CN215479749U - Hundred-ton-level water-phase mechanical stripping graphene production line - Google Patents

Hundred-ton-level water-phase mechanical stripping graphene production line Download PDF

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Publication number
CN215479749U
CN215479749U CN202122013177.3U CN202122013177U CN215479749U CN 215479749 U CN215479749 U CN 215479749U CN 202122013177 U CN202122013177 U CN 202122013177U CN 215479749 U CN215479749 U CN 215479749U
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pipeline
reation kettle
anchor
reaction kettle
hundred
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唐忠锋
许红伍
袁天刚
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Jiangsu Sijun Mechanical Equipment Co ltd
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Jiangsu Sijun Mechanical Equipment Co ltd
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Abstract

The utility model discloses a hundred-ton-level water phase mechanical stripping graphene production line, which comprises the following steps: a purified water pipeline, a CIP cleaning pipeline, a vacuum pipeline, a reaction kettle, a group of anchor type reaction kettles and a spray dryer, the vacuum pipeline, the CIP cleaning pipeline and the purified water pipeline are arranged above the reaction kettle and the anchor type reaction kettle in parallel, the purified water pipeline is connected with the reaction kettle, the vacuum pipeline and the CIP cleaning pipeline are connected with the reaction kettle and the anchor type reaction kettle, the reaction kettle, the anchor type reaction kettle and the spray dryer are oppositely arranged and are connected in series through pipelines, the structure design is reasonable, the automation degree is high, the reaction kettle and a group of anchor type reaction kettles are connected in series to work in sequence, the grinding dispersion machine, the explosion-proof rotor pump and the high-pressure homogenizer are matched for use to carry out secondary grinding emulsification, the aim of fully refining the graphene raw material is achieved, and then the CIP cleaning pipeline cleans the production line, reduces the amount of manual labor, improves the working efficiency and increases the enterprise benefit.

Description

Hundred-ton-level water-phase mechanical stripping graphene production line
Technical Field
The utility model belongs to the field of production and manufacturing, and particularly relates to a hundred-ton-level water-phase mechanical stripping graphene production line.
Background
The traditional method for preparing the graphene material mostly adopts a chemical oxidation method or a mechanical stripping method, wherein the chemical oxidation method belongs to chemical stripping, but the graphene oxide prepared by violent oxidation has high single-layer rate but more defects and damaged crystal structure, so that the performance is reduced in various aspects, even if the reduced graphene oxide material is obtained by reduction treatment, the defects in the crystal structure cannot be completely repaired and internal oxygen-containing functional groups are removed, so that the application range is limited, and the annual yield of the graphene single line prepared by the method can only reach the tonnage level, and the requirement of large-scale production cannot be met; the corresponding manufacturing cost is huge, the mechanical stripping method belongs to physical stripping, and mainly adopts liquid phase to carry out mechanical stripping, the liquid phase stripping usually uses an oil phase as a liquid phase carrier, the oil phase is an organic solvent, has certain corrosivity and pollution, has poor environmental protection benefit, higher cost and common quality, the annual output of a single line can reach ten tons, the large-scale production capacity is slightly improved, but the method has great test on the continuous operation of equipment, and the solvent discharge cost is very high.
SUMMERY OF THE UTILITY MODEL
Utility model purpose: in order to overcome the defects, the utility model aims to provide a hundred-ton-grade water-phase mechanical stripping graphene production line which is reasonable in structural design, high in automation degree and controllable in quality, a reaction kettle and a group of anchor type reaction kettles are connected in series to work in sequence, a grinding dispersion machine, an explosion-proof rotor pump and a high-pressure homogenizer are matched for secondary grinding and emulsification, the purpose of fully refining graphene raw materials is achieved, a CIP cleaning pipeline is used for cleaning the production line, the amount of manual labor is reduced, the working efficiency is improved, and the enterprise benefit is increased.
