CN218188210U - Device for synthesizing 2,5-dimethyl-2,5-dihydrohexane peroxide - Google Patents
Device for synthesizing 2,5-dimethyl-2,5-dihydrohexane peroxide Download PDFInfo
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- CN218188210U CN218188210U CN202222174565.4U CN202222174565U CN218188210U CN 218188210 U CN218188210 U CN 218188210U CN 202222174565 U CN202222174565 U CN 202222174565U CN 218188210 U CN218188210 U CN 218188210U
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Abstract
The application relates to the technical field of 2,5-dimethyl-2,5-dihydrohexane peroxide synthesis, and discloses a device for synthesizing 2,5-dimethyl-2,5-dihydrohexane peroxide, which comprises a reaction device, wherein a suction filtration device is arranged at the bottom of the reaction device, a base is fixedly connected to the bottom of the suction filtration device, and a scraping structure is arranged inside the reaction device. This equipment of synthetic 2,5-dimethyl-2,5-hydrogen peroxide hexane makes the lifter plate move down in the reaction equipment through the cooperation of square piece internal cylinder and piston rod, then moves connecting rod and scraper blade of one side through the lifter plate and moves down for scrape the solid particle that adsorbs to the reaction equipment inner wall in the scraper blade motion process and get, and then make the solid particle clearance of reaction equipment inner wall adsorption save time and laborsaving, be convenient for the staff with the help of reaction equipment to 2,5-dimethyl-2,5-hydrogen peroxide hexane carry out next synthetic use, reach the convenient effect of reaction equipment inner wall adsorption solid particle clearance.
Description
Technical Field
The application relates to the technical field of 2,5-dimethyl-2,5-dihydrohexane peroxide synthesis, in particular to equipment for synthesizing 2,5-dimethyl-2,5-dihydrohexane peroxide.
Background
The organic peroxide is a cross-linking agent with wide application, 2,5-dimethyl 2,5-dihexyl, and the abbreviation of bis-di-five is an organic peroxide with wide application and high cross-linking efficiency.
In the synthesis process of 2,5-dimethyl-2,5-dihydrohexane peroxide, an operator completes the peroxide of 2,5-dimethyl-2,5-hexanediol through reaction equipment to generate 2,5-dimethyl-2,5-dihydrohexane peroxide, then the solid-liquid mixture enters suction filtration equipment through a conveying pipe and is subjected to solid-liquid separation, and 2,5-dimethyl-2,5-dihydrohexane peroxide is further obtained, however, when the solid-liquid mixture of 2,5-dimethyl-2,5-dihydrohexane peroxide enters the suction filtration equipment, part of 2,5-dimethyl-2,5-dihydrohexane peroxide may be adsorbed on the inner wall of the reaction equipment, and the reaction equipment is closed equipment, so that the solid particles adsorbed on the inner wall of the reaction equipment are relatively clean, and the synthesis of 9843 zxft 3524-dimethyl-3524-dihydrohexane is inconvenient.
SUMMERY OF THE UTILITY MODEL
Aiming at the defects of the prior art, the application provides equipment for synthesizing 2,5-dimethyl-2,5-dihydrohexane peroxide, which has the advantage of convenience in cleaning solid particles adsorbed on the inner wall of reaction equipment and solves the problem of inconvenience in cleaning solid particles adsorbed on the inner wall of the reaction equipment in the background technology.
In order to achieve the above purpose, the present application provides the following technical solutions: the equipment for synthesizing 2,5-dimethyl-2,5-dihydroperoxide hexane comprises reaction equipment, wherein suction filtration equipment is arranged at the bottom of the reaction equipment, a base is fixedly connected to the bottom of the suction filtration equipment, and a scraping structure is arranged in the reaction equipment;
the scraping structure comprises a square block, an air cylinder, a piston rod, a lifting plate, a connecting rod and a scraper, wherein the square block is fixed at the top of the reaction equipment, the air cylinder is arranged inside the square block, the air cylinder output end is fixedly connected with the top end of the piston rod, the lifting plate is arranged on the inner top wall of the reaction equipment, the piston rod extends to the bottom end of the reaction equipment and is fixedly connected with the top end of the lifting plate, the outer wall of one side of the lifting plate is fixedly connected with one end of the connecting rod, and the outer wall of the other side of the connecting rod is fixedly connected with one side of the scraper.
