CN215028776U

CN215028776U - MOFs material crystal seed synthesis device

Info

Publication number: CN215028776U
Application number: CN202022139233.3U
Authority: CN
Inventors: 杜鑫; 胡思凡
Original assignee: Suzhou Na Chuangjia Environmental Protection Technology Engineering Co ltd
Current assignee: Suzhou Na Chuangjia Environmental Protection Technology Engineering Co ltd
Priority date: 2020-09-25
Filing date: 2020-09-25
Publication date: 2021-12-07
Anticipated expiration: 2030-09-25

Abstract

The utility model discloses a MOFs material crystal seed synthesizer, which comprises a shell, wherein a motor box is fixedly arranged at the top of the shell, a motor is fixedly arranged inside the motor box, the bottom of the motor is rotatably connected with a motor shaft, the bottom of the motor shaft is fixedly connected with a rotating shaft, the side wall of the rotating shaft is fixedly connected with a stirring rod, a reaction bin is fixedly arranged on the inner wall of the top of the shell, a heat conduction pipe is arranged inside the reaction bin, a blanking pipe is fixedly arranged at the bottom of the reaction bin, a solenoid valve is arranged on the blanking pipe, a hot air fan is started, the hot air fan leads hot air into the heat conduction pipe, so that the temperature inside the reaction bin is rapidly raised, the synthesis reaction efficiency is improved, the motor drives the rotating shaft and the stirring rod to rotate by starting the motor, the materials inside the reaction bin are stirred, the reaction speed between the materials is accelerated, and the stirring can enable the materials to react with reaction media more uniformly, thereby leading the synthesis reaction effect to be better and the quality to be higher.

Description

MOFs material crystal seed synthesis device

Technical Field

The utility model belongs to the technical field of the synthesis of MOFs material, concretely relates to MOFs material crystal seed synthesizer.

Background

The metal organic framework material is a crystalline porous material with a periodic network structure, which is called MOFs for short, formed by connecting an inorganic metal center (metal ion or metal cluster) and a bridged organic ligand through self-assembly. The MOFs material is an inorganic-organic hybrid material and is formed by the hybrid combination of inorganic metal ions and organic ligands, so that the MOFs material has the characteristics of both inorganic materials and organic materials, inorganic components enable the MOFs material to have fixed pore channels and specific functions, and organic components enable the MOFs material to have larger specific surface area and have the characteristics of designability, pore channel size adjustability, easy functionalization of pore channel surfaces and the like.

However, in the existing MOFs material synthesizing device, materials are usually directly put into a reaction device for reaction, which results in long reaction time, low reaction efficiency, and uneven reaction easily caused by the reaction of the materials under a static state.

SUMMERY OF THE UTILITY MODEL

An object of the utility model is to provide a MOFs material seed crystal synthesizer to solve the problem that proposes among the above-mentioned background art.

In order to achieve the above object, the utility model provides a following technical scheme: a MOFs material crystal seed synthesis device comprises a shell, wherein a feeding hole is formed in the top of the shell, a motor box is fixedly mounted at the top of the shell, a motor is fixedly mounted inside the motor box, the bottom of the motor is rotatably connected with a motor shaft, the bottom of the motor shaft is fixedly connected with a rotating shaft, the side wall of the rotating shaft is fixedly connected with a stirring rod, a brush is fixedly mounted on one side of the stirring rod, a reaction bin is fixedly mounted on the inner wall of the top of the shell, a heat conduction pipe is arranged inside the reaction bin, a discharging pipe is fixedly mounted at the bottom of the reaction bin, an electromagnetic valve is arranged on the discharging pipe, a collecting box is movably mounted inside the shell and is positioned below the discharging pipe, a fixing plate and a guide plate are fixedly mounted on the inner side wall of the shell, a liquid outlet is formed in the bottom of the guide plate, and a medium recovery box is arranged below the guide plate, and the medium recycling box is positioned under the liquid outlet, the right side wall of the shell is fixedly provided with a control panel, the front surface of the shell is provided with an inspection window, the left side wall of the shell is fixedly provided with an air heater, and one side of the air heater is fixedly connected with a vent pipe.

Preferably, a bearing is fixedly installed inside the housing.

Preferably, the bottom of the reaction bin is designed to be inclined.

Preferably, the bottom of the collecting box is provided with a filtering hole.

Preferably, the fixed plate is arranged above the guide plate, and the top of the fixed plate is provided with the collecting box.

Preferably, the motor, the electromagnetic valve and the air heater are all electrically connected with the control panel.