The technical scheme is as follows: in order to achieve the above object, the present invention provides a hundred-ton-level aqueous phase mechanical stripping graphene production line, including: the device comprises a purification water pipeline, a CIP cleaning pipeline, a vacuum pipeline, a reaction kettle, a group of anchor type reaction kettles and a spray dryer, wherein the vacuum pipeline, the CIP cleaning pipeline and the purification water pipeline are arranged above the reaction kettle and the anchor type reaction kettles in parallel, the purification water pipeline is connected with the reaction kettle, the vacuum pipeline and the CIP cleaning pipeline are connected with the reaction kettle and the anchor type reaction kettles, the reaction kettle, the anchor type reaction kettles and the spray dryer are arranged oppositely and connected in series through pipelines, the reaction kettle and the group of anchor type reaction kettles are connected in series to work in sequence, a grinding dispersion machine, an explosion-proof rotor pump and a high-pressure homogenizer are matched for use to carry out secondary grinding emulsification, the purpose of fully refining the graphene raw materials is achieved, and the production line is cleaned by the CIP cleaning pipeline.
Wherein, anchor reation kettle includes first anchor reation kettle, second anchor reation kettle, third anchor reation kettle and fourth anchor reation kettle, first anchor reation kettle, second anchor reation kettle, third anchor reation kettle and fourth anchor reation kettle set up relatively and pass through pipeline series connection.
Further, reation kettle outlet pipe says and is equipped with first grinding dispenser, the entry and reation kettle's exit linkage of first grinding dispenser, the export of first grinding dispenser and reation kettle's entry linkage make the further grinding dispersion of the graphite alkene raw materials that has the purified water.
Further, the export of first anchor reation kettle is equipped with explosion-proof rotor pump, the export of explosion-proof rotor pump is equipped with the second dispersion and grinds the machine, the entry of explosion-proof rotor pump passes through the exit linkage of pipeline with first anchor reation kettle, the export of explosion-proof rotor pump passes through the pipeline and grinds the entry linkage of machine with the second dispersion, the export of machine is ground through the pipeline and is connected with first anchor reation kettle in the second dispersion, makes the deeper grinding emulsification of graphite alkene raw materials.
Further, a high-pressure homogenizer is arranged at an outlet of the second anchor type reaction kettle, an inlet of the high-pressure homogenizer is connected with an outlet of the second anchor type reaction kettle through a pipeline, an outlet of the high-pressure homogenizer is connected with an inlet of the third anchor type reaction kettle through a pipeline, and the graphene slurry emulsified by the anchor type reaction kettle is homogenized and refined through the high-pressure homogenizer again.
Further, be equipped with a pair of dispenser on the first anchor reation kettle, a pair of dispenser passes through the bolt fastening on first anchor reation kettle, and the setting up of a pair of dispenser makes in the anchor reation kettle can carry out not equidirectional stirring to thick liquids.
Further, the dispersion machine is described in detail in a patent with a publication number of CN112090554A and a name of a special high-shear grinding dispersion system for graphene slurry, and includes a first motor, an upper flange plate, a flange seat, a middle flange plate, a lower flange plate, a mounting seat, a first connecting shaft, a connecting rod, a connecting plate, a stator and a rotor, wherein the flange seat is provided with the upper flange plate, the middle flange plate and the lower flange plate, the first motor is connected with the upper flange plate, the lower flange plate is connected with the mounting seat below through a screw, a group of connecting rods are arranged below the lower flange plate, the connecting plate is arranged below the connecting rods, the stator is sleeved on the first connecting shaft, the stator is further fixed on the connecting plate through a screw, and the rotor is connected with the tail end of the first connecting shaft.
Furthermore, all be equipped with agitating unit on the anchor reation kettle, agitating unit sets up in anchor reation kettle axle center position.
Further, agitating unit includes second motor, second connecting axle and impeller, the second connecting axle sets up in second motor below, the impeller sets up at first connecting axle end.
Furthermore, a dispersing device is arranged on the reaction kettle and is arranged at the axis position of the reaction kettle.
Further, the dispersing device comprises a third motor, a third connecting shaft and a dispersing head, the third connecting shaft is arranged below the third motor, and the dispersing head is arranged at the tail end of the third connecting shaft.