Preferably, the reaction equipment surface is provided with two sets of feed inlets that are the symmetric distribution, the reaction equipment bottom is provided with two conveying pipelines that are the symmetric distribution, the conveying pipeline bottom extends to inside the suction filtration equipment, conveying pipeline one side is provided with the discharge valve, suction filtration equipment one side bottom is provided with the drain pipe, the drain pipe top is provided with the valve.
Preferably, the top of the base is fixed with two groups of vertical rods which are symmetrically distributed, two fixed plates which are linearly distributed are fixed on the outer surface of the reaction equipment, and the outer walls of the vertical rods are fixedly connected with the inner walls of the fixed plates.
Through the cooperation of montant and fixed plate, play fixed effect to reaction equipment, make reaction equipment more stable at suction filtration equipment top.
Preferably, the inner wall of one side of the suction filtration equipment is fixed with filter cloth, one side of the top of the base is provided with a vacuum pump, one side of the vacuum pump is provided with an air exhaust pipeline, and the other end of the air exhaust pipeline extends into the suction filtration equipment.
Preferably, the discharge opening has been seted up to suction filtration equipment one side, the inside dog that is provided with of discharge opening, the dog outer wall is fixed with the sealing washer, sealing washer outer wall and discharge opening inner wall swing joint, the dog extends suction filtration equipment outer wall fixedly connected with and draws the piece, suction filtration equipment is inside, be located the filter cloth top and be provided with the collecting plate, collecting plate one side outer wall is fixed with a plurality of and is the pull rod of linear distribution, the pull rod is kept away from collecting plate one end and dog one side outer wall fixed connection.
The pull rod and the collecting plate at the top of the filter cloth are driven to move rightwards by the stop block, so that the collecting plate drives solid particles at the top of the filter cloth to move rightwards in the moving process, and the solid particles are convenient to collect by workers through the discharge holes.
Compared with the prior art, the application provides a synthetic 2,5-dimethyl-2,5-hydrogen peroxide hexane's equipment, has following beneficial effect:
1. the device for synthesizing 2,5-dimethyl-2,5-dihydroperoxide hexane is provided with a scraping structure, and particularly, when solid particles adsorbed on the inner wall of reaction equipment need to be cleaned, the lifting plate moves downwards in the reaction equipment through the matching of the cylinder in the square block and the piston rod, and then the connecting rod and the scraper on one side driven by the lifting plate move downwards, so that the solid particles adsorbed on the inner wall of the reaction equipment are scraped in the movement process of the scraper, time and labor are saved for cleaning the solid particles adsorbed on the inner wall of the reaction equipment, workers can conveniently perform next synthesis and use on 2,5-dimethyl-2,5-dihydroperoxide hexane by means of the reaction equipment, and the effect of convenient cleaning of the solid particles adsorbed on the inner wall of the reaction equipment is achieved.
2. This equipment of synthetic 2,5-dimethyl-2,5-hydrogen peroxide hexane, through being provided with the collecting plate, when the solid particles after the suction filtration need be collected, after the solid-liquid mixture passes through suction filtration equipment suction filtration, the solid particles are piled up at the filter cloth top, then the pulling block of pulling dog one side moves right, and then drive the pull rod at filter cloth top and collect the board through the dog and move right, make the solid particles that the collecting plate motion process drove the filter cloth top move right, and be convenient for the staff to the collection of solid particles through the discharge opening, reach the effect of being convenient for collecting the solid particles after the suction filtration.