Preferably, the front face of the shell is movably connected with a cabinet door, a hinge and a handle are arranged on the cabinet door, and the shell is connected with the cabinet door through the hinge.

Compared with the prior art, the beneficial effects of the utility model are that:

(1) this MOFs material crystal seed synthesizer, through setting up the motor, a rotating shaft, the puddler, the brush, air heater and heat pipe, when the device during operation, open the air heater, the air heater lets in steam in the heat pipe, thereby make the inside temperature in reaction storehouse rise fast, thereby improve synthetic reaction efficiency, through opening the motor, the motor drives pivot and puddler rotation, thereby stir the inside material in reaction storehouse, accelerate the reaction rate between the material, and the stirring can make material and reaction medium reaction more even, thereby make synthetic reaction better, the quality is higher.

(2) This MOFs material crystal seed synthesizer, through setting up collecting box, filtration pore, guide plate, liquid outlet and medium recycling bin, the collecting box can be collected the material after the synthetic reaction, and the setting of filtration pore in the bottom can let remaining reaction medium flow into the medium recycling bin that the below set up through the filtration pore in, be convenient for to the recycle of surplus reaction medium to reduce cost.

Drawings

Fig. 1 is a schematic perspective view of the present invention;

fig. 2 is a main sectional view of the present invention;

fig. 3 is a left side sectional view of the present invention.

In the figure: 1. a housing; 2. a feed inlet; 3. a motor case; 4. a motor; 5. a motor shaft; 6. a rotating shaft; 7. a stirring rod; 8. a brush; 9. a reaction bin; 10. a heat conducting pipe; 11. a discharging pipe; 12. an electromagnetic valve; 13. a collection box; 14. filtering holes; 15. a fixing plate; 16. a baffle; 17. a liquid outlet; 18. a media recovery tank; 19. a control panel; 20. a viewing window; 21. a cabinet door; 22. a hinge; 23. a handle; 24. a hot air blower; 25. a breather tube.

Detailed Description

The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.

Referring to fig. 1-3, the present invention provides a MOFs material seed crystal synthesizer, which comprises a housing 1, a charging opening 2 is disposed at the top of the housing 1, a motor box 3 is fixedly mounted at the top of the housing 1, a motor 4 is fixedly mounted inside the motor box 3, a motor shaft 5 is rotatably connected to the bottom of the motor 4, a rotating shaft 6 is fixedly connected to the bottom of the motor shaft 5, a stirring rod 7 is fixedly connected to the side wall of the rotating shaft 6, a brush 8 is fixedly mounted at one side of the stirring rod 7, a reaction chamber 9 is fixedly mounted on the inner wall of the top of the housing 1, a heat conducting pipe 10 is disposed inside the reaction chamber 9, a discharging pipe 11 is fixedly mounted at the bottom of the reaction chamber 9, a solenoid valve 12 is disposed on the discharging pipe 11, a collecting box 13 is movably mounted inside the housing 1, the collecting box 13 is located below the discharging pipe 11, a fixing plate 15 and a guide plate 16 are fixedly mounted on the inner side wall of the housing 1, and a liquid outlet 17 is disposed at the bottom of the guide plate 16, a medium recycling box 18 is arranged below the guide plate 16, the medium recycling box 18 is located under the liquid outlet 17, a control panel 19 is fixedly mounted on the right side wall of the shell 1, an inspection window 20 is formed in the front face of the shell 1, an air heater 24 is fixedly mounted on the left side wall of the shell 1, and a vent pipe 25 is fixedly connected to one side of the air heater 24.

In this embodiment, preferably, the bearing is fixedly installed inside the housing 1, and the friction force generated between the housing 1 and the motor shaft 5 is reduced by the arrangement of the bearing, so that the service life of the motor shaft 5 is prolonged.

In this embodiment, preferred, reaction bin 9 bottom is the slope design, and the slope design of bottom compares the unloading that can be more convenient quick with horizontal design, and can avoid material sediment reaction bin 9 bottom.

In this embodiment, preferably, the bottom of the collection box 13 is provided with a filter hole 14, and the through hole is provided with a filter hole 14, so that the material after the synthesis reaction is finished can be filtered, and the remaining reaction medium is filtered through the filter hole 14.

In this embodiment, preferably, the fixing plate 15 is disposed above the guide plate 16, the collecting box 13 is mounted on the top of the fixing plate 15, and the two ends of the bottom of the collecting box 13 are placed on the fixing plate 15, so that the position of the collecting box 13 is fixed, materials are conveniently collected, and the collecting box 13 is conveniently detached.

