reduced, and the environment is protected; the recycling of the neutralizing alkali can be realized, the utilization rate of the alkaline water is improved, the discharge amount of the waste alkaline water is reduced, and the production cost is reduced.

The continuous crude sec-octanol neutralizing device disclosed in the patent realizes continuous neutralization of crude sec-octanol, and a sampling detection port on a middle tank of the device is used for sampling and detecting the neutralized crude sec-octanol by personnel; however, the device still has some defects, the sampling detection port of the device lacks the function of automatic blocking and closing after sampling, (so that the phenomenon that the blocking and closing are forgotten after sampling due to carelessness of personnel is easily caused, and the neutralized crude sec-octanol easily flows out and is wasted in a large amount) cannot meet the use requirement, and the device is improved aiming at the problems existing in the technology, so that the device for continuously neutralizing the crude sec-octanol is provided for solving the problems.

SUMMERY OF THE UTILITY MODEL

The utility model aims at solving the defects existing in the prior art and providing a crude sec-octanol continuous neutralization device.

In order to achieve the above purpose, the utility model adopts the following technical scheme:

a continuous crude sec-octanol neutralizing device comprises a continuous neutralizing device body, wherein the continuous neutralizing device body comprises a continuous neutralizing tower and a middle tank connected with the continuous neutralizing tower, the right side of the bottom of the middle tank is communicated and fixed with a sampling detection port, and the bottom end of the sampling detection port is provided with a self-sealing sampling mechanism;

the utility model discloses a take out the sample mechanism from formula of proclaiming oneself, the mechanism includes the circle box of fixed connection in sampling test mouth bottom, the bottom of circle box sets up to the opening, set up the intercommunicating pore that is linked together with the sampling test mouth on the top inner wall of circle box, fixedly connected with and the conical cover that the intercommunicating pore is linked together on the top inner wall of circle box, the bell mouth has been seted up on the bottom inner wall of conical cover, the sealed movable sleeve that lives is equipped with in the bell mouth, the bottom fixedly connected with play appearance pipe of conical cover, the sealed slip cap of play appearance pipe is equipped with sealed extrusion drive assembly, the bottom fixedly connected with of stifled ball is located the L shape pole in appearance pipe, the left end of L shape pole extends to play appearance outside of pipe and with sealed extrusion drive assembly's left side inner wall fixed connection, sealed extrusion drive assembly is used for driving L shape pole and stifled ball rebound when receiving the extrusion, two elastic guide assembly of fixedly connected with between the top of sealed extrusion drive assembly and the top inner wall of circle box, elastic guide assembly is used for keeping out the sealed pressurization drive assembly from top and drives its rebound when relieving the extrusion, the bottom rotation of circle box is connected with and is kept out the dustproof assembly, the dustproof assembly is used for keeping out the inside keeping out the dustproof assembly of circle box.

Preferably, the sealed extrusion driving assembly comprises a blocking sleeve which is sleeved on the sample outlet pipe in a sealed sliding manner, the inner wall of the left side of the blocking sleeve is fixedly connected with the left end of the L-shaped rod, a pressing plate is fixedly sleeved on the blocking sleeve, and a sealing ring which is sleeved on the outer side of the blocking sleeve is fixedly bonded to the bottom of the pressing plate.

Preferably, the elastic guide assembly comprises a guide pipe fixedly connected to the inner wall of the top of the round box, the bottom end of the guide pipe is arranged to be a blocking structure, a T-shaped guide rod is sleeved in the guide pipe in a sliding mode, the bottom ends of the two T-shaped guide rods respectively extend to the lower portion of the corresponding guide pipe and are fixedly connected with the top of the pressing plate, springs are fixedly connected to the bottom ends of the guide pipe and the top of the pressing plate in front of the bottom ends of the guide pipe, and the springs are movably sleeved on the corresponding T-shaped guide rods.

Preferably, shelter from dustproof subassembly include with circle box bottom swing joint's apron, the top right side of apron inlays and is equipped with magnet, the bottom right side of circle box inlays and is equipped with the iron sheet, the top of magnet adsorbs with the bottom of iron sheet, the same hinge of left side bottom fixedly connected with of the left side of apron and circle box, the apron passes through the hinge and rotates the bottom of installing at the circle box.

