CN215427397U - Dulcitol drum sling circulation evaporation crystallization device - Google Patents

Dulcitol drum sling circulation evaporation crystallization device Download PDF

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Publication number
CN215427397U
CN215427397U CN202120837894.5U CN202120837894U CN215427397U CN 215427397 U CN215427397 U CN 215427397U CN 202120837894 U CN202120837894 U CN 202120837894U CN 215427397 U CN215427397 U CN 215427397U
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tank body
dulcitol
pipe
drum
jar body
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CN202120837894.5U
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马永华
刘仁民
王殿奎
李楠
吴宝君
何沛
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Zhongwei International Life Technology Co Ltd
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Zhongwei International Life Technology Co Ltd
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency

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Abstract

The utility model discloses a dulcitol drum sling circulation evaporation crystallization device, which comprises a base, wherein support columns are fixedly arranged at four corners of the top of the base, a tank body is fixedly arranged at the top of each support column, a first support plate is fixedly arranged at the left side of the tank body, a motor is fixedly arranged at the top of the first support plate, a rotating rod is movably connected to the right side of the motor, a spiral blade is fixedly arranged on the rotating rod, an interlayer is arranged in the tank body, a ring pipe is arranged in the interlayer, one end of the ring pipe penetrates through the tank body and is connected with a steam inlet, the other end of the ring pipe penetrates through the tank body and is connected with a steam outlet, a vacuum pump is arranged at the top of the tank body and is fixedly connected with the tank body through an air pipe, a second support plate is fixedly arranged at the bottom of the side wall of the tank body, and a ring pipe and a stirring device are arranged, so that dulcitol liquid can be uniformly heated conveniently and rapidly, the heating efficiency is greatly improved, and the practicability of the crystallization device is improved.