The technical scheme shows that the utility model has the following beneficial effects:
1. according to the hundred-ton-level water-phase mechanical stripping graphene production line, purified water is injected into a reaction kettle through a purified water pipeline, a dispersing device is used for stirring a mixture of the water and graphene powder, the mixture is further emulsified through an anchor type reaction kettle, and finally the mixture is dried through a spray dryer, so that high-speed mechanical stripping with water as a liquid-phase carrier is realized, the annual output can reach hundred tons, the large-scale production capacity is improved, the water phase is used for mechanical stripping, the crystal structure of the prepared graphene material is completely stored, the quality of the product is improved, a series of problems of cost, environment, quality, performance and the like are effectively solved, and a new industrial technical direction is introduced.
2. The reaction kettle and the anchor type reaction kettle are connected in series to work in sequence, the grinding dispersion machine, the explosion-proof rotor pump and the high-pressure homogenizer are matched for use to carry out secondary grinding emulsification, the aim of fully refining the graphene raw material is achieved, the CIP cleaning pipeline is used for cleaning a production line, the labor amount is reduced, and the working efficiency is improved.
3. The pair of dispersers are fixed on the first anchor type reaction kettle, and the arrangement of the pair of dispersers enables the anchor type reaction kettle to stir the slurry in different directions.
Drawings
Fig. 1 is a schematic structural diagram of a hundred-ton-level aqueous phase mechanical stripping graphene production line according to the utility model;
FIG. 2 is a schematic view of the structure of the raw material refining apparatus according to the present invention
FIG. 3 is a schematic view of the structure of the dispersing machine according to the present invention;
FIG. 4 is a schematic structural view of a stirring device according to the present invention;
FIG. 5 is a schematic view of a dispersing apparatus according to the present invention;
1 purified water pipeline, 2 CIP cleaning pipeline, 3 vacuum pipeline, 4 reaction kettles, 5 anchor type reaction kettles, 6 spray drier, 51 first anchor type reaction kettle, 52 second anchor type reaction kettle, 53 third anchor type reaction kettle, 54 fourth anchor type reaction kettle, 41 first grinding dispersion machine, 511 explosion-proof rotor pump, 512 second grinding dispersion machine, 521 high-pressure homogenizer, 513 dispersion machine, 5131 first motor, 5132 upper flange plate, 5133 flange seat, 5135 middle flange plate, 5135 lower flange plate, 5136 mounting seat, 5137 first connecting shaft, 5138 connecting rod, 5139 connecting plate, 5140 stator, 5141 rotor, 55 stirring device, 551 second motor, 552 second connecting shaft, 553 impeller, 42 dispersion device, 421 third motor, 422 third connecting shaft and 423 dispersion head.
Detailed Description
The utility model is further elucidated with reference to the drawings and the embodiments.
Examples
Reference will now be made in detail to embodiments of the present invention, examples of which are illustrated in the accompanying drawings, wherein like or similar reference numerals refer to the same or similar elements or elements having the same or similar function throughout. The embodiments described below with reference to the drawings are illustrative and intended to be illustrative of the utility model and are not to be construed as limiting the utility model.
In the description of the present invention, it is to be understood that the terms "center", "longitudinal", "lateral", "length", "width", "thickness", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "clockwise", "counterclockwise", and the like, indicate orientations and positional relationships based on those shown in the drawings, and are used only for convenience of description and simplicity of description, and do not indicate or imply that the device or element being referred to must have a particular orientation, be constructed and operated in a particular orientation, and thus, are not to be considered as limiting the present invention.
Furthermore, the terms "first", "second" and "first" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance or implicitly indicating the number of technical features indicated. Thus, a feature defined as "first" or "second" may explicitly or implicitly include one or more of that feature. In the description of the present invention, unless otherwise specified, "a plurality" means two or more unless explicitly defined otherwise.
In the present invention, unless otherwise expressly specified or limited, the terms "mounted," "connected," "secured," and the like are to be construed broadly and can, for example, be fixedly connected, detachably connected, or integrally connected; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meanings of the above terms in the present invention can be understood by those skilled in the art according to specific situations.
In the present invention, unless otherwise expressly stated or limited, "above" or "below" a first feature means that the first and second features are in direct contact, or that the first and second features are not in direct contact but are in contact with each other via another feature therebetween. Also, the first feature being "on," "above" and "over" the second feature includes the first feature being directly on and obliquely above the second feature, or merely indicating that the first feature is at a higher level than the second feature. A first feature being "under," "below," and "beneath" a second feature includes the first feature being directly under and obliquely below the second feature, or simply meaning that the first feature is at a lesser elevation than the second feature.