Preferably, a rectangular through hole is formed in the inner wall of the left side of the sample outlet pipe, and the front inner wall and the rear inner wall of the rectangular through hole are respectively connected with the front side and the rear side of the L-shaped rod in a sliding manner.

Preferably, a thin sealing rubber sleeve is bonded and sleeved in the baffle sleeve, and the inner side of the thin sealing rubber sleeve is in sliding connection with the outer side of the sample outlet pipe.

Preferably, the outer side of the blocking ball is wrapped with a sealing rubber sheet, and the bottom of the outer side of the sealing rubber sheet is in close contact with the inner wall of the conical hole.

Compared with the prior art, the beneficial effects of the utility model are that:

the round box, the cover plate, the magnet and the iron sheet are matched with the hinge, so that the bottom of the round box can be blocked and plugged when not in use;

through intercommunicating pore, conical cover, bell mouth, stifled ball, play appearance pipe, spacer sleeve, L shape pole, clamp plate, sealing washer, stand pipe, T shape guide arm and spring cooperation, can sample fast through simple extruded mode, and can close at the automatic quick shutoff of sample back.

The utility model discloses be convenient for through simple extruded mode quick sampling, be convenient for close the shutoff of sample detection mouth automatically fast after the sample, can effectively avoid forgetting the shutoff due to personnel's carelessness carelessly and close the extravagant phenomenon that leads to thick octanol to flow in a large number, and be convenient for shelter from the shutoff in the bottom that does not use the circle box, the phenomenon that causes the pollution in the dust gets into the circle box in a large number when preventing not using satisfies the user demand.

Drawings

FIG. 1 is a schematic structural diagram of a continuous crude sec-octanol neutralizing device provided by the utility model;

FIG. 2 is an enlarged cross-sectional view of part A of FIG. 1;

fig. 3 is the schematic view of the three-dimensional structure of the conical cover of the continuous neutralization device for crude sec-octanol provided by the utility model.

In the figure: 100. a continuous neutralization column; 101. an intermediate tank; 102. a sampling detection port; 1. a round box; 2. a communicating hole; 3. a conical cover; 4. a tapered hole; 5. blocking the ball; 6. a sample outlet pipe; 7. a blocking sleeve; 8. an L-shaped rod; 9. a rectangular perforation; 10. pressing a plate; 11. a seal ring; 12. a guide tube; 13. a T-shaped guide rod; 14. a spring; 15. a cover plate; 16. a magnet; 17. and (5) a hinge.

Detailed Description

The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments.

Referring to fig. 1-3, a crude sec-octanol continuous neutralization device comprises a continuous neutralization device body, wherein the continuous neutralization device body comprises a continuous neutralization tower 100 and a middle tank 101 connected with the continuous neutralization tower 100, the right side of the bottom of the middle tank 101 is communicated with and fixed with a sampling detection port 102, the continuous neutralization principle of the continuous neutralization device body is the prior art disclosed by a comparison document, and a self-sealing sampling mechanism is arranged at the bottom end of the sampling detection port 102;