Description

Dulcitol drum sling circulation evaporation crystallization device
Technical Field
The utility model relates to the technical field of evaporative crystallization, in particular to a dulcitol drum-hung circulating evaporative crystallization device.
Background
Dulcitol is one of the components of the root of tripterygium hypoglaucum, is colorless crystalline powder, has a melting point of 188-189 ℃, is slightly sweet, is soluble in water, is easily soluble in boiling water and is slightly soluble in ethanol.
However, when the existing crystallization device carries out evaporative crystallization on dulcitol feed liquid, the dulcitol feed liquid needs to be heated, a heating pipeline is usually arranged in a tank body, steam is introduced into the heating pipeline and then the heating pipeline is heated, the heating on the dulcitol feed liquid is uneven, and therefore the dulcitol drum-hanging circulation evaporative crystallization device is provided.
SUMMERY OF THE UTILITY MODEL
In order to overcome the defects of the prior art, the dulcitol drum-hanging circulation evaporation crystallization device provided by the utility model has the advantages that the annular pipeline and the stirring device are arranged, so that the dulcitol feed liquid can be conveniently and rapidly and uniformly heated, the heating efficiency is greatly improved, and the practicability of the crystallization device is further improved.
In order to solve the technical problems, the utility model provides the following technical scheme: a dulcitol drum sling circulation evaporation crystallization device comprises a base, wherein support columns are fixedly arranged at four corners of the top of the base, a tank body is fixedly arranged at the top of each support column, a first support plate is fixedly arranged at the left side of the tank body, a motor is fixedly arranged at the top of the first support plate, a rotating rod is movably connected to the right side of the motor, a spiral blade is fixedly arranged on the rotating rod, an interlayer is arranged inside the tank body, a ring pipe is arranged inside the interlayer, one end of the ring pipe penetrates through the tank body and is connected with a steam inlet, the other end of the ring pipe penetrates through the tank body and is connected with a steam outlet, a vacuum pump is arranged at the top of the tank body and is fixedly connected with the tank body through a gas pipe, a second support plate is fixedly arranged at the bottom of the side wall of the tank body, a cylinder is fixedly arranged at the top of the second support plate, and a piston rod is movably connected to one side of the cylinder, piston rod one end runs through a jar of internal portion of side wall and extends to a jar of internal portion fixedly connected with push pedal, base top fixed mounting has the liquid collecting box, the liquid collecting box top is provided with the crystallization collecting box, the liquid collecting box right side is connected with the circulating pump through the drain pipe, the circulating pump right side is provided with the feed liquor pipe, feed liquor pipe one end runs through a jar of side wall and extends to a jar of internal portion.
As a preferred technical scheme, the right side wall of the tank body is provided with a feeding pipe, the top of the feeding pipe is provided with a feeding port, a bearing is fixedly arranged in the tank body, the rotating rod is rotatably connected with the tank body through the bearing, and the bottom of the tank body is provided with a discharging pipe.
As a preferred technical scheme of the utility model, one end of the motor is rotatably connected with a rotating shaft, and the rotating rod is rotatably connected with the motor through the rotating shaft.
As a preferable technical scheme of the utility model, sealing gaskets are arranged at the joints of the rotating rod and the piston rod with the inner wall of the tank body.
As a preferable technical scheme of the utility model, the two cylinders are symmetrically distributed at two ends of the tank body.
As a preferred technical scheme of the utility model, the bottom of the crystallization collection box is of a filter screen structure.
As a preferable technical scheme of the utility model, valves are arranged on the feeding pipe and the discharging pipe.
As a preferred technical scheme of the utility model, the bottom end of the discharge pipe penetrates through the crystallization collection box and extends to the interior of the crystallization collection box.
Compared with the prior art, the utility model can achieve the following beneficial effects:
1. through being provided with annular tube, motor, bull stick and helical blade, when steam got into the annular tube, the motor drove the bull stick and rotates to drive helical blade and rotate, realize stirring the dulcitol feed liquid, make the dulcitol feed liquid be heated more evenly.
2. Through being provided with collection liquid case, drain pipe, circulating pump and feed liquor pipe, the circulating pump work is taken out the collection for crystallization dulcitol feed liquid in with the collection liquid case through the drain pipe, and the process feed liquor pipe gets into a jar internal portion, and the crystallization once more.
Drawings
FIG. 1 is a front cross-sectional view of the present invention;
FIG. 2 is a front view of the present invention;
FIG. 3 is a side view of the present invention;
FIG. 4 is a top view of the present invention;
fig. 5 is an enlarged view of the structure at a in fig. 1 according to the present invention.
Wherein: 1. a base; 2. a support pillar; 3. a tank body; 4. a first support plate; 5. a motor; 6. a rotating rod; 7. a helical blade; 8. an interlayer; 9. an annular tube; 10. a steam inlet; 11. a steam outlet; 12. a vacuum pump; 13. an air tube; 14. a second support plate; 15. a cylinder; 16. a piston rod; 17. pushing the plate; 18. a liquid collection tank; 19. a crystallization collection box; 20. a liquid outlet pipe; 21. a circulation pump; 22. a liquid inlet pipe; 23. a feed tube; 24. a feed inlet; 25. a bearing; 26. and (4) discharging the pipe.
Detailed Description
The present invention will be further described with reference to specific embodiments for the purpose of facilitating an understanding of technical means, characteristics of creation, objectives and functions realized by the present invention, but the following embodiments are only preferred embodiments of the present invention, and are not intended to be exhaustive. Based on the embodiments in the implementation, other embodiments obtained by those skilled in the art without any creative efforts belong to the protection scope of the present invention. The experimental methods in the following examples are conventional methods unless otherwise specified, and materials, reagents and the like used in the following examples are commercially available unless otherwise specified.
Example (b):