Example 1
A hundred-ton-level water phase mechanical stripping graphene production line as shown in the figure comprises: the device comprises a purified water pipeline 1, a CIP cleaning pipeline 2, a vacuum pipeline 3, a reaction kettle 4, a group of anchor type reaction kettles 5 and a spray dryer 6, wherein the anchor type reaction kettles 5 comprise a first anchor type reaction kettle 51, a second anchor type reaction kettle 52, a third anchor type reaction kettle 53 and a fourth anchor type reaction kettle 54, the first anchor type reaction kettle 51, the second anchor type reaction kettle 52, the third anchor type reaction kettle 53 and the fourth anchor type reaction kettle 54 are oppositely arranged and are connected in series through pipelines, an outlet pipeline of the reaction kettle 4 is provided with a first grinding dispersion machine 41, an inlet of the first grinding dispersion machine 41 is connected with an outlet of the reaction kettle 4, an outlet of the first grinding dispersion machine 41 is connected with an inlet of the reaction kettle 4, the vacuum pipeline 1, the CIP cleaning pipeline 2 and the purified water pipeline 3 are arranged above the reaction kettle 4 and the anchor type reaction kettle 5 in parallel, the purified water pipeline 3 is connected with the reaction kettle 4, vacuum line 1 and CIP wash pipeline 2 and reation kettle 4 and anchor reation kettle 5 are connected, reation kettle 4, anchor reation kettle 5 and spray dryer 6 set up relatively, and connect through the pipeline series connection.
In this embodiment, the outlet of the first anchor reactor 51 is provided with an explosion-proof rotor pump 511, the outlet of the explosion-proof rotor pump 511 is provided with a second dispersion grinder 512, the inlet of the explosion-proof rotor pump 511 is connected with the outlet of the first anchor reactor 51 through a pipeline, the outlet of the explosion-proof rotor pump 511 is connected with the inlet of the second dispersion grinder 512 through a pipeline, and the outlet of the second dispersion grinder 512 is connected with the first anchor reactor 51 through a pipeline, so that the graphene raw material is further ground and emulsified.
In this embodiment, a high-pressure homogenizer 521 is disposed at an outlet of the second anchor reactor 52, an inlet of the high-pressure homogenizer 521 is connected to an outlet of the second anchor reactor 52 through a pipeline, an outlet of the high-pressure homogenizer 521 is connected to an inlet of the third anchor reactor 53 through a pipeline, and the graphene slurry emulsified by the anchor reactor is homogenized and refined by the high-pressure homogenizer again.
Example 2
A hundred-ton-level water phase mechanical stripping graphene production line as shown in the figure comprises: purification water pipeline 1, CIP wash pipeline 2, vacuum line 3, reation kettle 4, a set of anchor formula reation kettle 5 and spray drier 6, be equipped with a pair of dispenser 513 on the anchor formula reation kettle 51, a pair of dispenser 513 passes through the bolt fastening on first anchor formula reation kettle 51, all be equipped with agitating unit 55 on the anchor formula reation kettle 5, agitating unit 55 sets up at anchor formula reation kettle 5 axle center position, vacuum pipeline 1, CIP wash pipeline 2 and purification water pipeline 3 set up side by side in reation kettle 4 and anchor formula reation kettle 5 top, purification water pipeline 3 is connected with reation kettle 4, vacuum pipeline 1 and CIP wash pipeline 2 are connected with reation kettle 4 and anchor formula reation kettle 5, reation kettle 4, anchor formula reation kettle 5 and spray drier 6 set up relatively, and pass through the pipeline series connection.
In this embodiment, the dispersing machine 513 includes a first motor 5131, an upper flange plate 5132, a flange seat 5133, a middle flange plate 5134, a lower flange plate 5135, a mounting seat 5136, a first connecting shaft 5137, a connecting rod 5138, a connecting plate 5139, a stator 5140, and a rotor 5141, where the flange seat 5133 is provided with the upper flange plate 5132, the middle flange plate 5134, and the lower flange plate 5135, the first motor 5131 is connected to the upper flange plate 5132, the lower flange plate 5135 is connected to the mounting seat 5136 below by screws, a set of connecting rods 5138 is arranged below the lower flange plate 5135, the connecting plate 5139 is arranged below the connecting rods 5138, the stator 5140 is sleeved on the first connecting shaft 5137, the stator 5140 is further fixed to the connecting plate 5139 by screws, and the rotor 5141 is connected to the end of the first connecting shaft 5137.