the self-sealing sampling mechanism comprises a round box 1 fixedly connected to the bottom end of a sampling detection port 102, the bottom of the round box 1 is provided with an opening, a communication hole 2 communicated with the sampling detection port 102 is formed in the inner wall of the top of the round box 1, a conical cover 3 communicated with the communication hole 2 is fixedly connected to the inner wall of the top of the round box 1, a conical hole 4 is formed in the inner wall of the bottom of the conical cover 3, a plugging ball 5 is movably sleeved in the conical hole 4 in a sealing mode, a sealing rubber sheet is wrapped on the outer side of the plugging ball 5, the bottom of the outer side of the sealing rubber sheet is in close contact with the inner wall of the conical hole 4, the plugging ball 5 plugs the conical hole 4 through the sealing rubber sheet on the outer side of the plugging ball, a sample outlet pipe 6 is fixedly connected to the bottom of the conical cover 3, a sealing extrusion driving assembly is sleeved on the sample outlet pipe 6 in a sliding mode, an L-shaped rod 8 positioned in the sample outlet pipe 6 is fixedly connected to the bottom of the plugging ball 5, the left end of the L-shaped rod 8 extends out of the sample outlet pipe 6 and is fixedly connected to the left side of the sealing extrusion driving assembly, the inner wall of the left side of the sample outlet pipe 6 is provided with a rectangular perforation 9, the inner wall of the front side and the inner wall of the rear side of the rectangular perforation 9 are respectively connected with the front side and the rear side of the L-shaped rod 8 in a sliding manner, so that the L-shaped rod 8 can penetrate through the rectangular perforation 9, the sealing extrusion driving assembly is used for driving the L-shaped rod 8 and the ball stopper 5 to move upwards when being extruded, the sealing extrusion driving assembly comprises a baffle sleeve 7 which is sleeved on the sample outlet pipe 6 in a sealing sliding manner, the rectangular perforation 9 is positioned in the baffle sleeve 7, a thin sealing rubber sleeve is sleeved in the baffle sleeve 7 in a bonding manner, the inner side of the thin sealing rubber sleeve is connected with the outer side of the sample outlet pipe 6 in a sliding manner, the inner wall of the left side of the baffle sleeve 7 is fixedly connected with the left end of the L-shaped rod 8, a pressing plate 10 is fixedly sleeved on the baffle sleeve 7, the top of the pressing plate 10 is provided with a round hole, the inner wall of the round hole is fixedly bonded with the outer side of the baffle sleeve 7, the pressing plate 10 is fixedly sleeved on the blocking sleeve 7 through a circular hole, and a sealing ring 11 sleeved on the outer side of the blocking sleeve 7 is fixedly bonded at the bottom of the pressing plate 10;

two elastic guide assemblies are fixedly connected between the top of the pressure plate 10 and the inner wall of the top of the round box 1, the elastic guide assemblies are used for guiding the pressure plate 10 up and down and driving the pressure plate to move back downwards when the extrusion is removed, wherein each elastic guide assembly comprises a guide pipe 12 fixedly connected to the inner wall of the top of the round box 1, the bottom end of each guide pipe 12 is of a plugging structure, a T-shaped guide rod 13 is slidably sleeved in each guide pipe 12, the bottom ends of the two T-shaped guide rods 13 respectively extend to the lower part of the corresponding guide pipe 12 and are fixedly connected with the top of the pressure plate 10, guide through holes are formed in the inner wall of the bottom end of each guide pipe 12, the inner wall of each guide through hole is slidably connected with the outer side of the corresponding T-shaped guide rod 13, each guide pipe 12 is slidably sleeved on the corresponding T-shaped guide rod 13 through the guide through holes, the conical cover 3, the conical hole 4, the plugging ball 5, the sample outlet pipe 6, the baffle sleeve 7, the L-shaped guide rod 8, the L-shaped guide rod 10, the pressure plate 12 can be movably sleeved on the corresponding T-shaped guide rod 13 in a simple and can be quickly extruded and can be rapidly plugged by the sampling guide through the simple and rapid plugging guide through the simple and rapid sampling guide through the simple and rapid extrusion mode of the guide pipe 13;