Drawings
FIG. 1 is a schematic diagram of the overall structure of the present application;
FIG. 2 is an enlarged view taken at A in FIG. 1 of the present application;
FIG. 3 is a perspective view of the structure of the present application;
FIG. 4 is a schematic diagram of a collection plate structure according to the present application;
fig. 5 is a schematic diagram of a lift plate structure according to the present application.
Wherein: 1. reaction equipment; 101. a square block; 102. a cylinder; 103. a piston rod; 104. a lifting plate; 105. a connecting rod; 106. a squeegee; 107. a feed inlet; 108. a delivery pipe; 109. a discharge valve; 110. a fixing plate; 2. suction filtration equipment; 201. a liquid outlet pipe; 202. a valve; 203. filtering cloth; 204. a discharge hole; 205. a stopper; 206. a seal ring; 207. pulling the block; 208. a collection plate; 209. a pull rod; 3. a base; 301. a vertical rod; 302. a vacuum pump; 303. an air exhaust pipeline.
Detailed Description
The present application is described in further detail below with reference to figures 1-5.
The embodiment of the application discloses a device for synthesizing 2,5-dimethyl-2,5-dihydrohexane peroxide.
Referring to fig. 1, 3 and 5, a device for synthesizing 2,5-dimethyl-2,5-dihydrohexane peroxide comprises a reaction device 1, wherein a suction filtration device 2 is arranged at the bottom of the reaction device 1, a base 3 is fixedly connected to the bottom of the suction filtration device 2, a scraping structure is arranged inside the reaction device 1, and comprises a square block 101, an air cylinder 102, a piston rod 103, a lifting plate 104, a connecting rod 105 and a scraper 106, the lifting plate 104 moves downwards inside the reaction device 1 through the matching of the air cylinder 102 and the piston rod 103 in the square block 101, and then the connecting rod 105 and the scraper 106 on one side are driven by the lifting plate 104 to move downwards, so that solid particles adsorbed on the inner wall of the reaction device 1 are scraped in the movement process of the scraper 106, and further the solid particles adsorbed on the inner wall of the reaction device 1 are cleaned in a time-saving and labor-saving manner, and a worker can conveniently synthesize 2,5-dimethyl-2,5-dihydrohexane peroxide by means of the reaction device 1 for the next time.
Referring to fig. 1 and 3, the outer surface of reaction equipment 1 is provided with two sets of feed inlets 107 that are symmetric distribution, reaction equipment 1 bottom is provided with two conveying pipelines 108 that are symmetric distribution, conveying pipeline 108 bottom extends to inside suction filtration equipment 2, conveying pipeline 108 one side is provided with discharge valve 109, 2 one side bottoms of suction filtration equipment are provided with drain pipe 201, drain pipe 201 top is provided with valve 202, can pour reactant and water into reaction equipment 1 inside through two sets of feed inlets 107, and after the reaction, open discharge valve 109, make the solid-liquid mixture in reaction equipment 1 get into inside suction filtration equipment 2, after the suction filtration is accomplished, open valve 202, can discharge liquid from suction filtration equipment 2.
Referring to fig. 1 and 3, the top of the base 3 is fixed with two sets of montants 301 that are the symmetric distribution, and the external surface of the reaction equipment 1 is fixed with two fixed plates 110 that are the linear distribution, and montant 301 outer wall and fixed plate 110 inner wall fixed connection play fixed effect to the reaction equipment 1 through the cooperation of montant 301 and fixed plate 110, make the reaction equipment 1 more stable at the 2 tops of suction filtration equipment.