as shown in figures 1-5, a dulcitol drum-hanging circulation evaporation crystallization device comprises a base 1, wherein four corners of the top of the base 1 are fixedly provided with support columns 2, the top of each support column 2 is fixedly provided with a tank body 3, the left side of the tank body 3 is fixedly provided with a first support plate 4, the top of the first support plate 4 is fixedly provided with a motor 5, the right side of the motor 5 is movably connected with a rotating rod 6, the rotating rod 6 is fixedly provided with a helical blade 7, the tank body 3 is internally provided with an interlayer 8, the interlayer 8 is internally provided with a ring pipe 9, one end of the ring pipe 9 penetrates through the tank body 3 to be connected with a steam inlet 10, the other end of the ring pipe 9 penetrates through the tank body 3 to be connected with a steam outlet 11, the top of the tank body 3 is provided with a vacuum pump 12, the vacuum pump 12 is fixedly connected with the tank body 3 through a gas pipe 13, the bottom of the side wall of the tank body 3 is fixedly provided with a second support plate 14, the top of the second support plate 14 is fixedly provided with a cylinder 15, a piston rod 16 is movably connected to one side of the air cylinder 15, one end of the piston rod 16 penetrates through the side wall of the tank body 3 and extends to the inside of the tank body 3 and is fixedly connected with a push plate 17, a liquid collecting box 18 is fixedly mounted at the top of the base 1, a crystallization collecting box 19 is arranged at the top of the liquid collecting box 18, the right side of the liquid collecting box 18 is connected with a circulating pump 21 through a liquid outlet pipe 20, a liquid inlet pipe 22 is arranged at the right side of the circulating pump 21, and one end of the liquid inlet pipe 22 penetrates through the side wall of the tank body 3 and extends to the inside of the tank body 3;
during the use, the staff adds the dulcitol feed liquid into jar body 3, when towards the inside steam that dashes into of ring channel 9 through steam inlet 10, starter motor 5, drive bull stick 6 and rotate, thereby drive helical blade 7 and rotate, realize stirring the dulcitol feed liquid, make the dulcitol feed liquid be heated more evenly, the heating efficiency of steam to the dulcitol feed liquid in ring channel 9 has been improved, after the heating is accomplished, vacuum pump 12 evacuates the inside air of jar body 3 through trachea 13, the crystallizer after the heating is concentrated under the suction of vacuum pump 12, thereby realize the crystallization to liquid dulcitol feed liquid, after the crystallization, start cylinder 15, control piston rod 16 promotes push pedal 17, promote the crystal after the crystallization to discharge from discharging pipe 26, get into crystallization collecting box 19, through the filter screen structure of crystallization collecting box 19 bottom with crystal and liquid separation, the liquid after the separation gets into collecting box 18, circulating pump 21 takes liquid out from liquid collection tank 18 through drain pipe 20, and inside liquid inlet pipe 22 reentrant jar body 3, recrystallization avoided the liquid waste of primary uncrystallized, realized circulation crystallization, resources are saved.
In other embodiments, as shown in fig. 1 and 5, a feeding pipe 23 is arranged on the right side wall of the tank 3, a feeding port 24 is arranged at the top of the feeding pipe 23, a bearing 25 is fixedly arranged inside the tank 3, the rotating rod 6 is rotatably connected with the tank 3 through the bearing 25, and a discharging pipe 26 is arranged at the bottom of the tank 3;
through being provided with filling tube 23 and charge door 24, the staff of being convenient for feeds in raw material toward jar internal portion of body 3, through setting up bearing 25, reduces the frictional force that produces between bull stick 6 and the jar body 3, increases the life of bull stick 6, through being provided with discharging pipe 26, the material of being convenient for in the jar body 3 is discharged.
In other embodiments, as shown in fig. 5, one end of the motor 5 is rotatably connected with a rotating shaft, and the rotating rod 6 is rotatably connected with the motor 5 through the rotating shaft;
through being provided with the pivot, be convenient for motor 5 control bull stick 6 to rotate.
In other embodiments, as shown in fig. 1, the joints of the rotating rod 6 and the piston rod 16 with the inner wall of the tank 3 are provided with sealing gaskets;
by arranging the sealing rings, the liquid is prevented from flowing out along the gap at the joint of the piston rod 16 and the rotating rod 6 with the tank body 3 during stirring.
In other embodiments, as shown in fig. 1 and 2, two cylinders 15 are provided and symmetrically distributed at two ends of the tank 3;
through being provided with two cylinders 15, be convenient for to the propelling movement of crystallization material.
In other embodiments, as shown in FIG. 1, the bottom of the crystallization collection tank 19 is a screen structure;
the bottom of the crystallization collection box 19 is set to be of a filter screen structure, so that materials can be conveniently fixed and separated.
In other embodiments, as shown in FIGS. 1-3, valves are provided on both the feed pipe 23 and the discharge pipe 26;
through set up the valve on filling tube 23, avoid the air to get into jar body 3 inside from filling tube 23, influence the crystallization effect, set up the valve on discharging pipe 26, avoid inside the dulcitol feed liquid inflow collecting box before not crystallizing.
In other embodiments, as shown in FIG. 1, the bottom end of the discharge pipe 26 extends through the crystallization collection tank 19 to the interior of the crystallization collection tank 19;
the collection of the crystals into the crystallization collection tank 19 is facilitated by connecting the discharge pipe 26 to the crystallization collection tank 19.
In the present invention, unless otherwise expressly stated or limited, "above" or "below" a first feature means that the first and second features are in direct contact, or that the first and second features are not in direct contact but are in contact with each other via another feature therebetween. Also, the first feature being "on," "above" and "over" the second feature includes the first feature being directly on and obliquely above the second feature, or merely indicating that the first feature is at a higher level than the second feature. A first feature being "under," "below," and "beneath" a second feature includes the first feature being directly under and obliquely below the second feature, or simply meaning that the first feature is at a lesser elevation than the second feature.
The foregoing shows and describes the general principles, essential features, and advantages of the utility model. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, and the preferred embodiments of the present invention are described in the above embodiments and the description, and are not intended to limit the present invention. The scope of the utility model is defined by the appended claims and equivalents thereof.