the bottom of the round box 1 is rotatably connected with a shielding dustproof component which is used for shielding and preventing dust inside the round box 1, wherein the shielding dustproof component comprises a cover plate 15 which is movably contacted with the bottom of the round box 1, the right side of the top of the cover plate 15 is embedded with a magnet 16, the right side of the top of the cover plate 15 is provided with a first embedded groove which is fixedly bonded with the outer side of the magnet 16, the magnet 16 is fixedly embedded at the right side of the top of the cover plate 15 through the first embedded groove, the right side of the bottom of the round box 1 is fixedly embedded with an iron sheet, the right side of the bottom of the round box 1 is provided with a second embedded groove which is fixedly bonded with the outer side of the iron sheet, the iron sheet is fixedly embedded at the right side of the bottom of the round box 1 through the second embedded groove, and the top of the magnet 16 is adsorbed with the bottom of the iron sheet, the left side of apron 15 and the same hinge 17 of left side bottom fixedly connected with of circle box 1, apron 15 rotates through hinge 17 and installs in the bottom of circle box 1, through circle box 1, apron 15, magnet 16, iron sheet and hinge 17 cooperate, can shelter from the shutoff to the bottom of circle box 1 when not using, the utility model discloses be convenient for through the quick sample of simple extruded mode, be convenient for automatic quick after the sample to the shutoff of sample detection mouth 102 close, can effectively avoid forgetting the shutoff because of personnel's carelessness and close the extravagant phenomenon that leads to thick major outflow of octanol, and be convenient for shelter from the shutoff in the bottom of circle box 1 of not using, the phenomenon that causes the pollution in a large number of entering circle box 1 of dust when preventing not using satisfies the user demand.

The working principle is as follows: the cover plate 15 can shield the bottom of the round box 1 for dust prevention, so that the phenomenon of pollution caused by a large amount of dust entering the round box 1 when the round box is not used is reduced, when sampling detection is needed, a person firstly rotates the cover plate 15 downwards, the cover plate 15 rotates downwards through the hinge 17 to be turned, and drives the magnet 16 to be separated from the iron sheet, so that shielding is removed;

at the moment, a person inserts an external sampling bottle into the round box 1, the external sampling bottle is utilized to upwards press the sealing ring 11, so that the sealing ring 11 upwards moves and drives the pressing plate 10 to upwards move, the pressing plate 10 drives the two T-shaped guide rods 13 to upwards slide in the corresponding guide pipes 12 respectively and compress the two springs 14, the pressing plate 10 drives the blocking sleeve 7 to upwards slide on the sample outlet pipe 6, the blocking sleeve 7 drives the blocking ball 5 to upwards separate from the conical hole 4 through the L-shaped rod 8, the blocking is released, at the moment, crude octanol downwards sequentially enters the conical cover 3 through the sampling detection port 102 and the communicating hole 2 and then downwards sequentially enters the external sampling bottle through the conical hole 4 and the sample outlet pipe 6, so that the crude octanol can be rapidly sampled by simple extrusion, after the sampling is completed, the crude octanol is downwards moved out of the external sampling bottle, at the moment, the elastic force of the two springs 14 in a compressed state drives the pressing plate 10 to downwards move back, the pressing plate 10 drives the blocking sleeve 7 to downwards move back, the blocking sleeve 7 drives the blocking ball 5 to downwards move back to the conical hole 4 through the L-shaped rod 8, the blocking ball 5 blocks the conical hole 4, the coarse octanol cannot be automatically blocked, the secondary octanol continuously closed, the crude octanol cannot be automatically closed by a large-scale sampling, and the secondary octanol cannot be automatically closed by an automatic blockage after the secondary sampling, the secondary octanol is effectively closed;

the apron 15 is closed to the last gyration of completion back of taking a sample, and apron 15 drives magnet 16 and adsorbs mutually with the iron sheet once more, and apron 15 shelters from the shutoff to the bottom of circle box 1 once more this moment, and the phenomenon that causes the pollution in the dust gets into in a large number the circle box 1 when preventing not using.

In the description of the present application, it should be further noted that, unless otherwise explicitly stated or limited, the terms "disposed," "mounted," "connected," and "connected" are to be construed broadly and may include, for example, a fixed connection, a detachable connection, an integral connection, a mechanical connection, an electrical connection, a direct connection, a connection through an intermediate medium, and a connection between two elements. The specific meaning of the above terms in the present application can be understood by those of ordinary skill in the art according to specific circumstances.

The above, only be the embodiment of the preferred of the present invention, but the protection scope of the present invention is not limited thereto, and any person skilled in the art is in the technical scope of the present invention, according to the technical solution of the present invention and the utility model, which are designed to be replaced or changed equally, all should be covered within the protection scope of the present invention.

