CN216537005U

CN216537005U - 3, 5-di-tert-butyl salicylic acid secondary extraction equipment

Info

Publication number: CN216537005U
Application number: CN202220031446.0U
Authority: CN
Inventors: 乔斌; 刘多娇; 潘玉福; 胡玉柱; 成勇
Original assignee: Shandong Yanggu Liya New Material Co ltd
Current assignee: Shandong Yanggu Liya New Material Co ltd
Priority date: 2022-01-07
Filing date: 2022-01-07
Publication date: 2022-05-17
Anticipated expiration: 2032-01-07

Abstract

The utility model discloses a secondary 3, 5-di-tert-butyl salicylic acid extraction device which comprises a containing tank, wherein the containing tank is connected with a first liquid outlet at the bottom end of a base body through a connecting pipeline, the top end of the base body is provided with a containing tank for storing an extracting agent, the output end of a motor is fixedly connected with a tooth block, the outer side of the tooth block is connected with a gear, a gear shaft is connected to the inner side of the top end of the base body, the outer surface of the shaft end of the gear is provided with a torsion spring, the outer end of the gear is provided with a through hole, the position of the through hole corresponds to the output end of a liquid storage bottle, and the inner end of the base body is provided with a stirring blade. This 3, 5-ditert-butyl salicylic acid secondary extraction equipment is provided with tooth piece and gear, drives the tooth piece through the motor output end and rotates for the tooth piece meshes the transmission with the gear, because only part has the tooth structure in tooth piece outer end, makes gear inner through-hole and stock solution bottle output end intermittent type nature correspond the intercommunication and carry out the unloading, makes even and the former solution contact of extractant in the stock solution bottle.

Description

3, 5-di-tert-butyl salicylic acid secondary extraction equipment

Technical Field

The utility model relates to the technical field of salicylic acid extraction, in particular to secondary 3, 5-di-tert-butyl salicylic acid extraction equipment.

Background

In the production process of 3, 5-di-tert-butyl salicylic acid, the raw solution is extracted by an extractant to prepare the 3, 5-di-tert-butyl salicylic acid, but the existing extraction equipment has certain defects, such as the following defects;

when traditional extraction equipment is using, the solute mixing effect is relatively poor in extractant and former solution in production efficiency angle and the device, can not carry out abundant contact for former solution can not obtain make full use of, and the waste of the raw materials that causes has also reduced the output of salicylic acid, and can produce the residue in traditional extraction equipment after the extraction to and the liquid outlet is easily caused to the residue at play liquid in-process.

Aiming at the problems, innovative design is urgently needed on the basis of the original extraction equipment.

SUMMERY OF THE UTILITY MODEL

The utility model aims to provide secondary extraction equipment for 3, 5-di-tert-butyl salicylic acid, which solves the problems that when the traditional extraction equipment provided in the background art is used, the production efficiency is high, the mixing effect of an extracting agent in the device and a solute in an original solution is poor, the extraction agent cannot be in full contact with the solute in the original solution, the original solution cannot be fully utilized, the raw material waste is caused, the yield of the salicylic acid is reduced, and in the traditional extraction equipment, the original solution can generate residues after extraction, and the residues can easily block a liquid outlet in the liquid outlet process.

In order to achieve the purpose, the utility model provides the following technical scheme: a secondary extraction device for 3, 5-di-tert-butyl salicylic acid comprises a base body, an observation window, a liquid inlet, a first liquid outlet and a second liquid outlet, wherein the observation window is formed in the outer end of the base body, the liquid inlet is formed in the top end of the base body, and the first liquid outlet and the second liquid outlet are formed in the bottom end of the base body;

further comprising:

the containing tank is connected with the first liquid outlet at the bottom end of the base body through a connecting pipeline, the containing tank for storing the extracting agent is arranged at the top end of the base body, a liquid storage bottle and a motor are arranged at the top end of the base body, a tooth block is fixedly connected to the output end of the motor, the outer side of the tooth block is connected with a gear, a gear shaft is connected to the inner side of the top end of the base body, a torsion spring is arranged on the outer surface of the shaft end of the gear, a through hole is formed in the outer end of the gear, meanwhile, the position of the through hole corresponds to that of the output end of the liquid storage bottle, and a stirring blade is arranged at the inner end of the base body;

the installation piece, fixed mounting in the bottom of base member, and the installation piece inner end is provided with the runner to the output fixed connection of runner and motor, the guide way has been seted up to the surface of runner simultaneously, the outside of guide way is connected with the guiding axle, and the guiding axle is connected with the installation piece through the spread groove, the bottom of base member is provided with the filter screen, and the inboard and the guiding axle fixed connection of filter screen.