Claims (8)

1. The utility model provides a dulcitol drum sling circulation evaporation crystallization device, includes base (1), its characterized in that: the steam-water heater is characterized in that support columns (2) are fixedly mounted at four corners of the top of the base (1), a tank body (3) is fixedly mounted at the top of the support column (2), a first support plate (4) is fixedly mounted at the left side of the tank body (3), a motor (5) is fixedly mounted at the top of the first support plate (4), a rotating rod (6) is movably connected to the right side of the motor (5), a spiral blade (7) is fixedly mounted on the rotating rod (6), an interlayer (8) is formed in the tank body (3), a ring pipe (9) is arranged in the interlayer (8), one end of the ring pipe (9) penetrates through the tank body (3) and is connected with a steam inlet (10), the other end of the ring pipe (9) penetrates through the tank body (3) and is connected with a steam outlet (11), a vacuum pump (12) is arranged at the top of the tank body (3), and the vacuum pump (12) is fixedly connected with the tank body (3) through a gas pipe (13), the utility model discloses a solar water heater, including jar body (3), jar body (3) lateral wall bottom fixed mounting have second backup pad (14), second backup pad (14) top fixed mounting has cylinder (15), cylinder (15) one side swing joint has piston rod (16), piston rod (16) one end runs through jar body (3) lateral wall and extends to jar body (3) inside fixedly connected with push pedal (17), base (1) top fixed mounting has header tank (18), header tank (18) top is provided with crystallization collecting box (19), header tank (18) right side is connected with circulating pump (21) through drain pipe (20), circulating pump (21) right side is provided with feed liquor pipe (22), feed liquor pipe (22) one end runs through jar body (3) lateral wall and extends to jar body (3) inside.
2. The dulcitol drum-circulating evaporative crystallization apparatus of claim 1, wherein: the utility model discloses a jar body (3) is provided with charging tube (23) to the wall of jar body (3) right side, charging tube (23) top is provided with charge door (24), the inside fixed mounting of the jar body (3) has bearing (25), bull stick (6) are connected with jar body (3) rotation through bearing (25), jar body (3) bottom is provided with discharging pipe (26).
3. The dulcitol drum-circulating evaporative crystallization apparatus of claim 1, wherein: one end of the motor (5) is rotatably connected with a rotating shaft, and the rotating rod (6) is rotatably connected with the motor (5) through the rotating shaft.
4. The dulcitol drum-circulating evaporative crystallization apparatus of claim 1, wherein: and sealing gaskets are arranged at the joints of the rotating rod (6) and the piston rod (16) and the inner wall of the tank body (3).
5. The dulcitol drum-circulating evaporative crystallization apparatus of claim 1, wherein: the number of the cylinders (15) is two, and the cylinders are symmetrically distributed at two ends of the tank body (3).
6. The dulcitol drum-circulating evaporative crystallization apparatus of claim 1, wherein: the bottom of the crystallization collection box (19) is of a filter screen structure.
7. The dulcitol drum-circulating evaporative crystallization apparatus of claim 2, wherein: and valves are arranged on the feeding pipe (23) and the discharging pipe (26).
8. The dulcitol drum-circulating evaporative crystallization apparatus of claim 2, wherein: the bottom end of the discharge pipe (26) penetrates through the crystallization collection box (19) and extends to the interior of the crystallization collection box (19).
CN202120837894.5U 2021-04-22 2021-04-22 Dulcitol drum sling circulation evaporation crystallization device Active CN215427397U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202120837894.5U CN215427397U (en) 2021-04-22 2021-04-22 Dulcitol drum sling circulation evaporation crystallization device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202120837894.5U CN215427397U (en) 2021-04-22 2021-04-22 Dulcitol drum sling circulation evaporation crystallization device

Publications (1)

Publication Number Publication Date
CN215427397U true CN215427397U (en) 2022-01-07

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116139531A (en) * 2023-04-20 2023-05-23 莱州市莱玉化工有限公司 Crystallization separation device for magnesium sulfate production

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116139531A (en) * 2023-04-20 2023-05-23 莱州市莱玉化工有限公司 Crystallization separation device for magnesium sulfate production
CN116139531B (en) * 2023-04-20 2023-07-18 莱州市莱玉化工有限公司 Crystallization separation device for magnesium sulfate production

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