Referring to fig. 1, a filter cloth 203 is fixed on the inner wall of one side of a suction filtration device 2, a vacuum pump 302 is arranged on one side of the top of a base 3, an air extraction pipeline 303 is arranged on one side of the vacuum pump 302, the other end of the air extraction pipeline 303 extends into the suction filtration device 2, the height of the water surface of the solid-liquid mixture in the suction filtration device 2 is not higher than that of the air extraction pipeline 303, air in the suction filtration device 2 is extracted by the vacuum pump 302 and discharged through the air extraction pipeline 303, the pressure in the suction filtration device 2 is reduced, and then the solid-liquid mixture can be subjected to solid-liquid separation, so that solid particles are accumulated on the top of the filter cloth 203.
Referring to fig. 1, fig. 2 and fig. 4, a discharge hole 204 has been seted up on one side of the suction filtration device 2, a stopper 205 is provided inside the discharge hole 204, a sealing ring 206 is fixed on the outer wall of the stopper 205, the outer wall of the sealing ring 206 is movably connected with the inner wall of the discharge hole 204, the stopper 205 extends out of a pull block 207 fixedly connected with the outer wall of the suction filtration device 2, a collection plate 208 is provided inside the suction filtration device 2 and located at the top of the filter cloth 203, a plurality of pull rods 209 which are linearly distributed are fixed on the outer wall of one side of the collection plate 208, one end of the pull rod 209 away from the collection plate 208 is fixedly connected with the outer wall of one side of the stopper 205, after the solid-liquid mixture is suction filtered by the suction filtration device 2, the solid particles are accumulated at the top of the filter cloth 203, then the pull block 207 on one side of the stopper 205 is pulled to move rightwards, and then the pull rod 209 and the collection plate 208 at the top of the filter cloth 203 are driven to move rightwards by the stopper 205, so that the solid particles at the top of the collection plate 203 are driven by the movement process of the collection plate 208, and the staff can collect the solid particles conveniently by the discharge hole 204.
The implementation principle of the device for synthesizing 2,5-dimethyl-2,5-dihydrohexane peroxide in the embodiment of the application is as follows: when solid particles adsorbed on the inner wall of the reaction equipment 1 need to be cleaned, the lifting plate 104 moves downwards in the reaction equipment 1 through the matching of the cylinder 102 and the piston rod 103 in the square block 101, and then the lifting plate 104 drives the connecting rod 105 and the scraper 106 on one side to move downwards, so that the solid particles adsorbed on the inner wall of the reaction equipment 1 are scraped during the movement process of the scraper 106, and further the cleaning of the solid particles adsorbed on the inner wall of the reaction equipment 1 is time-saving and labor-saving, and workers can conveniently perform next synthesis and use on 2,5-dimethyl-2,5-dihydrohexane peroxide by means of the reaction equipment 1.
The utility model discloses the standard part that uses all can purchase from the market, dysmorphism piece all can be customized according to the description with the record of attached drawing in the specification, the concrete connection mode of each part all adopts conventional means such as ripe bolt, rivet, welding among the prior art, machinery, part and equipment all adopt among the prior art, conventional model, including the conventional connection mode among the circuit connection adoption prior art, no detailed description here again, and the part that technical staff in the field knows, its structure and principle all can learn or learn through conventional experimental approach for this technical staff's accessible technical manual.
Although embodiments of the present application have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the application, the scope of which is defined in the appended claims and their equivalents.
Claims (5)
1. An apparatus for synthesizing 2,5-dimethyl-2,5-dihydrohexane peroxide, comprising a reaction apparatus (1), characterized in that: the bottom of the reaction equipment (1) is provided with suction filtration equipment (2), the bottom of the suction filtration equipment (2) is fixedly connected with a base (3), and a scraping structure is arranged in the reaction equipment (1);
the scraping structure comprises a square block (101), a cylinder (102), a piston rod (103), a lifting plate (104), a connecting rod (105) and a scraper (106), the square block (101) is fixed at the top of the reaction equipment (1), the cylinder (102) is arranged inside the square block (101), the output end of the cylinder (102) is fixedly connected with the top end of the piston rod (103), the lifting plate (104) is arranged on the inner top wall of the reaction equipment (1), the piston rod (103) extends to the bottom end of the reaction equipment (1) and the top of the lifting plate (104), the outer wall of one side of the lifting plate (104) is fixedly connected with one end of the connecting rod (105), and the other end of the connecting rod (105) is fixedly connected with the outer wall of one side of the scraper (106).