Preferably, the outer surface of the gear block is only partially provided with a toothed structure, the gear block is in meshed connection with the gear, the gear is in rotary connection with the top end of the base body, and the gear is in meshed connection with the gear through the toothed structure of the gear block, so that the gear intermittently rotates.

Preferably, the gear passes through torsion spring and constitutes elastic construction with the base member top, and the through-hole has been seted up to the gear outer end to the position and the corresponding intercommunication of stock solution bottle output of through-hole, the intermittent type nature through the gear rotates and makes extractant carry out even drippage in the stock solution bottle, makes extractant and former solution fully contact.

Preferably, the mounting blocks are symmetrically distributed and mounted about the central line of the base body, the mounting blocks are connected with the rotating wheel in a clamping manner, the rotating wheel is fixedly mounted at the bottom end of the output end of the motor, and the position of the rotating wheel is fixed through the mounting blocks.

Preferably, the outer surface of the rotating wheel is provided with a guide groove, the guide groove is connected with the guide shaft in a clamping manner, the front view of the guide groove is of an inclined structure, and the guide shaft is driven by the inclined guide groove to reciprocate.

Preferably, the guiding axle is provided with two sets ofly about runner central line symmetric distribution, and the guiding axle passes through the spread groove and constitutes sliding construction with the installation piece to guiding axle fixed mounting blocks the residue through the filter screen in the inboard of filter screen, avoids the residue to block up the liquid outlet.

Compared with the prior art, the utility model has the beneficial effects that: the secondary extraction equipment of the 3, 5-di-tert-butyl salicylic acid;

1. the extraction solution storage bottle is provided with a gear block and a gear, the gear block is driven to rotate through the output end of a motor, so that the gear block and the gear are in meshing transmission, and the through hole in the inner end of the gear is intermittently and correspondingly communicated with the output end of the liquid storage bottle for blanking due to the fact that only part of the outer end of the gear block is of a toothed structure, so that an extraction solution in the liquid storage bottle is uniformly contacted with an original solution;

2. be provided with runner and guide way, drive the runner through the motor output and rotate in the installation piece for the guide way drives the guiding axle and removes, and the guiding axle is installed in the filter screen the inner, drives the filter screen and vibrates and avoid the residue to block up the filter screen, and the filter screen also blocks the residue simultaneously, avoids the residue to get into the liquid outlet.

Drawings

FIG. 1 is a schematic view of the overall front view structure of the present invention;

FIG. 2 is a schematic cross-sectional structural view of a substrate according to the present invention;

FIG. 3 is a schematic top view of the tooth block of the present invention;

FIG. 4 is an enlarged view of the structure at A in FIG. 2 according to the present invention;

FIG. 5 is a perspective view of the wheel of the present invention.

In the figure: 1. a substrate; 2. an observation window; 3. a liquid inlet; 4. a first liquid outlet; 5. a second liquid outlet; 6. an accommodating tank; 7. a liquid storage bottle; 8. a motor; 9. a tooth block; 10. a gear; 11. a torsion spring; 12. a through hole; 13. stirring blades; 14. mounting blocks; 15. a rotating wheel; 16. a guide groove; 17. a guide shaft; 18. connecting grooves; 19. and (5) filtering by using a filter screen.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