Example 3
The hundred-ton-level water phase mechanical stripping graphene production line comprises a purified water pipeline 1, a CIP cleaning pipeline 2, a vacuum pipeline 3, a reaction kettle 4, a group of anchor type reaction kettles 5 and a spray dryer 6, wherein each anchor type reaction kettle 5 comprises a first anchor type reaction kettle 51, a second anchor type reaction kettle 52, a third anchor type reaction kettle 53 and a fourth anchor type reaction kettle 54, the first anchor type reaction kettle 51, the second anchor type reaction kettle 52, the third anchor type reaction kettle 53 and the fourth anchor type reaction kettle 54 are oppositely arranged and connected in series through pipelines, the vacuum pipeline 1, the CIP cleaning pipeline 2 and the purified water pipeline 3 are arranged above the reaction kettle 4 and the anchor type reaction kettle 5 in parallel, the purified water pipeline 3 is connected with the reaction kettle 4, the vacuum pipeline 1 and the CIP cleaning pipeline 2 are connected with the reaction kettle 4 and the anchor type reaction kettle 5, the reaction kettle 4, the anchor type reaction kettle 5 and the spray dryer 6 are oppositely arranged, and are connected in series by a pipe.
In this embodiment, the outlet pipeline of the reaction kettle 4 is provided with a first grinding disperser 41, the inlet of the first grinding disperser 41 is connected to the outlet of the reaction kettle 4, and the outlet of the first grinding disperser 41 is connected to the inlet of the reaction kettle 4.
In this embodiment, the outlet of the first anchor reactor 51 is provided with an explosion-proof rotor pump 511, the outlet of the explosion-proof rotor pump 511 is provided with a second dispersion grinder 512, the inlet of the explosion-proof rotor pump 511 is connected with the outlet of the first anchor reactor 51 through a pipeline, the outlet of the explosion-proof rotor pump 511 is connected with the inlet of the second dispersion grinder 512 through a pipeline, and the outlet of the second dispersion grinder 512 is connected with the first anchor reactor 51 through a pipeline.
In this embodiment, a high-pressure homogenizer 521 is disposed at an outlet of the second anchor reactor 52, an inlet of the high-pressure homogenizer 521 is connected to an outlet of the second anchor reactor 52 through a pipeline, an outlet of the high-pressure homogenizer 521 is connected to an inlet of the third anchor reactor 53 through a pipeline, and the graphene slurry emulsified by the anchor reactor is homogenized and refined by the high-pressure homogenizer again.
In this embodiment, a pair of dispersers 513 is disposed on the first anchor reactor 51, and the pair of dispersers 513 is fixed to the first anchor reactor 51 by bolts.
In this embodiment, the dispersing machine 513 includes a first motor 5131, an upper flange plate 5132, a flange seat 5133, a middle flange plate 5134, a lower flange plate 5135, a mounting seat 5136, a first connecting shaft 5137, a connecting rod 5138, a connecting plate 5139, a stator 5140, and a rotor 5141, where the flange seat 5133 is provided with the upper flange plate 5132, the middle flange plate 5134, and the lower flange plate 5135, the first motor 5131 is connected to the upper flange plate 5132, the lower flange plate 5135 is connected to the mounting seat 5136 below by screws, a set of connecting rods 5138 is arranged below the lower flange plate 5135, the connecting plate 5139 is arranged below the connecting rods 5138, the stator 5140 is sleeved on the first connecting shaft 5137, the stator 5140 is further fixed to the connecting plate 5139 by screws, and the rotor 5141 is connected to the end of the first connecting shaft 5137.
In this embodiment, all be equipped with agitating unit 55 on anchor reation kettle 5, agitating unit 55 sets up in anchor reation kettle 5 axle center position.