In this embodiment, preferably, the motor 4, the electromagnetic valve 12 and the air heater 24 are all electrically connected to the control panel 19, and in an electrically connected manner, the control panel 19 is convenient for a worker to control the motor 4, the electromagnetic valve 12 and the air heater 24.

In this embodiment, it is preferred, casing 1 openly swing joint has cabinet door 21, is provided with hinge 22 and handle 23 on the cabinet door 21, and casing 1 and cabinet door 21 are connected through hinge 22, and the setting of this structure is convenient for the staff to open and close casing 1 to be convenient for operate casing 1 is inside.

The utility model discloses a theory of operation and use flow: when the device is used, a worker firstly adds a reaction medium into a reaction bin 9, an air heater 24 is started, the air heater 24 sends hot air into a heat conduction pipe 10 through a vent pipe 25, so that the temperature inside the reaction bin 9 is improved, at the moment, a synthetic reaction raw material is added from a feed inlet 2, a motor 4 is started simultaneously, the motor 4 drives a motor shaft 5 and a rotating shaft 6 to rotate, the rotating shaft 6 rotates to drive a stirring rod 7 and a brush 8 to rotate, the stirring rod 7 rotates to stir materials inside the reaction bin 9, so that the raw materials are more comprehensively contacted with the reaction medium, the synthetic reaction speed and the reaction quality are improved, insufficient reaction of the raw materials is avoided, the reaction result is influenced, the arrangement of the brush 8 is realized, the side wall of the reaction bin 9 is cleaned, the materials are prevented from remaining on the side wall of the reaction bin 9, the reaction quality is improved, the reaction cost is reduced, after the synthetic reaction is finished, open solenoid valve 12, the material flows to in the collecting box 13 through unloading pipe 11, and through the filtration pore 14 that sets up in the bottom of collecting box 13, can filter remaining reaction medium, and reaction medium flows to in the medium collection box 18 through guide plate 16 and the liquid outlet 17 of below to retrieve remaining reaction medium, then can reuse, practice thrift the cost.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims

1. A MOFs material crystal seed synthesis device, comprising a shell (1), characterized in that: the feeding port (2) is formed in the top of the shell (1), the motor box (3) is fixedly mounted at the top of the shell (1), the motor (4) is fixedly mounted in the motor box (3), the motor shaft (5) is rotatably connected to the bottom of the motor (4), the rotating shaft (6) is fixedly connected to the bottom of the motor shaft (5), the stirring rod (7) is fixedly connected to the side wall of the rotating shaft (6), the brush (8) is fixedly mounted on one side of the stirring rod (7), the reaction bin (9) is fixedly mounted on the inner wall of the top of the shell (1), the heat conduction pipe (10) is arranged in the reaction bin (9), the discharging pipe (11) is fixedly mounted at the bottom of the reaction bin (9), the electromagnetic valve (12) is arranged on the discharging pipe (11), the collecting box (13) is movably mounted in the shell (1), and the collecting box (13) is positioned below the discharging pipe (11), casing (1) inside wall fixed mounting has fixed plate (15) and guide plate (16), liquid outlet (17) have been seted up to guide plate (16) bottom, guide plate (16) below is provided with medium collection box (18), and medium collection box (18) are located under liquid outlet (17), casing (1) right side wall fixed mounting has control panel (19), inspection window (20) have openly been seted up in casing (1), casing (1) left side wall fixed mounting has air heater (24), air heater (24) one side fixedly connected with breather pipe (25).

2. A MOFs material seed synthesis apparatus according to claim 1, wherein: and a bearing is fixedly arranged in the shell (1).

3. A MOFs material seed synthesis apparatus according to claim 1, wherein: the bottom of the reaction bin (9) is designed to be inclined.

4. A MOFs material seed synthesis apparatus according to claim 1, wherein: the bottom of the collecting box (13) is provided with a filtering hole (14).

5. A MOFs material seed synthesis apparatus according to claim 1, wherein: the fixed plate (15) is arranged above the guide plate (16), and the collecting box (13) is arranged at the top of the fixed plate (15).

6. A MOFs material seed synthesis apparatus according to claim 1, wherein: the motor (4), the electromagnetic valve (12) and the hot air blower (24) are electrically connected with the control panel (19).

7. A MOFs material seed synthesis apparatus according to claim 1, wherein: the front face of the shell (1) is movably connected with a cabinet door (21), a hinge (22) and a handle (23) are arranged on the cabinet door (21), and the shell (1) is connected with the cabinet door (21) through the hinge (22).