Referring to fig. 1-5, the present invention provides a technical solution: a secondary extraction device for 3, 5-di-tert-butyl salicylic acid comprises a base body 1, an observation window 2, a liquid inlet 3, a first liquid outlet 4 and a second liquid outlet 5, wherein the observation window 2 is arranged at the outer end of the base body 1, the liquid inlet 3 is arranged at the top end of the base body 1, and the first liquid outlet 4 and the second liquid outlet 5 are arranged at the bottom end of the base body 1;

further comprising:

the containing tank 6 is connected with the first liquid outlet 4 at the bottom end of the base body 1 through a connecting pipeline, the containing tank 6 for storing the extracting agent is arranged at the top end of the base body 1, a liquid storage bottle 7 and a tooth block 9 are fixedly connected with the output end of a motor 8 are arranged at the top end of the base body 1, the outer side of the tooth block 9 is connected with a gear 10, the gear 10 is connected to the inner side of the top end of the base body 1 in a shaft mode, a torsion spring 11 is arranged on the outer surface of the shaft end of the gear 10, a through hole 12 is formed in the outer end of the gear 10, meanwhile, the position of the through hole 12 corresponds to the output end of the liquid storage bottle 7, and a stirring blade 13 is arranged at the inner end of the base body 1;

the installation block 14 is fixedly installed at the bottom end of the base body 1, the inner end of the installation block 14 is provided with a rotating wheel 15, the rotating wheel 15 is fixedly connected with the output end of the motor 8, meanwhile, the outer surface of the rotating wheel 15 is provided with a guide groove 16, the outer side of the guide groove 16 is connected with a guide shaft 17, the guide shaft 17 is connected with the installation block 14 through a connecting groove 18, the bottom end of the base body 1 is provided with a filter screen 19, and the inner side of the filter screen 19 is fixedly connected with the guide shaft 17.

The outer surface of the tooth block 9 is only partially of a toothed structure, the tooth block 9 is meshed with the gear 10, the gear 10 is rotatably connected with the top end of the base body 1, the gear 10 forms an elastic structure with the top end of the base body 1 through the torsion spring 11, the outer end of the gear 10 is provided with a through hole 12, the through hole 12 is correspondingly communicated with the output end of the liquid storage bottle 7, the mounting blocks 14 are symmetrically distributed and mounted on the center line of the base body 1, the mounting blocks 14 are connected with the rotating wheel 15 in a clamping mode, and the rotating wheel 15 is fixedly mounted at the bottom end of the output end of the motor 8.

The outer surface of runner 15 is seted up guide way 16, and guide way 16 is for block connection with guiding axle 17, and guide way 16 is the slope column structure in the front view, and guiding axle 17 is provided with two sets of about runner 15 central line symmetry distribution, and guiding axle 17 constitutes sliding construction through connecting groove 18 and installation piece 14, and guiding axle 17 fixed mounting is in the inboard of filter screen 19.

The working principle is as follows: when the 3, 5-di-tert-butyl salicylic acid secondary extraction device is used, according to the graph shown in the figure 1-5, firstly, the device is placed at a position to be operated, raw liquid to be extracted is put into the base body 1 through the liquid inlet 3, then, an extracting agent is put into the liquid storage bottle 7, the motor 8 is powered on, the output end of the motor drives the tooth block 9 to rotate, so that the tooth block 9 drives the gear 10 to synchronously rotate, the through hole 12 is not correspondingly communicated with the output end of the liquid storage bottle 7 due to the rotation of the gear 10, because only part of the outer surface of the tooth block 9 is of a toothed structure, when the toothed structure is disengaged from the gear 10, the gear 10 automatically resets under the action of the torsion spring 11 on the outer surface of the shaft end, so that the through hole 12 is correspondingly communicated with the output end of the liquid storage bottle 7 again, the extracting agent is discharged, and the extracting agent is intermittently put through the continuous rotation of the tooth block 9, therefore, the extractant can be more uniformly mixed with the stock solution at the inner end of the matrix 1, and meanwhile, the output end of the motor 8 drives the stirring blade 13 to rotate, so that the extractant and the solute in the stock solution are fully contacted and mixed;

after the extraction, can form the residue in the stoste, can drive bottom runner 15 along with the rotation of motor 8 and carry out synchronous motion, runner 15 will rotate with in the time of the 14 blocks of installation piece, make runner 15 outer end slope column structure's guide way 16 drive guiding axle 17 carry out perpendicular reciprocating motion, guiding axle 17 slides in installation piece 14 inner spread groove 18, and drive filter screen 19 and vibrate, make at follow-up play liquid in-process, the residue can not get into the liquid outlet, simultaneously because filter screen 19 can produce to vibrate and make the residue can not block up filter screen 19, the solution after the extraction can get into holding jar 6 through first liquid outlet 4 and store, holistic practicality has been increased.