Claims

1. A continuous crude sec-octanol neutralizing device comprises a continuous neutralizing device body, wherein the continuous neutralizing device body comprises a continuous neutralizing tower (100) and a middle tank (101) connected with the continuous neutralizing tower (100), the right side of the bottom of the middle tank (101) is communicated and fixed with a sampling detection port (102), and the continuous neutralizing device is characterized in that the bottom end of the sampling detection port (102) is provided with a self-sealing sampling mechanism;

the utility model discloses a take out the sample mechanism and seal extrusion drive assembly's left side inner wall fixed connection, the self-sealing type sampling mechanism includes circle box (1) of fixed connection in sample detection mouth (102) bottom, the bottom of circle box (1) sets up to the opening, intercommunication hole (2) that are linked together with sample detection mouth (102) are seted up on the top inner wall of circle box (1), fixedly connected with conical cover (3) that are linked together with intercommunication hole (2) on the top inner wall of circle box (1), bell mouth (4) have been seted up on the bottom inner wall of conical cover (3), bell mouth (4) inner seal movable sleeve is equipped with stifled ball (5), the bottom fixedly connected with of conical cover (3) goes out appearance pipe (6), go out the sealed sliding sleeve of appearance pipe (6) and be equipped with sealed extrusion drive assembly, the bottom fixedly connected with two elastic guide assemblies of fixedly connected with between the top of sealed extrusion drive assembly and the top inner wall of circle box (1), the bottom of rotation box (1) is connected with the subassembly that shelters from dust.

2. The continuous neutralizing device for the crude sec-octanol according to claim 1, wherein the sealing extrusion driving assembly comprises a blocking sleeve (7) which is sleeved on the sample outlet pipe (6) in a sealing sliding manner, the left inner wall of the blocking sleeve (7) is fixedly connected with the left end of the L-shaped rod (8), a pressing plate (10) is fixedly sleeved on the blocking sleeve (7), and a sealing ring (11) which is sleeved on the outer side of the blocking sleeve (7) is fixedly bonded to the bottom of the pressing plate (10).

3. The continuous neutralizing device for the crude sec-octanol according to claim 2, wherein the elastic guide assembly comprises a guide tube (12) fixedly connected to the inner wall of the top of the round box (1), the bottom end of the guide tube (12) is provided with a blocking structure, a T-shaped guide rod (13) is slidably sleeved in the guide tube (12), the bottom ends of the two T-shaped guide rods (13) respectively extend to the lower part of the corresponding guide tube (12) and are fixedly connected with the top of the pressing plate (10), a spring (14) is fixedly connected between the bottom end of the guide tube (12) and the top of the pressing plate (10), and the spring (14) is movably sleeved on the corresponding T-shaped guide rod (13).

4. The continuous neutralizing device for the crude sec-octanol according to claim 1, wherein the shielding dustproof component comprises a cover plate (15) movably contacted with the bottom of the round box (1), a magnet (16) is embedded on the right side of the top of the cover plate (15), an iron sheet is embedded and fixed on the right side of the bottom of the round box (1), the top of the magnet (16) is adsorbed with the bottom of the iron sheet, the same hinge (17) is fixedly connected on the left side of the cover plate (15) and the bottom of the left side of the round box (1), and the cover plate (15) is rotatably installed on the bottom of the round box (1) through the hinge (17).

5. The continuous neutralizing device for crude sec-octanol according to claim 1, wherein the sample outlet pipe (6) has a rectangular through hole (9) in its left inner wall, and the front inner wall and the rear inner wall of the rectangular through hole (9) are slidably connected to the front and the rear sides of the L-shaped bar (8), respectively.

6. The continuous neutralizing device for crude sec-octanol according to claim 2, wherein the spacer (7) is internally glued with a thin sealing rubber sleeve, and the inner side of the thin sealing rubber sleeve is slidably connected with the outer side of the sample outlet pipe (6).

7. The continuous neutralization apparatus according to claim 1, wherein the outer side of the ball plug (5) is covered with a rubber sheet, and the outer bottom of the rubber sheet is in close contact with the inner wall of the tapered hole (4).