The stirring device 55 in this embodiment includes a second motor 551, a second connecting shaft 552, and an impeller 553, the second connecting shaft 552 is disposed below the second motor 551, and the impeller 553 is disposed at a distal end of the first connecting shaft 552.
In this embodiment, the reaction kettle 4 is provided with the dispersing device 42, the dispersing device 42 includes a third motor 421, a third connecting shaft 422 and a dispersing head 423, the third connecting shaft 422 is disposed below the third motor 421, and the dispersing head 423 is disposed at the end of the third connecting shaft 422.
The specific working mode of the hundred-ton-level aqueous phase mechanical stripping graphene production line in the embodiment is as follows: filling a graphene powder raw material into a reaction kettle 4, simultaneously opening a purified water pipeline 1, wherein the ratio of the graphene powder to water is 1: 2, the dispersing device 42 works to stir, the vacuum pipeline 3 is opened, the air pressure in the five kettles is reduced to 0.3 atmospheric pressure, the first GBI2000/20 grinding disperser 41 is started, the inlet valve of the first GBI2000/20 grinding disperser 41 is opened, the mixture of water and powder enters the first grinding disperser 41 to be ground and dispersed, and then is discharged into the reaction kettle 4, the mixture circulates in the first GBI2000/20 grinding disperser 41 and the reaction kettle 4, when the granularity of the mixture reaches a certain degree, the valve on the pipeline between the reaction kettle 4 and the first anchor type reaction kettle 51 is opened, the mixture flows into the first anchor type reaction kettle 51, the first anchor type reaction kettle 51 is started, the mixture in the kettles is further emulsified, the explosion-proof rotor pump 511 and the GMSD2000/20 second grinding disperser 512 are started, and the mixture flows into the first anchor type reaction kettle 51, the explosion-proof rotor pump 511, the GMSD2000/20 second grinding disperser 512 are started, and the mixture is stirred in the first anchor type reaction kettle 51, Circulating flow emulsification between GMSD2000/20 second grinding disperser 512. After the materials are emulsified to a certain degree, an upper valve of a pipeline between the first anchor type reaction kettle 51 and the second anchor type reaction kettle 52 is opened, the materials are discharged into the second anchor type reaction kettle 52, the materials are emulsified in the second anchor type reaction kettle 52 and then discharged into the high-pressure homogenizer 521 for homogenization and refinement, then the materials are discharged into the third anchor type reaction kettle 53 through the high-pressure homogenizer 521, the mixed materials are further emulsified through the third anchor type reaction kettle 53 and the fourth anchor type reaction kettle 54 in sequence, and the granularity of the graphene meets the expected requirement. And finally, drying the emulsified graphene slurry by a spray dryer 6 to obtain a finished graphene material, cleaning the production line by the CIP cleaning pipeline 2, powering off the equipment, and ending a working process.
The foregoing is only a preferred embodiment of the present invention, and it should be noted that modifications can be made by those skilled in the art without departing from the principle of the present invention, and these modifications should also be construed as the protection scope of the present invention.

Claims (10)

1. The utility model provides a hundred tons of grades of aqueous phase machinery peel off graphite alkene production lines which characterized in that: the method comprises the following steps: purification water pipeline (1), CIP wash pipeline (2), vacuum pipeline (3), reation kettle (4), a set of anchor formula reation kettle (5) and spray dryer (6), vacuum pipeline (3), CIP wash pipeline (2) and purification water pipeline (1) set up side by side in reation kettle (4) and anchor formula reation kettle (5) top, purification water pipeline (1) is connected with reation kettle (4), vacuum pipeline (3) and CIP wash pipeline (2) and reation kettle (4) and anchor formula reation kettle (5) are connected, reation kettle (4), anchor formula reation kettle (5) and spray dryer (6) set up relatively, and connect through the pipeline series connection.
2. The hundred-ton-grade aqueous phase mechanical stripping graphene production line according to claim 1, characterized in that: anchor formula reation kettle (5) include first anchor formula reation kettle (51), second anchor formula reation kettle (52), third anchor formula reation kettle (53) and fourth anchor formula reation kettle (54), first anchor formula reation kettle (51), second anchor formula reation kettle (52), third anchor formula reation kettle (53) and fourth anchor formula reation kettle (54) set up relatively and pass through pipeline series connection.