Those not described in detail in this specification are within the skill of the art.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the utility model, the scope of which is defined in the appended claims and their equivalents.

Claims

1. A secondary extraction device for 3, 5-di-tert-butyl salicylic acid comprises a base body (1), an observation window (2), a liquid inlet (3), a first liquid outlet (4) and a second liquid outlet (5), wherein the observation window (2) is arranged at the outer end of the base body (1), the liquid inlet (3) is arranged at the top end of the base body (1), and the first liquid outlet (4) and the second liquid outlet (5) are arranged at the bottom end of the base body (1);

it is characterized by also comprising:

the device comprises a containing tank (6) connected with a first liquid outlet (4) at the bottom end of a base body (1) through a connecting pipeline, wherein the containing tank (6) for storing an extracting agent is arranged at the top end of the base body (1), a liquid storage bottle (7) and a motor (8) are arranged at the top end of the base body (1), a tooth block (9) is fixedly connected with the output end of the motor (8), the outer side of the tooth block (9) is connected with a gear (10), the gear (10) is connected to the inner side of the top end of the base body (1) in a shaft mode, a torsion spring (11) is arranged on the outer surface of the shaft end of the gear (10), a through hole (12) is formed in the outer end of the gear (10), meanwhile, the position of the through hole (12) corresponds to the output end of the liquid storage bottle (7), and a stirring blade (13) is arranged at the inner end of the base body (1);

installation piece (14), fixed mounting in the bottom of base member (1), and installation piece (14) inner is provided with runner (15) to the output fixed connection of runner (15) and motor (8), guide way (16) have been seted up to the surface of runner (15) simultaneously, the outside of guide way (16) is connected with guiding axle (17), and guiding axle (17) are connected with installation piece (14) through spread groove (18), the bottom of base member (1) is provided with filter screen (19), and the inboard and the guiding axle (17) fixed connection of filter screen (19).

2. A secondary 3, 5-di-tert-butyl salicylic acid extraction apparatus according to claim 1, characterized in that the outer surface of the tooth block (9) is only partially provided with a tooth structure, the tooth block (9) is in meshed connection with the gear (10), and the gear (10) is in rotary connection with the top end of the base body (1).

3. The secondary extraction equipment of 3, 5-di-tert-butyl salicylic acid according to claim 2, characterized in that the gear (10) forms an elastic structure with the top end of the base body (1) through a torsion spring (11), and the outer end of the gear (10) is provided with a through hole (12), and the position of the through hole (12) is correspondingly communicated with the output end of the liquid storage bottle (7).

4. The secondary extraction equipment of 3, 5-di-tert-butyl salicylic acid according to claim 1, characterized in that the mounting blocks (14) are symmetrically arranged about the center line of the base body (1) in two groups, the mounting blocks (14) are connected with the rotating wheel (15) in a clamping manner, and the rotating wheel (15) is fixedly arranged at the bottom end of the output end of the motor (8).

5. The secondary extraction equipment of 3, 5-di-tert-butyl salicylic acid according to claim 4, characterized in that the outer surface of the rotating wheel (15) is provided with a guide groove (16), the guide groove (16) is connected with a guide shaft (17) in a clamping manner, and the guide groove (16) is in an inclined structure in front view.

6. The secondary extraction equipment of 3, 5-di-tert-butyl salicylic acid according to claim 1, characterized in that the guide shafts (17) are symmetrically distributed about the center line of the rotating wheel (15) in two groups, the guide shafts (17) and the mounting block (14) form a sliding structure through the connecting groove (18), and the guide shafts (17) are fixedly mounted on the inner side of the filter screen (19).