2. The apparatus of claim 1, wherein the apparatus comprises 2,5-dimethyl-2,5-dihydrohexane peroxide, and wherein: reaction unit (1) surface is provided with two sets of feed inlets (107) that are the symmetric distribution, reaction unit (1) bottom is provided with two conveying pipeline (108) that are the symmetric distribution, inside conveying pipeline (108) bottom extended to suction filtration equipment (2), conveying pipeline (108) one side is provided with discharge valve (109), suction filtration equipment (2) one side bottom is provided with drain pipe (201), drain pipe (201) top is provided with valve (202).
3. The apparatus of claim 1, wherein the apparatus comprises 2,5-dimethyl-2,5-dihydrohexane peroxide, and wherein: the reactor is characterized in that two groups of vertical rods (301) which are symmetrically distributed are fixed at the top of the base (3), two fixing plates (110) which are linearly distributed are fixed on the outer surface of the reaction equipment (1), and the outer walls of the vertical rods (301) are fixedly connected with the inner walls of the fixing plates (110).
4. The apparatus of claim 1, wherein the apparatus comprises 2,5-dimethyl-2,5-dihydrohexane peroxide, and wherein: the filter cloth (203) is fixed on the inner wall of one side of the suction filtration equipment (2), a vacuum pump (302) is arranged on one side of the top of the base (3), an air suction pipeline (303) is arranged on one side of the vacuum pump (302), and the other end of the air suction pipeline (303) extends to the inside of the suction filtration equipment (2).
5. The apparatus of claim 4 for synthesizing 2,5-dimethyl-2,5-dihydroperoxide hexane, wherein: discharge opening (204) have been seted up to suction filtration equipment (2) one side, inside dog (205) that is provided with of discharge opening (204), dog (205) outer wall is fixed with sealing washer (206), sealing washer (206) outer wall and discharge opening (204) inner wall swing joint, dog (205) extend suction filtration equipment (2) outer wall fixedly connected with and draw piece (207), inside, the filter cloth (203) top that is located suction filtration equipment (2) is provided with collecting plate (208), collecting plate (208) one side outer wall is fixed with pull rod (209) that a plurality of is linear distribution, collecting plate (208) one end and dog (205) one side outer wall fixed connection are kept away from in pull rod (209).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202222174565.4U CN218188210U (en) | 2022-08-18 | 2022-08-18 | Device for synthesizing 2,5-dimethyl-2,5-dihydrohexane peroxide |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202222174565.4U CN218188210U (en) | 2022-08-18 | 2022-08-18 | Device for synthesizing 2,5-dimethyl-2,5-dihydrohexane peroxide |
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| Publication Number | Publication Date |
|---|---|
| CN218188210U true CN218188210U (en) | 2023-01-03 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202222174565.4U Active CN218188210U (en) | 2022-08-18 | 2022-08-18 | Device for synthesizing 2,5-dimethyl-2,5-dihydrohexane peroxide |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN218188210U (en) |
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- 2022-08-18 CN CN202222174565.4U patent/CN218188210U/en active Active
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Address after: 730311 No. 778, west section of Huaihe Avenue, xixiaochuan village, Qinchuan Town, Lanzhou New Area, Yongdeng County, Lanzhou City, Gansu Province Patentee after: Lanzhou Auxiliary Factory Co.,Ltd. Address before: 730311 No. 778, west section of Huaihe Avenue, xixiaochuan village, Qinchuan Town, Lanzhou New Area, Yongdeng County, Lanzhou City, Gansu Province Patentee before: Lanzhou Auxiliary Factory Co.,Ltd. |
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| CP01 | Change in the name or title of a patent holder |