3. The hundred-ton-grade aqueous phase mechanical stripping graphene production line according to claim 1, characterized in that: reation kettle (4) outlet pipe says and is equipped with first grinding dispenser (41), the entry of first grinding dispenser (41) and the exit linkage of reation kettle (4), the exit linkage of the entry of first grinding dispenser (41) and reation kettle (4).
4. The hundred-ton-grade aqueous phase mechanical stripping graphene production line according to claim 2, characterized in that: the export of first anchor reation kettle (51) is equipped with explosion-proof rotor pump (511), the export of explosion-proof rotor pump (511) is equipped with second dispersion and grinds machine (512), the entry of explosion-proof rotor pump (511) passes through the exit linkage of pipeline with first anchor reation kettle (51), the exit linkage of explosion-proof rotor pump (511) passes through the pipeline with the entry linkage of second dispersion and grinds machine (512), the export of second dispersion and grinds machine (512) passes through the pipeline and is connected with first anchor reation kettle (51).
5. The hundred-ton-grade aqueous phase mechanical stripping graphene production line according to claim 2, characterized in that: and a high-pressure homogenizer (521) is arranged at the outlet of the second anchor type reaction kettle (52), the inlet of the high-pressure homogenizer (521) is connected with the outlet of the second anchor type reaction kettle (52) through a pipeline, and the outlet of the high-pressure homogenizer (521) is connected with the inlet of the third anchor type reaction kettle (53) through a pipeline.
6. The hundred-ton-grade aqueous phase mechanical stripping graphene production line according to claim 2, characterized in that: a pair of dispersing machines (513) is arranged on the first anchor type reaction kettle (51), and the pair of dispersing machines (513) is fixed on the first anchor type reaction kettle (51) through bolts.
7. The hundred-ton-grade aqueous phase mechanical stripping graphene production line according to claim 6, is characterized in that: the dispersion machine (513) comprises a first motor (5131), an upper flange plate (5132), a flange seat (5133), a middle flange plate (5134), a lower flange plate (5135), a mounting seat (5136), a first connecting shaft (5137), a connecting rod (5138), a connecting plate (5139), a stator (5140) and a rotor (5141), the flange seat (5133) is provided with an upper flange plate (5132), a middle flange plate (5134) and a lower flange plate (5135), the first motor (5131) is connected with an upper flange plate (5132), the lower flange plate (5135) is connected with a lower mounting seat (5136) through screws, a group of connecting rods (5138) are arranged below the lower flange plate (5135), a connecting plate (5139) is arranged below the connecting rods (5138), the stator (5140) is sleeved on the first connecting shaft (5137), the stator (5140) is further fixed on the connecting plate (5139) through screws, and the rotor (5141) is connected with the tail end of the first connecting shaft (5137).
8. The hundred-ton-grade aqueous phase mechanical stripping graphene production line according to claim 1, characterized in that: all be equipped with agitating unit (55) on anchor reation kettle (5), agitating unit (55) set up in anchor reation kettle (5) axle center position.
9. The hundred-ton-grade aqueous phase mechanical stripping graphene production line according to claim 8, characterized in that: the stirring device (55) comprises a second motor (551), a second connecting shaft (552) and an impeller (553), wherein the second connecting shaft (552) is arranged below the second motor (551), and the impeller (553) is arranged at the tail end of the first connecting shaft (5137).
10. The hundred-ton-grade aqueous phase mechanical stripping graphene production line according to claim 1, characterized in that: be equipped with dispersion devices (42) on reation kettle (4), dispersion devices (42) include third motor (421), third connecting axle (422) and dispersion head (423), third connecting axle (422) set up in third motor (421) below, dispersion head (423) set up at third connecting axle (422) end.
CN202122013177.3U 2021-08-25 2021-08-25 Hundred-ton-level water-phase mechanical stripping graphene production line Active CN215479749U (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116179005A (en) * 2022-12-21 2023-05-30 徐州中盛远达新材料有限公司 Metal material for fire resistance of steel structure and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116179005A (en) * 2022-12-21 2023-05-30 徐州中盛远达新材料有限公司 Metal material for fire resistance of steel structure and preparation method thereof

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